• 한국세라믹학회지
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• 제26권3호
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• pp.445-451
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• 1989

Hydrolysis of aluminum isopropoxide with excess water in the presence of excess isopropyl alcohol resulted in the formation of boehmite in independence of temperature of hydrolysis and aging. Stoichiometric and substoichiometric amount of water hydrolyzed aluminum isopropoxide to pseudo-boehmite and amorphous one, respectively. $\alpha$-Al2O3 with 0.3${\mu}{\textrm}{m}$ in median size was produced by calcination of boehmite, bseudo-boehmite and amorphous boehmite at 125$0^{\circ}C$, 120$0^{\circ}C$, and 115$0^{\circ}C$ for one hour, respectively. Singnificant reduction in particle size was found during transition from $\theta$-Al2O3 to $\alpha$-Al2O3. $\alpha$-Al2O3 produced in this study was relatively uniform spherical and its purity was found to be over 99.9%.

• The Korean Journal of Ceramics
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• 제3권2호
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• pp.116-123
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• 1997

A chemically stabilized $\beta$-cristobalite, which is stabilized by stuffing cations of $Ca^{2+}$ and $Al^{3+}$, was prepared by a solution-polymerization route employing Pechini resin or PVA solution as a polymeric carrier. The polymeric carrier affected the crystallization temperature, morphology of calicined powder, and particle size distribution. In case of the polyvinyl alcohol (PVA) solution process, a fine $\beta$-cristobalite powder with a narrow particle size distribution (average particle size : 0.3$\mu\textrm{m}$) and a BET specific surface area of 72 $\m^2$/g was prepared by an attrition-milling for 1 h after calcination at 110$0^{\circ}C$ for 1h. Wider particle size distribution and higher specific surface area were observed for the $\beta$-cristobalite powder derived from Pechini resin. The cubie(P1-to-tetraganalb) phase transformation in polynystalline $\beta$-cristobalite was induced at approximately 18$0^{\circ}C$. Like other materials showing transformation toughening, a critical size effect controlled the $\beta$-to-$\alpha$ transformation. Densifed cristobalite sample had some cracks in its internal texture after annealing. The cracks, occurred spontaneoulsy on cooling, were observed in the sample with an average grain sizes of 4.0 $\mu\textrm{m}$ or above. In case of the sintered cristobalite having a composition of CaO.$2Al_2O_3$.40SiO$_2$, small amount of amorphous phase and slow grain growth during annealing were observed. Shear stress-induced transformation was also observed in ground specimen. Cristobalite having a composition of CaO.2Al2O3.80SiO2 showed a more sensitive response to shear stress than the CaO.$2Al_2O_3$.40SiO$_2$ type cristobalite. Shear-induced transformation resulted in an increase of volume about 13% in $\alpha$-cristobalite phase on annealing for above 10 h in the case of the former composition.

• Applied Microscopy
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• 제19권2호
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• pp.119-137
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• 1989

Turtle bladder의 상피조직(上皮組織)과 세포막(細胞膜) 투과성(透過性)을 분석하기 위하여 동결절단법(凍結切斷法)을 적용(適用)하여 전자현미경(電子顯微鏡) 관찰을 하였으며 그 결과 다음과 같이 요약(要約)된다. 1. 방광상피(膀胱上皮)의 3가지 주요세포형(主要細胞形)은 granular-cell, ${\alpha}$ 및 ${\beta}$형(形)의 CA-rich cell로서 구분된다. 2. 과립성세포(顆粒性細胞)의 주요기능(主要機能)은 $Na^+$ 재흡수(再吸收)이며, 두 단계(段階)의 수송과정(輸送過程)으로 설명되며 정단세포막(頂端細胞膜)을 통한 $Na^+$의 세포내(細胞內) 확산이동(擴散移動)과 그후 기저막(基底膜)에 위치한 $Na^{+}\;-K^{+}$ 펌프에 의한 능동수송과정(能動輸送過程)이다. 3. ${\alpha}$ 및 ${\beta}$형(形) CA-rich cell은 $Na^+$ 수송(輸送)에 관여하지 않으며, ${\alpha}$형(形)의 CA-cell은 정단세포막(頂端細胞膜)의 proton펌프를 이용하여 proton 분필(分泌)에 관여한다. 또한 ${\beta}$형(形)의 CA-cell는 정단세포막(頂端細胞膜)을 통한 $HCO_{3}^-$ 분필수송(分泌輸送)의 기능을 가지고 있다. 4. 동결절단법(凍結切斷法)의 적용하에 세포막표면(細胞膜表面)의 특성(特性)을 관찰한 바, ${\alpha}$형(形)의 CA-cell의 정단세포막(頂端細胞膜)은 proton펌프를 함유하는 것으로 보이는 intramembrane particle이 다수 관찰되고 있으며, ${\beta}$형(形) CA-cell은 기저세포막(基底細胞膜)에서 이와같은 intramembrane particle이 나타나고 있다. 5. 상술(上述)한 두 type의 CA-cell에서 수송특성(輸送特性)의 차이는 proton 및 $HCO_{3}^-$ 분필수송(分泌輸送)이 서로 반대의 방향으로 일어나는 것으로 사료된다.

• 한국결정성장학회지
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• 제7권1호
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• pp.47-58
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• 1997

본 연구에서는 수열성장법을 이용해서 알루미늄 수화물인 깁사이트로부터 코런덤($\alpha$-$Al_2O_3$) 단결정 분말을 제조하였으며, 주요 반응인자로서 광화제와 성장기질의 특성이 생성물의 입도분포와 결정성에 미치는 영향을 조사했다. 실험결과 성장용액의 용해도를 증가시키기 위해 광화제로 사용된 KOH의 첨가량이 증가할수록 코런덤 입자의 크기가 커졌고, 수열반응 온도는 낮아졌으나, 영양제인 깁사이트의 농도가 증가할수록 합성된 코런덤 입자는 작아졌다. 성장기질의 물성특성 차이에 따라 수열합성 조건이 달라졌다. 수열합성을 통해 400~$470^{\circ}C$인 반응온도 범위에서 1~10 $\mu \t extrm{m}$ 정도의 중량평균 입경을 갖는 육방정의 코런덤 결정을 합성하였다.

• 한국세라믹학회지
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• 제28권12호
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• pp.996-1004
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• 1991

In this study, we tried to synthesis iron hydroxide suitable for longitudinal magnetic recording media from waste acid, which is a by-product of an iron works factory. Effects of initial pH of reactants, reaction temperature, reaction time for the synthesis of acicular iron hydroxide were studied in relation to particle properties of iron hydroxide and magnetic properties of maghemite powders. As the pH in reactant solution increased, $\beta$-FeOOH(pH=4.5), mixture of $\beta$-FeOOH and $\alpha$-FeOOH(4.5$\alpha$-FeOOH and Fe3O4(6.4$\alpha$-FeOOH (pH>13) was found to from in order. Especially, $\alpha$-FeOOH formed above pH 13 was single phase with superior acicularity. The temperature range over which the single-phase goethite can be formed increased as the initial pH of reactants increased (pH 13:10~5$0^{\circ}C$, pH 13.2:10~7$0^{\circ}C$, pH 13.5:0~8$0^{\circ}C$). The goethite formed between 40~6$0^{\circ}C$ has superior characteristics because the acicularity increased with increasing temperature but at high temperature (>6$0^{\circ}C$) Fe3O4 (pH=13) was found to start to form. Generally, single phase of goethite was found to form after one hour when an optimized condition. The particle size of goethite did not change as the reaction time increased over one hour. Accordingly, the magnetic properties of ${\gamma}$-Fe2O3 produced from goethite were not altered.

• 한국추진공학회지
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• 제17권5호
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• pp.27-36
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• 2013

본 연구에서는 고체로켓 모터의 연소 불안정성을 예측하고 분석 할 수 있는 해석도구의 개발을 위해 음향에너지의 분석과 선형 안정성 해석을 수행하였다. 음향 해석의 경우 상용 프로그램인 COMSOL을 이용하여 단면적이 일정한 실린더 형상의 연소실 음향 해석 및 모드 해를 도출하였다. Culick에 의해 정립된 고체추진 로켓의 선형 안정성 해석에 기초하여 연소 불안정성을 진단하였으며 압력결합, 노즐감쇠, 입자감쇠의 안정성 요소(stability alpha) 외에 유동방향변환(flow turning) 요소와 점성감쇠(viscous loss) 요소를 추가하여 연료 표면 근처의 유동 및 점성효과를 포함하는 연소 불안정의 경향을 파악하였다. 또한 입자의 크기에 따른 주파수 영역별 연소 불안정 감쇠 특성을 파악하였다.

• 한국입자에어로졸학회지
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• 제9권4호
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• pp.209-219
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• 2013

We have used the modified diffusion flame burner to synthesize silica coated iron oxide nanoparticles having enhanced superparamagnetic property. Silica-encapsulated iron oxide particles were directly observed using a high resolution transmission electron microscope. From the energy dispersive X-ray spectroscopy (EDS) and zeta potential measurements, the iron oxide particles were found to be completely covered by a silica coating layer. X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD) measurements revealed that the iron oxide core consists of ${\gamma}-Fe_2O_3$ rather than ${\alpha}-Fe_2O_3$. Our magnetization measurements support this conclusion. Biocompatibility test of the silica-coated iron oxide nanoparticles is also conducted using the protein adsorption onto the coated particle.

• 한국의학물리학회지:의학물리
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• 제8권1호
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• pp.47-52
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• 1997

양성자나 알파입자와 같은 무거운 하전입자가 매질 속을 진행하는 경우에 매질과 상호작용 하여 일어날 수 있는 물리적인 현상을 알아보기 위하여 몬테칼로 기법을 이용하여 시뮬레이션 하였다. 양성자선의 Bragg peak가 에너지의 증가에 따라 물 속에서 깊어짐을 확인하였다. 이러한 Bragg peak 현상을 방사선치료에 이용할 경우에 표적 조직의 흡수선량이 광자와 전자선에 비하여 국소화 되고 주변조직의 보호효과가 탁월함을 알 수 있었다.

• 열처리공학회지
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• 제9권1호
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• pp.62-68
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• 1996

In order to establish making process of water atomized iron powder for powder metallurgy, effect of heat treatment condition on change of powder properties and impurities was investigated at each tempeature of $850{\sim}950^{\circ}C$. The results are as follows. Particle morphology of iron powder changed slightly from sphercial type to irregular type and the amount of fine particle decreased more and more with increasing of heat treatment time at each temperature. The flow rate and apparent desity of iron powder also decreased due to particle coalescence in order of $850^{\circ}C$, $950^{\circ}C$, $900^{\circ}C$. Those powder Properties became to decrease particularly at $900^{\circ}C$ in alpha iron region. On the other hand, residual carbon and oxygen contents in iron powder decreased extremely with increasing of heat treatment temperature and time.

• 한국군사과학기술학회지
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• 제14권3호
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• pp.517-523
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• 2011

The estimation filter in radar systems must track targets' position within low tracking error. In the Multi-Function Radar(MFR), ${\alpha}-{\beta}$ filter and Kalman filter are widely used to track single or multiple targets. However, due to target maneuvering, these filters may not reduce tracking error, therefore, may lost target tracks. In this paper, a target tracking filter based on particle filtering algorithm is proposed for the MFR. The advantage of this method is that it can track targets within low tracking error while targets maneuver and reduce impoverishment of particles by the proposed resampling method. From the simulation results, the improved tracking performance is obtained by the proposed filtering algorithm.