• Title/Summary/Keyword: Alpha phase

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Effect of α-Fe Content on the Magnetic Properties of MnBi/α-Fe Nanocomposite Permanent Magnets by Micro-magnetic Calculation

  • Li, Y.Q.;Yue, M.;Zuo, J.H.;Zhang, D.T.;Liu, W.Q.;Zhang, J.X.;Guo, Z.H.;Li, W.
    • Journal of Magnetics
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    • v.18 no.3
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    • pp.245-249
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    • 2013
  • A finite element model was built for MnBi/${\alpha}$-Fe nanocomposite permanent magnets, and the demagnetization curves of the magnets were simulated by micro-magnetic calculation. The microstructure of the cubic model is composed of 64 irregular grains with an average grain size of 20 nm. With the volume fraction of soft magnetic phase (t vol. %) ranged from 5 to 20 vol. %, both isotropic and anisotropic nanocomposite magnets show typical single-phase permanent magnets behavior in their demagnetization curves, illustrating good intergranular exchange coupling effect between soft and hard magnetic phases. With the increase of volume fraction of soft magnetic phase in both isotropic and anisotropic magnets, the coercive force of the magnets decreases monotonically, while the remanence rises at first to a peak value, then decreases. The optimal values of maximum energy products of isotropic and anisotropic magnets are 84 and $200kJ/m^3$, respectively. Our simulation shows that the MnBi/${\alpha}$-Fe nanocomposite permanent magnets own excellent magnetic properties and therefore good potential for practical applications.

Characterization of Microstructure and Mechanical Properties of Mg-8Li-3Al-1Y Alloy Subjected to Different Rolling Processes

  • Zhou, Xiao;Liu, Qiang;Liu, Ruirui;Zhou, Haitao
    • Metals and materials international
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    • v.24 no.6
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    • pp.1359-1368
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    • 2018
  • The mechanical properties and microstructure evolution of Mg-8Li-3Al-1Y alloy undergoing different rolling processes were systematically investigated. X-ray diffraction, optical microscope, scanning electron microscopy, transmission electron microscopy as well as electron backscattered diffraction were used for tracking the microstructure evolution. Tensile testing was employed to characterize the mechanical properties. After hot rolling, the $MgLi_2Al$ precipitated in ${\beta}-Li$ matrix due to the transformation reaction: ${\beta}-Li{\rightarrow}{\beta}-Li+MgLi_2Al+{\alpha}-Mg$. As for the alloy subjected to annealed hot rolling, ${\beta}-Li$ phase was clearly recrystallized while recrystallization rarely occurred in ${\alpha}-Mg$ phase. With regard to the microstructure undergoing cold rolling, plenty of dislocations and dislocation walls were easily observed. In addition, the microstructure of alloys subjected to annealed cold rolling revealed the formation of new fresh ${\alpha}-Mg$ grains in ${\beta}-Li$ phase due to the precipitation reaction. The mechanical properties and fracture modes of Mg-8Li-3Al-1Y alloys can be effectively tuned by different rolling processes.

Adjusting GPC Control Parameters Based on Gain and Phase Margins

  • Haeri, Mohammad
    • 제어로봇시스템학회:학술대회논문집
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    • 2004.08a
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    • pp.1838-1842
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    • 2004
  • Gain and phase margins of a first order plus delayed time (FOPDT) process controlled by generalized predictive controller (GPC) are related to the control parameters ${\lambda}$ (control move suppression parameter) and ${\alpha}$ (smoothing filter coefficient) and the normalized delay of the process. Variation ranges of gain and phase margins are determined. It is shown that the margins cannot be assigned independently for a wide range of variation and the range is narrowing by increase of the normalized delay of the process. And finally curves are given to use for adjustment of the controller parameters in order to obtain a specific pair of gain and phase margins.

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3-Dimensional SVM Technique for the Three-Phase Four-Leg Voltage Source Inverter System (3상 4레그 전압형 인버터를 위한 3차원 공간벡터변조 기법)

  • Doan, Van-Tuan;Choi, Woo-Jin
    • Proceedings of the KIPE Conference
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    • 2013.11a
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    • pp.111-112
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    • 2013
  • The three-phase four-leg voltage source inverter (VSI) topology can be an interesting option for the three phase-four wire system. With an additional leg, this topology can handle the neutral current, hence the DC link capacitance can be reduced significantly. In this paper the three dimensional space vector modulation (3D SVM) in ${\alpha}{\beta}{\gamma}$ coordinates for the three-phase four-leg VSI is presented. By using the 3D SVM method, the DC link voltage can be reduced by 16% compared with the split DC link capacitor topology and the output distortion can also be reduced under the unbalanced load condition.

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Effects of Low Temperature Plasma Nitriding Treatment on Mechanical Properties of Stainless Steel (스테인리스강의 기계적 성질에 미치는 저온 플라즈마 질화처리조건의 영향)

  • Bin, Jeonguk;Kim, Hangoon
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.5
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    • pp.269-276
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    • 2010
  • This study has been carried out to the low temperature plasma nitriding treatment on the mechanical properties of stainless steel at temperature range between $400^{\circ}C$ and $500^{\circ}C$. It was found that there was precipitated to free CrN matrix below $400^{\circ}C$ and there was precipitated S-phase of STS 316L, ${\varepsilon}$-phase of STS 409L and ${\alpha}N$-phase of STS 420J2. STS 316L has formed relatively abundant CrN phase and ${\gamma}^{\prime}-Fe_4N$ phase at $500^{\circ}C$, alternatively STS 409L and STS 420J2 were more deeply nitrided than STS 316L at $500^{\circ}C$.

Preparation and Magnetic Properties of Amorphous Spinel Ferrite (비정질 Spinel Ferrite의 제조와 그 자기적 특성)

  • 김태옥;김창곤
    • Journal of the Korean Magnetics Society
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    • v.2 no.1
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    • pp.29-36
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    • 1992
  • The fundamental research about the amorphous ferrite, which is expected as the important material for electronic and information imdustry in future, was carried out in this work. Because the ferromagnetic amorphous ferrites reported recently are very inferior in magnetic properties than the crystalline ferrites, the development of the more ferromagnetic amorphous ferrites is required. In order to obtain the fundamental data for the preparation of amorphous ferrites, the hand-made twin-roller quenching apparatus was used for rapid quenching. Investigation on amorphous ferrite in the system $CaO-Bi_{2}O_{3}-Fe_{2}O_{3}$ has been carried out in the composition of 10-50 mole% CaO, 10-50 mole% $Bi_{2}O_{3}$, 40-70 mole% $Fe_{2}O_{3}$. Large magnetization values were obtained near the composition of the mixture of $BiFeO_{3}$ and $CaFe_{4}O_{7}$. Especially, an amorphous ${(CaO)}_{20}{(Bi_{2}O_{3})_{15}{(Fe_{2}O_{3})}_{65}$ specimen has a magmetization value of about 21.84 emu/g at 0K(10 kOe). Fe $M\"{o}ssbauer$ absorption spectrum indicates that this specimen is compsed of two amorphous phases, antiferromagnetic phase($\alpha$-phase) and ferromagnetic phase($\beta$-phase). Crystallization of this amorphous ferrite was happened in steps-$550^{\circ}C$ and $775^{\circ}C$, then observed crystal phases were perovskite phase of $BiFeO_{3}$ and $Fe_{2}O_{3}$ phase.

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Characterization of LiCoO2 Synthesized via Structural and Compositional Variations of Precursors Prepared by Precipitation (침전법으로 제조된 전구체 성질에 의한 LiCoO2의 특성에 관한 연구)

  • Jeong, Myoung Kuk;Hwang, Chi Seok;Choi, Cheong Song
    • Clean Technology
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    • v.12 no.2
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    • pp.101-106
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    • 2006
  • HT-$LiCoO_2$ powders were synthesized from hydroxide precursors in this study. The cobalt hydroxide compounds with hydrotalcite-like(${\alpha}$-phase) and/or brucite-like(${\beta}$-phase) structures as a component of the precursor were prepared in various PH conditions using precipitation method. It was found that various phase and compositions of cobalt hydroxides could be tailor-prepared via a careful control of preparation parameters such as the concentration ratio of $[OH^-]/[CO^{2+}]$ and aging time. The hydroxides $Co(OH)_2$ and LiOH were mixed with aqueous methyl-alcohol. The precursor of a HT-$LiCoO_2$ was synthesized via subsequent processes including evaporation, drying and aging. The transformation of tailor-made ${\beta}$-phase $Co(OH)_2$ to CoOOH and formation of solid solution in the precursor were achieved during aging. These results cause HT-$LiCoO_2$ to be synthesized at low temperature($600^{\circ}C$ ) for a short time(10min).

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Formation and Microstructure Characteristics of $\beta-Al_5FeSi$ Intermetallic Compound in the Al-Si-Cu Alloys with the Variation of Fe Content (Al-Si-Cu합금에서 Fe 함량에 따른 $\beta-Al_5FeSi$ 금속간화합물의 형성 및 응고미세조직 특성)

  • Kim, Bong-Hwan;Lee, Sang-Mok
    • Journal of Korea Foundry Society
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    • v.29 no.5
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    • pp.225-232
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    • 2009
  • For comprehensive understanding of the formation behavior of $\beta-Al_5FeSi$ phase in Al-Si-Cu alloys with the existence of Fe element, microstructure characterizations were performed using combined analysis of OM, SEM-EDS, XRD. Especially, experimental and predictive works on solidification events of $\beta-Al_5FeSi$ phase as well as other phases formed together with $\beta-Al_5FeSi$ have been carried out by using DSC analysis and Java-based Materials Properties software (J. Mat. Pro.). Primary and eutectic $\beta-Al_5FeSi$ phases were able to distinguish from each other on microstructures by their morphological features. Primary $\beta-Al_5FeSi$ phase was seen to have rough surface perpendicular to growth direction, indicating free attachment of solute atoms in liquid state. On the other hand, the eutectic $\beta-Al_5FeSi$ phase was formed with plain and straight surface during eutectic reaction together with $\alpha$-Al phase. The eutectic reaction of $\beta-Al_5FeSi$ and $\alpha$-Al phases was seen to be able to separate into each formation depending on cooling rate.

SAR Data Correction Based on Calibrated-Scatterometer Measurements (보정된 Scatterometer의 측정데이터를 사용한 SAR 데이터 교정)

  • 정구준;홍진영;오이석
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.15 no.2
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    • pp.121-126
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    • 2004
  • This paper presents an SAR-data calibration technique using a well-calibrated scatterometer. At first a fully-polarimetric antenna pattern(magnitude and phase) of the antenna main-beam using a conducting sphere was measured. Then, this data were used to calibrate polarimetrically an auto-mounted network analyzer-based scatterometer system. This scatterometer system can be used to measure the accurate Mueller matrices of earth surfaces such as grass fields, rice fields and bare soil surfaces; i.e., the phase-difference parameters can be obtained as well as the radar scattering coefficients. If a polarimetrically calibrated scatterometer is operated at the same time with the SAR system, the scatterometer data can be used to correct the SAR data, especially the phase-difference parameters. It was found that the correction effect is remarkable for the degree of correlation ${\alpha}$, which is one of the phase-difference parameter, while the correction effect is negligible for the magnitude parameters(backscattering coefficients).

Effect of Increased Oxygen Content due to Intensive Milling on Phase and Microstructural Development of Silicon Nitride

  • Kim, Hai-Doo;Ellen Y. Sun;Paul F. Becher;Kim, Hyo-Jong;Han, Byung-Dong;Park, Dong-Soo
    • Journal of the Korean Ceramic Society
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    • v.38 no.5
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    • pp.405-411
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    • 2001
  • Compacts of a mixture of fine $\alpha$-Si$_3$N$_4$powders, 6% $Y_2$O$_3$and 1% $Al_2$O$_3$were attrition milled time on phase and microstructural development in silicon nitride ceramics. The sintered surface and the interior showed different behaviors in phase and microstructral developments. Increased oxygen content with increased milling time of powder mixture leads to the formation of Si$_2$$N_2$O phase at temperatures as low as 155$0^{\circ}C$. Si$_2$$N_2$O is stable in the interior of the samples but unstable in the surface region of the specimen sintered at higher temperature. This results in a duplex structure where the interior consists of Si$_2$$N_2$O grains dispersed in $\beta$-Si$_3$N$_4$matrix and a surface which contains only $\beta$-Si$_3$N$_4$. The alpha to beta phase transformation and the microstructural development are shown to be influenced by the formation and decomposition of the Si$_2$$N_2$O.

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