• Title/Summary/Keyword: Aging heat treatment

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The Effect of Heat Treatment on the Martensitic Transformation in an Cu-Al-Ni Single Crystal (Cu-Al-Ni계 단결정 합금의 마르텐사이트 변태특성에 미치는 열처리의 영향)

  • Kim, Y.S.;Jang, W.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.3
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    • pp.177-182
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    • 2000
  • The effects of betatizing and aging temperatures on the martensitic transformation characteristics in an Cu-13.4wt%Al-4.2wt%Ni single crystal have been studied. Microstructures show that the specimen betatized above $800^{\circ}C$ has only ${{\beta}_1}^{\prime}$ martensite while the specimen betatized of below $700^{\circ}C$ has two phases i.e., ${{\beta}_1}^{\prime}+{\gamma}_2$ When betatizing temperature increase from $600^{\circ}C$ upto $900^{\circ}C$, Ms and As temperatures decrease due to the dissolution of which ${\gamma}_2$ phase depletes Al content in the matrix thereafter makes the both Ms and As temperatures significantly increased. Ms and As temperatures of the specimen aged at $200^{\circ}C$ are relatively stable but those of the specimen aged at $300^{\circ}C$ are shifted rapidly with aging time, especially within the first 30min.

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Mechanical Properties of Ti-Zr-Nb-Pd Based Alloys for Biomedical Applications (생체용 Ti-Zr-Nb-Pd계 합금의 기계적 성질)

  • Jung, Jong-Hyun
    • Journal of Technologic Dentistry
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    • v.24 no.1
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    • pp.95-104
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    • 2002
  • For biomedical applications, Ti-X%Zr-Y%Nb-0.2%Pd(X:10$\sim$20, Y:2$\sim$8) alloys not containing harmful Al and V were newly designed, and the effect of alloy composition and heat treatment on the microstructure and mechanical properties was investigated. From the results, it was shown that the mechanical properties were enhanced with the addition of Zr or Nb. The effect of heat treating on room temperature strength was investigated by aging treatment after solution treatment. The mechanical properties of Ti-20%Zr-4%Nb-0.2%Pd alloy aged at 400$^{\circ}C$ for 10hrs was found to be superior to those of the pure Ti and Ti-6%Al-4%V ELI alloy.

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A Study of Tensile Strength in 18% Ni Maraging Steel Sheet Welded with Electron Beam (E.B 용접된 18% Ni 마르에이징강 박판의 인장이음강도에 관한 연구)

  • 정병호;김무길;김원녕
    • Journal of Advanced Marine Engineering and Technology
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    • v.21 no.2
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    • pp.157-165
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    • 1997
  • The strength level of welded joint in room temperature and elevated temperature up to $600^{\circ}C$ was investigated in 250 and 300 grade 18% Ni maraging steel sheet welded with electron beam. The results obtained in this study are as follows; 1. Optimum welding heat input was 600J/cm in 1.0mm thickness and the room temperature tensile strength, joint efficiency of welded joint treated with optimum aging condition were found to be about 166kg/$mm^2$, 95% in 250 grade, 189kg/$mm^2$, 92% in 300 grade maraging steel sheet, respectively. 2. Tensile strength of welded joint in room temperature increased slightly by aging after repeated solution heat treatment, but the fracture mode showed a shear. 3. Joint efficiency at a temperature between $540^{\circ}C$and $600^{\circ}C$ found to be about 72% to 55%, but the joint efficiency exceeded about 90% below $300^{\circ}C$. 4. The fracture occurred in most weld metal, and the fracture surface showed a shallow dimple.

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A Study on the Precipitation Behavior of $L2_1$-type $Ni_2AlTi$ Phase in B2-Ordered NiAl System (B2-규칙 NiAl계에 $L2_1$$Ni_2AlTi$상의 석출거동에 관한 연구)

  • Han, Chang-Suk
    • Journal of the Korean Society for Heat Treatment
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    • v.20 no.4
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    • pp.187-194
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    • 2007
  • A transmission electron microscope (TEM) investigation has been performed on the precipitation of $L2_1$-type $Ni_2AlTi$ phase in B2-ordered NiAl system. The hardness after solution treatment is high in NiAl-Ti alloys suggesting the large contribution of solid solution strengthening in this alloy system. However, the amount of age hardening is not large as compared to the large microstructural variations during aging. At the beginning of aging, the $L2_1$-type $Ni_2AlTi$ precipitates keep a lattice coherency with the NiAl matrix. By longer periods of aging $Ni_2AlTi$ precipitates lose their coherency and change their morphology to the globular ones surrounded by misfit dislocations. Misfit dislocations, which are observed on {100} planes of H-precipitates have the Burgers vector of a <100> with a pure edge type. The lattice misfits of NiAl-$Ni_2AlTi$ system is estimated from the spacings of misfit dislocations to be 1.1% at 1273 K. The lattice misfits decrease with increasing aging temperature in this system.

Heat Treatment of AZ91-5wt.%Sn Magnesium Alloy (AZ91-5wt.%Sn 마그네슘 합금의 열처리의 특성)

  • Kim, Dae-Hwan;Lim, Su-Gun
    • Journal of Korea Foundry Society
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    • v.37 no.1
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    • pp.14-20
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    • 2017
  • The microstructure, electrical conductivity and hardness variation of an AZ91-5wt%Sn Mg alloy sample during a solid-solution and aging heat treatment were instigated by optical microscopy, scanning electron microscopy, X-ray diffraction and by Rockwell hardness techniques in this study. The XRD result shows that the main phases in the as-casted alloy are ${\alpha}$-Mg, $Mg_{17}Al_{12}$ and $Mg_2Sn$. From the SEM images of the AZ91-5wt%Sn Mg alloy after the solution treatment, the $Mg_{17}Al_{12}$ phases in the alloy were found to have dissolved into the matrix with an increase in the holding time during the solution treatment, but $Mg_2Sn$ phases were clearly observable. The highest peak hardness of the AZ91-5wt%Sn Mg alloy is 82HRE at an aging temperature of $200^{\circ}C$.

The Study on the Migration of Carbon in T23/T91 Dissimilar Metal Welds for Boiler (보일러용 T23/T91 이종용접부의 탄소이동에 관한 연구)

  • Park, Ki-Duck;Jung, Byong-Ho;Kang, Chang-Yong
    • Journal of the Korean Society for Heat Treatment
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    • v.27 no.6
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    • pp.288-294
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    • 2014
  • The study on the migration of carbon in T23/T91 dissimilar metal welds for the boiler was conducted at $600^{\circ}C$ with an increase of aging time from 1 to 100 hrs. Following results were obtained. The heavily etched dark band tended to increase from a molten boundary owing to an increase of aging time, which leads to form hard (T91) and soft (T23) zones with different hardness. It was found that carbon was migrated from T23 area to T91 area due to different carbon activities. In addition, soft and hard zones were formed in regional area mainly resulted from carbide dissolutions and precipitates.

Microstructure and Properties of Mg-RE-Zn Alloys for High Conductivity Parts (고전도성 부품용 Mg-RE-Zn계 합금의 미세조직 및 특성)

  • Kim, Jeong-Min;Kim, Nam-Hoon
    • Journal of Korea Foundry Society
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    • v.34 no.5
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    • pp.151-155
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    • 2014
  • The relatively low conductivity of conventional Mg-Al alloys often limits their areas of application. Therefore, several attempts to develop new high-conductivity magnesium alloys have been made recently. In this research, A Ce-rich rare-earth (RE)material and zinc were added to magnesium which contained no aluminum. As the RE and Zn content were increased, both the hardness and tensile strength were gradually increased, despite the fact that the electrical conductivity decreased slightly. The effects of an aging treatment on the conductivity and mechanical properties of Mg-RE-Zn alloys were also investigated. The electrical conductivity did not change according to the heat treatment conditions; however, the mechanical properties could be enhanced by proper aging heat treatments.

Changes in Hardness and Damping Capacity of Aged Mg-5%Sn Alloy (시효한 Mg-5%Sn 합금의 경도와 진동감쇠능 변화)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.35 no.5
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    • pp.255-261
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    • 2022
  • In this work, the strain-amplitude independent and strain-amplitude dependent damping capacities of Mg-5%Sn alloy have been investigated as a function of its age-hardening response. The hardness increased with an increase in aging time, reached a peak value after 48 h, and then it gradually decreased. The damping capacities of the Mg-5%Sn alloy exhibited a decreasing tendency in the order of solution-treated, under-aged, peakaged, and over-aged states in the strain-amplitude dependent region, whereas they increased continuously with aging time in the strain-amplitude independent region. The microstructural examination during aging revealed that the lower concentration of Sn solutes in the α-(Mg) matrix and the lower density of the Mg2Sn precipitate particles may well be the crucial factors for better damping values in the strain-amplitude independent and strain-amplitude dependent regions, respectively.

The Effects of Aging Heat Treatments on the Hardness and Electrocemical Corrosion for the Nimonic 80A Superalloy (Nimonic 80A 초내열합금의 경도와 전기화학적부식에 미치는 시효열처리의 효과)

  • 나은영
    • Journal of Advanced Marine Engineering and Technology
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    • v.22 no.5
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    • pp.660-669
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    • 1998
  • In this paper the Hardness and Electro-chemical corrosion of the Nimonic 80A superalloy were studied. It aging heat treatments was carried out at $650^{\circ}C$, $700^{\circ}C$, $750^{\circ}C$,$800^{\circ}C$ and $850^{\circ}C$ with different time of 20min , 30min 1hour, 2hours, 4hours, and 16hours additionally 64hours and 128hours at $650^{\circ}C$. The obtained results were as follows; 1. As aging temperature increased the time for the maximum hardness was reduced from 128hours at $650^{\circ}C$ to 30min at $850^{\circ}C$ whereas the highest hardness was reduced from Hv 381 at $650^{\circ}C$ to Hv 321 at $850^{\circ}C$. 2. In the Electro-chemical corrosion test as a function of aging heat treatment time and tem-perature the corrosion potential was reversely proportional to Hardness which indicated the effects of ${\gamma}/{\gamma}'$ coherency of base material and precipitate. 3. Initiation point of the pitting was observed at grain boundary twin boundary and near${\gamma}'$ pre-cipitates. The results of composition analysis by EDS at this point indicated that sulphur originat-ed from 1N $H_2SO_4$ solution was found in depletion at the grain boundaries and the pit which arouse in the near precipitates were lack of Al Ti and Ni which are the main element of ${\gamma}'$ The depletion of such element was cause breakdown of passive film.

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Effect of Aging Treatment on the Microstructure and Low Temperature Tensile Properties in 5083 Aluminum Alloy Weldments (5083 Al합금 용접재의 조직 및 저온 인장성질메 미치는 시효처리의 영향)

  • Lee, T.C.;Lee, H.W.;Joo, D.W.;Lee, J.H.;Sung, J.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.1
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    • pp.1-9
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    • 2000
  • The microstructural characteristics and low temperature tensile properties between $25^{\circ}C$ and $-196^{\circ}C$ for as-welded and age hardened specimen by using Al 5083-H321 for base metal, 5083-5356 and 5083-4043 weldments have been investigated. The hardness of 5083-5356 weldment decreases with aging treatment, whereas the weld region of 5083-4043 weldment shows remarkable increase in hardness after aging due to the precipitation of fine Si particle at the grain boundaries and interiors. Low temperature tensile properties of 5083 AI base metal, 5083-5356 and 5083-4043 weldments appear to be the increment of tensile strengths and elongations at the room temperature and $-196^{\circ}C$, while the decrement of tensile properties around $-50^{\circ}C$ is shown. Through the observation of fine serration to fracture in the stress-strain curve and tensile fractography, the increment of localized deformation leading to promote the neck initiation and the increment of the dimple size cause to decrease in tensile strengths and elongations around $-50^{\circ}C$. For the tensile specimen of the 5083 base metal, 5083-5356 and 5083-4043 weldments, the reason to increase in elongation after solution and aging treatment is the diminishment of fine pit, the resolution of Mg into the matrix and the spheridization of the eutectic Si.

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