• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.21 no.6
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• pp.976-981
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• 2012

In this study, hardness, microstructure and temperature of glass transition are measured respectively by using SEM (Scanning electron microscope) and DSC (Differential scanning calorimeter) to analyze the effects on material properties by after-curing in the epoxy resin. As the result of hardness test according to the after-curing conditions, the higher the temperature of after-curing, hardness and heat resistance are, the higher hardness is. As a result of microstructure for each specimen by SEM, it could be confirmed that the specimen with after-curing has more dense fracture surface. It is also found that temperatures of glass transitions by DSC are comparatively higher in the specimens with after-curing, and the differences between after-curing conditions are negligible.

• Restorative Dentistry and Endodontics
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• v.18 no.1
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• pp.1-26
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• 1993

The purpose of this study was to investigate the effect of acid etching on the surface appearance and fracture toughness of five glass ionomer cements. Five kinds of commercially available glass ionomer cements including chemical curing filling type, chemical curing lining type, chemical curing metal reinforced type, light curing tilling type and light curing lining type were used for this study. The specimens for SEM study were fabricated by treating each glass ionomer cement with either visible light curing or self curing after being inserted into a rubber mold (diameter 4mm, depth 1mm). Some of the specimens were etched with 37% phosphoric acid for 0, 15, 30, 60, go seconds, at 5 minutes, 1 hour and 1 day after mixing of powder and liquid. Unetched ones comprised the control group and the others were the experimental groups. The surface texture was examined by using scanning electron microscope at 20 kV. (S-2300, Hitachi Co., Japan). The specimens for fracture toughness were fabricated by curing of each glass ionomer cement previously inserted into a metal mold for the single edge notch specimen according to the ASTME399. They were subjected to a three-point bend test after etching for 0, 30, 60, and 90 seconds at 5 minutes-, 1 hour-and 1 day-lapse after the fabrication of the specimens. The plane strain fracture toughness ($K_{IC}$) was determined by three-point bend test which was conducted with cross-head speed of 0.5 mm/min using Instron universal testing machine (Model No. 1122) following seven days storage of the etched specimens under $37^{\circ}C$, 100% humidity condition. Following conclusions were drawn. 1. In unetched control group, crack was present, but the surface was generally smooth. 2. Deterioration of the surface appearance such as serious dissolving of gel matrix and loss of glass particles occured as the etching time was increased beyond 15 s following Immediate etching of chemical curing type of glass ionomer cements. 3. Etching after 1 h, and 1 d reduced surface damage, 15 s, and 30s etch gave rough surface appearance without loss of glass particle of chemical curing type of glass ionomer cements. 4. Light curing type glass ionomer cement was etched by acid, but there was no difference in surface appearances according to various waiting periods. 5. It was found that the value of plane stram fracture toughness of glass ionomer cements was highest in the light curing filling type as $1.79\;MNm^{-1.5}$ followed by the light curing lining type, chemical curing metal reinforced type, chemical curing filling type and chemical curing lining type. 6. The value of plane stram fracture toughness of the chemical curing lining type glass ionomer cement etched after 5 minutes was lower than those of the cement etched after 1 hour or day or unetched (P < 0.05). 7. Light curing glass ionomer cement showed Irregular fractured surface and chemical curing cement showed smooth fractured surface.

• Journal of the Korean Society of Tobacco Science
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• v.22 no.2
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• pp.114-122
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• 2000

This study was carried out to investigate the changes in the composition of essential oils for the improvement of air-curing process of burley tobacco leaves. From the essential oils isolated from the cured tobacco leaves by steam distillation method, 90 compounds including 15 acids and esters, 19 alcohols, 23 aldehydes and ketones, 19 hydrocarbons, and 14 miscellaneous compounds, could be identified by gas chromatography and gas chromatography-mass spectrometry. Among them, acids and esters were gradually decreased during the progress of curing after harvesting. A rapid increase in alcohol content was observed in the earlier stage of curing, but thereafter, decrease followed until the end of curing However, aldehyde and ketone groups were continuously increased during curing and were 3 times higher in quantity after curing than at the harvesting time. The concentration of hydrocarbons was increased in the earlier stage of curing, but gradually decreased from the middle stage. The miscellaneous compounds were continuously increased in content until the end stage of curing, with rapid increased in the earlier stage of curing.

• International Journal of Highway Engineering
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• v.19 no.2
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• pp.67-74
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• 2017

PURPOSES : The objective of this study is to ascertain the curing period of cementless cold central plant recycled asphalt base-layer, using mechanical analyses and specimen quality tests on the field. METHODS : Cold central plant recycled asphalt base-layer mixture was produced in the plant from reclaimed asphalt, natural aggregate, filler for the cold mix, and the modified emulsion AP using asphalt mix design and plant mix design. In order to examine the applicability of the curing period during the field test, the international standards for the possibility of core extraction and the degree of compaction and LFWD deflection were analyzed. Moreover, Marshall stability test, porosity test, and indirect tensile strength test were performed on the specimens of asphalt mix and plant mix design. RESULTS : The plant production process and compaction method of cementless cold central plant recycled asphalt base-layer were established, and the applicability of the optical moisture content for producing the mixture was verified through the field test. In addition, it was determined that the core extraction method of the conventional international curing standard was insufficient to ensure performance, and the LFWD test demonstrated that the deflection converges after a two-day curing. However, the back-calculation analysis reveals that a three-day curing is satisfactory, resulting in a general level of performance of dense asphalt base-layer. Moreover, from the result of the specimen quality test of the asphalt mix design and plant mix design according to the curing period, it was determined that the qualities satisfied both domestic and international standards, after a two-day curing. However, it was determined that the strength and stiffness after three-day curing are higher than those after a two-day curing by approximately 3.5 % and 20 %, respectively. CONCLUSIONS:A three-day curing period is proposed for the cementless cold central plant recycled asphalt base-layer; this curing period can be demonstrated to retain the modulus of asphalt-base layer in the field and ensure stable quality characteristics.

• Proceedings of the Korea Concrete Institute Conference
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• 1997.04a
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• pp.170-176
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• 1997

The published works on steam curing effect have been generally concentrated on the subject, "compressive strength". However a practical test for durable steam curing concrete products has not been performed in domestic. In this study, the maximum temperature of steam is considered as a major variable to investigate the freezing and thawing resistance of the steam curing concrete. All of the specimen were cured for 24 hours which included presteaming 4 hour. Finally we found that the most effective curing condition is the case of one-day and 14-day specimens after the 24 hours steam curing at $74^{\cire}C$ degree curing temperature. It is also found that the durability of one-day samples are much weaker than those of 14-day samples. Consequently, we can conclude that the samples that produced immediately after a steam curing are more possible to deteriorate from the freezing and thawing environment.vironment.

• Restorative Dentistry and Endodontics
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• v.41 no.4
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• pp.239-245
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• 2016

The purpose of this article was to review the changes in translucency of direct esthetic restorative materials after curing, aging and treatment. As a criterion for the evaluation of clinical translucency changes, visual perceptibility threshold in translucency parameter difference (${\Delta}TP$) of 2 was used. Translucency changes after curing were perceivable depending on experimental methods and products (largest ${\Delta}TP$ in resin composites = 15.9). Translucency changes after aging were reported as either relatively stable or showed perceivable changes by aging protocols (largest ${\Delta}TP$ in resin composites = -3.8). Translucency changes after curing, aging and treatment were perceivable in several products and experimental methods. Therefore, shade matching of direct esthetic materials should be performed considering these instabilities of translucency in direct esthetic materials.

• Current Research on Agriculture and Life Sciences
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• v.32 no.3
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• pp.125-130
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• 2014

This study used transmission electron microscopy (TEM) to investigate the micro-morphological features of two formaldehyde to urea (F/U) mole ratio liquid urea-formaldehyde (UF) resins with three hardener levels as a function of the curing time. The micro-morphological features of the liquid UF resins were characterized after different curing times. As a result, the TEM examination revealed the presence of globular/nodular structures in both liquid UF resins, while spherical particles were only visible in the low F/U mole ratio resins. The high F/U mole ratio liquid UF resins also showed extensive particle coalescence after adding the hardener, along with the appearance of complex filamentous networks. When the resins were cured with a higher amount of hardener and longer curing time, the spherical particles disappeared. For the low mole UF resins, the particles tended to coalesce with a higher amount of hardener and longer curing time, although discrete spherical particles were still observed in some regions. This is the first report on the distinct features of the crystal structures in low F/U mole ratio UF resins cured with 5% hardener and after 0.5 h of curing time. In conclusion, the present results indicate that the crystal structures of low F/U mole ratio UF resins are formed during the curing process.

• Proceedings of the Korean Geotechical Society Conference
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• 2002.03a
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• pp.305-312
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• 2002

To estimate the effects of lime and cement on the surplus soil, the engineering properties of the marine deposited clay and the fresh water clay were analyzed. The specimen were prepared under several curing conditions, namely, underwater curing, wet condition curing and underwater curing after heating. Unconfined compression strength were estimated after 7, 14, 28 and 60 days, respectively. The strength were steeply increased with time until first 14 days. Specially the increase of the strength of the heated soil were large.

• Computers and Concrete
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• v.24 no.3
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• pp.249-258
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• 2019

In order to investigate the strength recovery of fire-damaged concrete after post-fire curing, concrete specimens were heating at $2^{\circ}C/min$ or $5^{\circ}C/min$ to 400, 600 and $800^{\circ}C$, and these exposed specimens were soaked in the water for 24 hours and following by 29-day post-fire curing. The compressive strength and split tensile strength of the high-temperature-exposed specimens before and after post-fire curing were tested. The proportion of split aggregate in the split surfaces was analyzed to evaluate the mortar-aggregate interfacial strength. After the post-fire curing process, the split tensile strength of specimens exposed to all temperatures was recovered significantly, while the recovery of compressive strength was only obvious within the specimens exposed to $600^{\circ}C$. The tensile strength is more sensitive to the mortar-aggregate interfacial cracks, which caused that the split tensile strength decreased more after high-temperature exposure and recovery more after post-fire curing than the compressive strength. The mortar-aggregate interfacial strength also showed remarkable recovery after post-fire curing, and it contributed to the recovery of split tensile strength.

• Magazine of the Korean Society of Agricultural Engineers
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• v.33 no.2
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• pp.61-72
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• 1991

This study was carried out to research the strength drop of concrete in dry environment. The mixing ratio of cement-fine aggregate was 1: 1, 1 : 2, 1: 3 and 1 : 4. The curing was compared standard curing with dry curing immediately after casting. It is analysis of strength change by water-proof mixing. The curing age of cement mortar was 3days, 7days, l4days and 28days. The result obtained from this study are summarized as follows. 1. The compressive and bending strength change by increasing the curing age, dry curing mortar the increasing rate of strength was decreased than standard curing mortar. 2. The compressive and bending strength change in early curing, strength difference between standard curing mortar and dry curing motar was gradually closed by increasing the W/C. 3. The dry curing mortar was decreased than standard curing mortar in decreasing rate of compressive and bending strength by increasing the W/C. 4. The compressive strength of water-proof mortar in early curing, liquid water-proof mortar was shown high strength in dry curing than standard curing. The powder and liquid water-proof mortar have a small effect in dry environment. The liquid water-proof mortar was high strength without relation change of curing age in dry environment than standard curing. 5. The compressive strength of liquid water-proof mortar in poverty mix, dry curing was shown high strength than standard curing. 6. The bending strength was increased than compressive strength by decreasing the volume of cement in early curing. The increasing rate of bending strength was decreased to compressive stength by increasing the curing age.