• Title/Summary/Keyword: Additional curing

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Development of Self-Repairing Smart Concrete Using Micro-Biologically Induced Calcite Precipitation (미생물의 방해석 석출 작용을 이용한 자기보수 스마트 콘크리트 개발에 관한 연구)

  • Kim, Wha-Jung;Ghim, Sa-Youl;Park, Sung-Jin;Choi, Kil-Jun;Chun, Woo-Young
    • Journal of the Korea Concrete Institute
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    • v.22 no.4
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    • pp.547-557
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    • 2010
  • This paper presents a study on the development of next generation smart concrete in an eco-friendly manner using micro-biologically induced calcite precipitation (MICP) via microbial biomineralization. It seems that currently, the reformation and functional improvement of concrete using MICP can be achieved using Sporosarcina pasteurii, which is a representative microorganism that produces calcite precipitation. Based on previous studies on MICP the biochemical tests and crystallinity evaluation of cement using sporoasrcina pasteurii and four additional micro-organisms from the concrete structures as identified by 16S rDNA sequence analysis were conducted. Also by applying the Sporosarcina pasteurii and separated four effective micro-organisms from the concrete structures to mortar, the compressive strength improvement by varying curing conditions, repair of crack were examined, and plans for future study were suggested. The effect of the application of effective micro-organisms can lead to the development of a new material that will contribute to resolution of environmental problems and facilitate repair work, and this can also serve as a new research theme in the future. In addition, the importance of this study is to use micro-organism, which is found common in concrete structures, this new microbial is not only environmentally safe but also persists in the natural environment for an extended period of time. Therefore, it seems to have a great potential to became a new environmentally low-burdened functional material.

A Study on the Manufacturing Processability of Automatic Winding Device for Manufacturing Strand Specimens (스트랜드 시편 제작 장치의 제작 공정성 연구)

  • Cha, Jae Ho;Jang, Jeong Keun;Lee, Bo Mi;Yoon, Sung Ho
    • Composites Research
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    • v.33 no.5
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    • pp.315-320
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    • 2020
  • In this study, when strand specimens were manufactured using an automatic winding device to obtain uniform strand specimens, analysis and test were conducted to investigate the effect of thermal expansion of the mandrel on strand specimens. Also, necessity of changing materials and mandrel configuration was checked. According to the results, strand specimen received unintended tension that was created by thermal expansion of the mandrel and this unintended tension depended on the curing temperature and position of specimens. Tensile test was conducted to check that initial tension affected on the performance of carbon fiber tow prepreg. All other conditions were fixed and only the initial tension was controlled at 40 N, 60 N, and 80 N. From the results of analysis and test, neither additional tension and tension deviation due to the thermal expansion of the mandrel and the initial tension difference had a significant effect on tensile test results, because carbon fiber had sufficiently high strength compared with tension. Therefore, it was confirmed that the change of the mandrel material and configuration of the automatic winding device was unnecessary.

Static and Fatigue Characteristics of Urethane Foam Cored Sandwich Structures (우레탄 폼 코아 샌드위치 구조물의 정적 및 피로 특성)

  • 김재훈;이영신;박병준;김덕회;김영기
    • Composites Research
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    • v.12 no.6
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    • pp.74-82
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    • 1999
  • The static and fatigue characteristics of polyurethane foam cored sandwich structures are investigated. Three types of the specimens with the glass fabric faces and the polyurethane foam core are used; non-stitched. stitched, and stiffened sandwich specimen. Especially additional structural reinforcements with the twisted polyester and glass fiber for thickness direction are made to stitched sandwich structure panel to minimize the delamination of structure which is stitched the upper and lower faces through the core and the resin is impregnated Into stitched fiber with the characteristics of low viscosity of resin at resin flow temperature and cured together with during the curing process. Bending strength of stitched specimen which is 50 mm $50{\times}50{\;}mm$ pitched is improved by 50 % as com-pared with non-stitched specimen and stiffened specimen is improved 10 times more than non-stitched structure. After fatigue testing of $10^6$cycles by 20% of ultimate load under monotonic load, the bending fatigue strength of non-stitched specimen is decreased by 27% of monotonic bending strength, 39% for stitched structure and 20% for stiffened specimen. To verify the aging effect of polyurethane form core, Ultrasonic C-scanning equipment is used to detect the damage of skin laminate alone after fatigue test. From results of UT C-scan images, there is no defect that can be damaged occurred during fatigue test. It is concluded that the decrease of bending strength for foam cored sandwich specimen is caused by the decrease of stiffness due to the aging of polyurethane foam core during fatigue cycles.

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Effects of Organic Acids Mix and Modified Atmosphere Packaging on the Storage Quality of Sliced Bacon

  • Muhlisin, Muhlisin;Kang, Sun-Moon;Choi, Won-Hee;Lee, Keun-Taik;Cheong, Sung-Hee;Lee, Sung-Ki
    • Food Science of Animal Resources
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    • v.31 no.5
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    • pp.710-718
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    • 2011
  • The effects of organic acids mix (0.4%) and modified atmosphere packaging (MAP) on the storage quality of sliced bacon were investigated. Pork bellies were treated with or without organic acids at the curing stage. The organic acids mix comprised 35% sodium acetate, 25% salt, 15% calcium lactate, 11% trisodium citrate, 7% ascorbate, and 7% citric acid. The cured pork bellies were smoked and packaged with 50% $CO_2$ + 50% $N_2$ (50% $CO_2$-MAP) and 100% $N_2$ (100% $N_2$-MAP), and stored at $5^{\circ}C$ for 14 d. The 50% $CO_2$-MAP showed a higher pH value (p<0.05) up to 10 d, a lower protein deterioration (p<0.05) as measured by volatile basic nitrogen (VBN) from 6 to 14 d, and a higher color value of lightness (CIE $L^*$) compared to 100% $N_2$-MAP. The development of lipid oxidation measured by thiobarbituric acid reactive substance (TBARS) values seemed to be effectively controlled throughout the storage period in both 50% $CO_2$-MAP and 100% $N_2$-MAP regardless of the application of organic acids. The 50% $CO_2$-MAP inhibited the growth of aerobic and anaerobic bacteria (p<0.05) both in non-added and bacon added with organic acids mix. The 50% $CO_2$-MAP alone seemed to be effective in delaying the growth of bacteria since the use of organic acids mix gave no additional effects. The addition of organic acids mix lowered the pH value (p<0.05), effectively retarded the protein deterioration (p<0.05), and showed a higher color value of lightness (CIE $L^*$) value (p<0.05) and lower color value of redness (CIE $a^*$) value (p<0.05). In conclusion, 50% $CO^2$-MAP showed better quality and self-life of sliced bacon during storage. However, the beneficial effect of organic acids mix was not noticed in the concentration used in this experiment.

Copper Interconnection and Flip Chip Packaging Laboratory Activity for Microelectronics Manufacturing Engineers

  • Moon, Dae-Ho;Ha, Tae-Min;Kim, Boom-Soo;Han, Seung-Soo;Hong, Sang-Jeen
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.431-432
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    • 2012
  • In the era of 20 nm scaled semiconductor volume manufacturing, Microelectronics Manufacturing Engineering Education is presented in this paper. The purpose of microelectronic engineering education is to educate engineers to work in the semiconductor industry; it is therefore should be considered even before than technology development. Three Microelectronics Manufacturing Engineering related courses are introduced, and how undergraduate students acquired hands-on experience on Microelectronics fabrication and manufacturing. Conventionally employed wire bonding was recognized as not only an additional parasitic source in high-frequency mobile applications due to the increased inductance caused from the wiring loop, but also a huddle for minimizing IC packaging footprint. To alleviate the concerns, chip bumping technologies such as flip chip bumping and pillar bumping have been suggested as promising chip assembly methods to provide high-density interconnects and lower signal propagation delay [1,2]. Aluminum as metal interconnecting material over the decades in integrated circuits (ICs) manufacturing has been rapidly replaced with copper in majority IC products. A single copper metal layer with various test patterns of lines and vias and $400{\mu}m$ by $400{\mu}m$ interconnected pads are formed. Mask M1 allows metal interconnection patterns on 4" wafers with AZ1512 positive tone photoresist, and Cu/TiN/Ti layers are wet etched in two steps. We employed WPR, a thick patternable negative photoresist, manufactured by JSR Corp., which is specifically developed as dielectric material for multi- chip packaging (MCP) and package-on-package (PoP). Spin-coating at 1,000 rpm, i-line UV exposure, and 1 hour curing at $110^{\circ}C$ allows about $25{\mu}m$ thick passivation layer before performing wafer level soldering. Conventional Si3N4 passivation between Cu and WPR layer using plasma CVD can be an optional. To practice the board level flip chip assembly, individual students draw their own fan-outs of 40 rectangle pads using Eagle CAD, a free PCB artwork EDA. Individuals then transfer the test circuitry on a blank CCFL board followed by Cu etching and solder mask processes. Negative dry film resist (DFR), Accimage$^{(R)}$, manufactured by Kolon Industries, Inc., was used for solder resist for ball grid array (BGA). We demonstrated how Microelectronics Manufacturing Engineering education has been performed by presenting brief intermediate by-product from undergraduate and graduate students. Microelectronics Manufacturing Engineering, once again, is to educating engineers to actively work in the area of semiconductor manufacturing. Through one semester senior level hands-on laboratory course, participating students will have clearer understanding on microelectronics manufacturing and realized the importance of manufacturing yield in practice.

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Evaluation of Flexural Behavior of Hollow Prestressed Concrete Pile for Continuous Pile Wall (주열식 벽체용 중공 프리스트레스트 콘크리트 파일의 휨거동 평가)

  • Lee, Young-Geun;Jang, Min-Jun;Yoon, Soon-Jong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.18 no.3
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    • pp.20-27
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    • 2014
  • In the construction site, various earth retaining systems are developed and applied to maintain stability of excavated area and structures. Among the methods, the underground continuous wall and the column-type diaphragm wall methods are especially used in construction site nearby buildings or roads. However, these methods have some disadvantages such as the difficulty of quality control and long curing time because these methods need to cast fresh concrete at the construction site. In addition, these methods are usually applied to the site for the temporary purpose. In this paper, we suggest precast hollow prestressed concrete pile for continuous pile wall system. To investigate the structural behavior of suggested pile, which is the main member of the suggested system, tests pertaining to the structural behavior and prestressing force applied in the pile are conducted. From the test results, it was found that the prestressing force measured is sufficient compared with the value obtained by the design equation and the cracking moment measured is 34% higher than the design value. In addition to the above, this precast hollow prestressed concrete pile has an additional safety margin that the maximum moment is 59.2% higher than the cracking moment which is one of the serviceability limits for the design of the system.

An Analysis of the Mechanism of Crack Stop-bar for Floor Plastering of Apartment Buildings (공동주택 바닥미장 균열차단막의 메커니즘 분석)

  • Song, Yong-Sik;Lee, Dong-Hoon;Lee, Sung-Ho;Kim, Sun-Kuk
    • Journal of the Korea Institute of Building Construction
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    • v.11 no.4
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    • pp.333-344
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    • 2011
  • The recent expansion in the number of housing construction projects has been accompanied by substantial improvements in construction quality, which can be attributed to the development of new construction technologies and materials. In apartment complex construction projects, numerous mechanization technologies have been adopted as part of the floor plastering process to counter increasing difficulties in securing labor and the pressing need to reduce lead time, but these have also triggered setbacks such as additional costs or loss of time to fix cracks in or loosening of floor. Cracks developing in the floor of an apartment housing unit, in terms of materials in use, are the products of a complex combination of material makeup, construction workmanship, concrete curing and the protection method. Controlling such elements from the perspective of materials in use may ensure partial success in reducing cracks, but fall short of eliminating them completely. Any attempt to prevent cracks from developing in the first place requires systematic analysis as to their potential causes and viable solutions to reduce them. On this backdrop, this paper aims to provide an analysis of potential causes of cracks found in floor plastering, and consider the mechanism of a crack stop-bar as a fundamental safeguard against them.

Surface-modified Nanoparticle Additives for Wear Resistant Water-based Coatings for Galvanized Steel Plates

  • Becker-Willinger, Carsten;Heppe, Gisela;Opsoelder, Michael;Veith, H.C. Michael;Cho, Jae-Dong;Lee, Jae-Ryung
    • Corrosion Science and Technology
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    • v.9 no.4
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    • pp.147-152
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    • 2010
  • Conventional paints for conversion coating applications in steel production derived mainly from water-based polymer dispersions containing several additives actually show good general performance, but suffer from poor scratch and abrasion resistance during use. The reason for this is because the relatively soft organic binder matrix dominates the mechanical surface properties. In order to maintain the high quality and decorative function of coated steel sheets, the mechanical performance of the surface needs to be improved significantly. In fact the wear resistance should be enhanced without affecting the optical appearance of the coatings by using appropriate nanoparticulate additives. In this direction, nanocomposite coating compositions (Nanomer$^{(R)}$) have been derived from water-based polymer dispersions with an increasing amount of surface-modified nanoparticles in aqueous dispersion in order to monitor the effect of degree of filling with rigid nanoparticles. The surface of nanoparticles has been modified for optimum compatibility with the polymer matrix in order to achieve homogeneous nanoparticle dispersion over the matrix. This approach has been extended in such a way that a more expanded hybrid network has been condensed on the nanoparticle surface by a hydrolytic condensation reaction in addition to the quasi-monolayer type small molecular surface modification. It was expected that this additional modification will lead to more intensive cross-linking in coating systems resulting in further improved scratch-resistance compared to simple addition of nanoparticles with quasi-monolayer surface modification. The resulting compositions have been coated on zinc-galvanized steel and cured. The wear resistance and the corrosion protection of the modified coating systems have been tested in dependence on the compositional change, the type of surface modification as well as the mixing conditions with different shear forces. It has been found out that for loading levels up to 50 wt.-% nanoparticles, the mechanical wear resistance remains almost unaffected compared to the unmodified resin. In addition, the corrosion resistance remained unaffected even after $180^{\circ}$ bending test showing that the flexibility of coating was not decreased by nanoparticle addition. Electron microscopy showed that the inorganic nanoparticles do not penetrate into the organic resin droplets during the mixing process but rather formed agglomerates outside the polymer droplet phase resulting in quite moderate cross linking while curing, because of viscosity. The proposed mechanisms of composite formation and cross linking could explain the poor effect regarding improvement of mechanical wear resistance and help to set up new synthesis strategies for improved nanocomposite morphologies, which should provide increased wear resistance.

The Effect of Reinforcing Materials on the Transverse Strength of Denture Base Resin (의치상 레진 강화재가 의치상 굽힘강도에 미치는 영향)

  • Lee, Jun-Sik;Song, Young-Gyun;Cho, In-Ho
    • Journal of Dental Rehabilitation and Applied Science
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    • v.28 no.4
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    • pp.327-337
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    • 2012
  • The object of this study was to find out the effect of various reinforcing materials including Quarts Splint$^{TM}$ Mesh on the transverse strength of the denture resin. QC-20 and Lucitone199$^{(R)}$ were used as the denture resin, and polyethylene fiber Ribbond$^{(R)}$, light curing quarts fiber Quarts Splint$^{TM}$ Mesh, metal mesh were used as the reinforcing materials. Ten specimens were fabricated for each group and the size of specimens was $2.0{\times}10.0{\times}65.0mm$. To compare the effect of resin thickness, additional specimens of $2.5{\times}10.0{\times}65.0mm$, $3.0{\times}10.0{\times}65.0mm$ were fabricated. In the control group, the transverse strength of Lucitone199$^{(R)}$ was significantly higher than that of QC-20(p<0.05). Among the specimens of 2.0 mm thickness fabricated with $Lucitone199^{(R)}$ and QC-20, they showed high transverse strength in the order of metal mesh, Quarts Splint$^{TM}$ Mesh, Ribbond$^{(R)}$, and control group. In the specimens of 2.0 mm, 2.5 mm thickness, the transverse strength of Quarts Splint$^{TM}$ Mesh were significantly higher than that of QC-20(p<0.05). But in the specimens of 3.0 mm thickness, there was no significant difference.

EFFECT OF CAVITY DIVERGENCY ON CEMENT THICKNESS AND BOND STRENGTH OF RESIN INLAY (와벽 이개도가 레진 인레이의 시멘트 두께 및 접착 강도에 미치는 영향)

  • Cha, Yoon-Seog;Cho, Yong-Bum;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.21 no.2
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    • pp.619-627
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    • 1996
  • There are increasing use of composite resin in the posterior teeth and the new indirect inlay technique was introduced for compensating much troubles faced in direct technique. Many researchers insisted that overall properties of restorative materials were enhanced by an additional curing but this technique still has a problems about using cement material. Resin inlay obtains retention force from friction and another adhesion to tooth structure. A shape of cavity preparation was noted but studies about cement thickness and bond strength with cavity divergency are rare. The purpose of this study is to assess the effect of cavity divergency on cement thickness and bond strength of resin inlay. Cavities, which divergency was $6^{\circ}$, $16^{\circ}$, and $26^{\circ}$ in each group, were prepared and their divergency was verified by Adobe Photoshop program through the image capture with stereo microscope and FlexCam. Inlays were fixed into the cavities with a resin cement, Superbond and were handled under chemical (in 75% ethanol for 24 hrs.) and thermal stress (500 cycles from $5^{\circ}$ to $55^{\circ}C$). MXT 70 (x400) was used for measuring the cement thickness and bond strength was evaluated with a universal testing machine. Following results were obtained : 1. The cement thickness in Mean (S.D.) were; 35.58 (10.31)${\mu}m$ in $6^{\circ}$ group, 35.97 (10.49)${\mu}m$ in $16^{\circ}$ group, and 41.43 (9.33)${\mu}m$ in $26^{\circ}$ group. But there was no significant difference between groups. 2. The bond strength in Mean (S.D.) were ; 33.18 (5.53)kg in $6^{\circ}$ group, 23.47 (13.40)kg in $16^{\circ}$ group, and 19.75 (10.48)kg in $26^{\circ}$ group. $6^{\circ}$ group showed significantly higher value compared to $16^{\circ}$ and $26^{\circ}$ groups (p<0.05). Although the results of this study indicate $6^{\circ}$ divergency will be good for resin inlay, cavity preparation with this type will have lots of difficulties in manufacturing, try-in, and cementation procedures, such as deformation. So it is concluded that $16^{\circ}$ divergent cavity preparation is recommended in resin inlay technique.

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