• 한국결정성장학회지
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• 제31권6호
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• pp.247-257
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• 2021

본 연구는 오토클레이브 양생시편이 예상과 달리 초기강도는 잘 발현되지 않는 반면, 수중에 장기 침지할 경우 압축강도가 향상되는 현상을 규명하기 위해 시작되었다. 증류수 및 알칼리 용액에 침지하였고, 세 가지 양생방법이 시도되었다. 알칼리용액에 침지할 경우 증류수 침지 시편이 추가적인 지오폴리머 반응에 의해 보다 더 높은 압축강도를 가질 것으로 예상하였으나, 실제로 추가적인 지오폴리머 반응에 의해 생성된 결정립들과 알칼리골재 반응에 의한 시편의 팽창 때문에 21일 침지 후 침지용액에 의한 압축강도의 변화는 크게 나타나지 않은 것으로 사료되었다. 지오폴리머의 수중 및 알칼리용액 내 장기공용성을 확보하기 위해서는 오토클레이브를 이용하여 양생 후 21일 이상 수중 침지를 시키면서 숙성(aging) 시키는 것이 바람직 한 것으로 결론지을 수 있었다.

• 열처리공학회지
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• 제36권2호
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• pp.77-85
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• 2023

In this study, the mechanical properties of the Al-Mg-X (X=Cr, Si) alloy, which clearly showed the influence of the specimen and grain size, were investigated by changing the specimen size extensively. In addition, the effect on the specimen size, grain size and aging condition on the mechanical properties of the grain refining alloy according to the addition of Cr was clarified, and the relationship between these factors was studied. As the specimen size decreased, the yield stress decreased and the fracture elongation increased. This change was evident in alloys with coarse grain sizes. Through FEM analysis, it was confirmed that the plastic deformation was localized in the parallel part of specimen S2. Therefore, when designing a tensile specimen of plate material, the W/L balance should be considered along with the radius of curvature of the shoulder. In the case of under-aged materials of alloys with coarse grain size, the fracture pattern changed from intergranular fracture to transgranular fracture as W/d decreased, and δ increased. This is due to the decrease in the binding force between grains due to the decrease in W. In the specimen with W/d > 40 or more, intergranular fracture occurred, and local elongation did not appear. Under-aged materials of alloys with fine grain size always had transgranular fracture over a wide range of W/d = 70~400. As W/d decreased, δ increased, but the change was not as large as that of alloys with coarse grain sizes. Compared to the under-aged material, the peak-aged material did not show significant dependence on the specimen size of σ_0.2 and δ.

• 전기학회논문지
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• 제63권3호
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• pp.367-370
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• 2014

The accelerated thermal aging of a CSPE were carried out for 0, 80.82, 161.63 days at $100^{\circ}C$, which are equal to 0, 40 and 80 years, respectively. The volume electrical resistivities of the non-accelerated thermally aged CSPE and the accelerated thermally aged CSPE for 40y and 80y were $9.620{\times}10^{12}{\sim}1.246{\times}10^{13}{\Omega}{\cdot}cm$, $5.066{\times}10^{12}{\sim}7.576{\times}10^{12}{\Omega}{\cdot}cm$ and $7.195{\times}10^{12}{\sim}9.208{\times}10^{12}{\Omega}{\cdot}cm$ at room temperature, respectively. The dielectric constant of the non-accelerated thermally aged CSPE and the accelerated thermally aged CSPE for 40y and 80y were 3.355~4.030, 2.996~3.963 and 3.020~4.776 at room temperature, respectively. After seawater and freshwater flooding, the volume electrical resistivity of the CSPE trend slightly upward according to drying day at room temperature. After seawater flooding, the dielectric constant of the accelerated thermally aged CSPE were not measured. After seawater flooding, bright open pores of the accelerated thermally aged CSPE were partly transferred to dark close pores due to salinity. After freshwater flooding, dark close pores of the accelerated thermally aged CSPE were partly transferred to bright open pores because salinity of them is decreased. An insulation property of a cable in NPPs was decreased because of the seawater flooding, and an insulation property of them was recovered through the freshwater flooding. As a result, it is considered that an insulation property of a contaminated cable through Tsunami can be recovered if it is cleaned quickly.

• Journal of Welding and Joining
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• 제30권5호
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• pp.64-69
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• 2012

Sn-Bi eutectic alloy has been widely used as one of the key solder materials for step soldering at low temperature. The Sn-58Bi solder paste containing chloride flux was adopted to compare with that using the chloride-free flux. The paste was applied on the electroless nickel-immersion gold (ENIG) surface finish by stencil printing, and the reflow process was then performed at $170^{\circ}C$ for 10 min. After reflow, the solder joints were aged at $125^{\circ}C$ for 100, 200, 300, 500 and 1000 h in an oven. The interfacial microstructures were obtained by using scanning electron microscopy (SEM), and the composition of intermetallic compounds (IMCs) was analyzed using energy dispersive spectrometer (EDS). Two different IMC layers, consisting of $Ni_3Sn_4$ and relatively very thin Sn-Bi-Ni-Au were formed at the solder/surface finish interface, and their thickness increased with increasing aging time. The wettability of solder joints was investigated by wetting balance test. The mechanical property of each aging solder joint was evaluated by the ball shear test in accordance with JEDEC standard (JESD22-B117A). The results show that the highest shear force was measured when the aging time was 100 h, and the fracture mode changed from ductile fracture to brittle fracture with increasing aging time. On the other hand, the chloride flux in the solder paste did not affect the shear force and fracture mode of the solder joints.

• Elastomers and Composites
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• 제42권1호
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• pp.20-31
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• 2007

고무의 안정성과 신뢰성 확보를 위해 재료 특성과 수명 평가는 매우 중요하다. 본 연구에서는 연료전지용 고무 가스켓으로 사용되는 황으로 가황한 NBR compound의 수명을 예측하였다. 5, 6, 7 vol% 황산농도에서 120, 140, $160^{\circ}C$ 온도로 각각 3시간에서 600시간까지 가속 노화시험을 하였다. 고무를 황산용액 안에 침지시키기 위해 pyrex glass tube를 사용하였다. 그리고 가열 시간 동안 용액의 증발을 막기 위하여 pyrex glass tube 양쪽 끝을 막았다. 연료전지용 가스켓인 NBR 고무의 수명을 예측하기 위하여 가속 산-열 노화시험 후 물성 실험을 하였으며 산-열 노화시험에서 물리적 특성의 영향을 연구하기 위하여 인장강도, 신장율, 경도, 가교밀도를 측정하였다. 인장강도는 황산농도와 온도가 증가함에 따라서 감소되었는데 이 결과로 Arrhenius 식을 유도하여 수명을 평가하였다.

• 마이크로전자및패키징학회지
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• 제18권4호
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• pp.1-9
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• 2011

Understanding the void characterization in the solder joints has become more important because of the application of lead free solder materials and its reliability in electronic packaging technology. According to the JEDEC 217 standard, it describes void types formed in the solder joints, and divides into some categories depending on the void position and formation cause. Based on the previous papers and the standards related to the void, reliability of the BGA solder joints is determined by the size of void, as well as the location of void inside the BGA solder ball. Prior to reflow soldering process, OSP(organic surface preservative) finished Cu electrode was exposed under $85^{\circ}C$/60%RH(relative humidity) for 168 h. Voids induced by the exposure of $85^{\circ}C$/60%RH became larger and bigger with increasing aging times. The void position has more influence on mechanical strength property than the amount of void growth does.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집A
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• pp.250-255
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• 2001

It is inevitable to evaluate the life of turbine rotor because the operating periods of power plants need to be extended. The magnetic methods utilizing Magnetic Barkhausen noise curve were applied to detect the degradation caused by thermal aging. The Magnetic property of material depends on the domain dynamics and it is affected by the microstructure of material. Therefore the magnetic property is very sensitive to the microstructure change of the material. It is, thus, very useful to detect the state of degradation of varying materials. The test specimen made of 1Cr-1Mo-0.25V steel was used widely for turbine rotor material, and seven kinds of specimens with different degradation levels were prepared by the isothermal heat treatment at $630^{\circ}C$. With the increase of degradation, BHN was decreased. The result was compared with coercive force and vickers hardness.

• 한국포장학회지
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• 제13권3_4호
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• pp.89-95
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• 2007

식물성 천연항균제인 BAAG와 기능성 무기계 첨가제인 zeolite를 이용하여 항균 및 ethylene 가스 포집 능력을 갖는 포장원지를 제조하였다. 기능성 포장원지의 인장강도와 파열강도는 항균제와 zeolite를 첨가하지 않았을 때보다 다소 감소하는 경향을 나타내었고, 반면에 강성과 인열강도는 항균제와 zeolite를 첨가하지 않았을 때보다 증가하는 경향을 나타내었다. 과채류 숙성 호르몬인 ethyene 가스는 포장원지에 zeolite를 첨가하면서 빠르게 감소하였다. 포자원지의 발수성은 중성 사이즈제인 AKD를 첨가하면서 높은 내수성을 나타내었다.

• 열처리공학회지
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• 제22권6호
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• pp.368-374
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• 2009

Nickel titanium shape memory alloys (NiTi) have been investigated for applications in the biomedical industry. However, little is known about the influences of surface modifications on the propertise of these alloys. The effect of electropolishing and heat treatments was found to exhibit significant surface roughness. Change of phase was B2, r-phase and B19' by heat treatments. In this study, effect of the electropolishing conditions on surface roughness is investigated in Ni-Ti alloys (Nitinol). Variation in phases with heat treatment temperature is investigated for a Ni-Ti alloy by X-ray diffraction and DSC. Characteristic of the microstructure have been observed by SEM. Surface roughness have been measured by AFM. The results clearly show that significant different in surface property to heat treated at $500^{\circ}C$ (R-phase). $TiO_2$ phases preciritated all of the specimens. It is not good effect of surface roughness because made to surface relief. The surface roughness appears to be important in the property of Ni-Ti alloys for biomedical applications.

• 한국임상수의학회지
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• 제24권2호
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• pp.201-207
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• 2007

The teat cup liner compounds with improved physical property were developed using tri-polymer blend of natural rubber(NR), ethylene propylene diene monomer rubber(EPDM) and butyl rubber, and the changes of the physical properties of compounds were measured under various conditions such as standard, thermal, alkaline detergent and acid solutions aging conditions. The hardness of the new teat cup liner compound 1 was 50 and that of the compound 2 was 51 under standard condition. The tensile strength and elongation of the new compound 1 were $154kgf/cm^2$ and 675% under the standard condition, respectively. Also, those of the new compound 2 were 180 kgf/cm and 634% under the same condition. Their hardness were increased about $2{\sim}6%$ and the tensile strength and elongation were decreased about 10% under the $25^{\circ}C$ water and detergent solutions. Even though the new teat cup liner compounds exhibited so much decreased tensile properties under the $105^{\circ}C$ thermal aged condition, they sustained more stable aged physical properties including tensile strength and elongation than those of imported teat cup liner materials. Consequently, the new teat cup liner compounds would give prolonged lift cycle if they are used as a teat cup liner product.