• Title/Summary/Keyword: Acoustic microscopy

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Preparation and Characterization of Small Sized PZT Powders: A Sol-Gel Modified Approach

  • Choi, Kyu-Man;Lee, Hae-Chun
    • The Journal of Korea Institute of Information, Electronics, and Communication Technology
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    • v.1 no.2
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    • pp.27-32
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    • 2008
  • A current research basically diverted towards an increase in the operational output with the minimization of the materials used, which ultimately scaled down the dimensions of ceramic electronic components. In this direction the nano-technology pave the revolutionary changes in particular the electronic industries. The applications of nano-sized particles or nano-sized materials are hence, playing a significant role for various purposes. The PZT(lead, zirconium, titanium) based ceramics which, are reported to be ferroelectric materials have their important applications in the areas of surface acoustic waves (SAW), filters, infrared detectors, actuators, ferroelectric random access memory, speakers, electronic switches etc. Moreover, these PZT materials possess the large electro mechanical coupling factor, large spontaneous polarization, low dielectric loss and low internal stress etc. Hence, keeping in view the unique properties of PZT piezoelectric ceramics we also tried to synthesize indigenously the small sized PZT ceramic powder in the laboratory by using the modified sol-gel approach. In this paper, propyl alcohol based sol-gel method was used for preparation of PZT piezoelectric ceramic. The powder obtained by this sol-gel process was calcined and sintering to reach a pyrochlore-free crystal phase. The characterization of synthesized material was carried out by the XRD analysis and the surface morphology was determined by high resolution scanning electron microscopy.

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Precise Estimation of Nonlinear Parameter in Pulse-Like Ultrasonic Signal (펄스형 초음파 신호에서 비선형 파라미터의 정밀 추정)

  • Ha, Job;Jhang, Kyung-Young;Sasaki, Kimio;Tanaka, Hiroaki
    • Journal of the Korean Society for Nondestructive Testing
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    • v.26 no.2
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    • pp.77-83
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    • 2006
  • Ultrasonic nonlinearity has been considered as a solution for the detection of microcracks or interfacial delamination in a layered structure. The distinguished phenomenon in nonlinear ultrasonics is the generation of higher-order harmonic waves during the propagation. Therefore, in order to quantify the nonlinearity, the conventional method measures a parameter defined as the amplitude ratio of a second-order harmonic component and a fundamental frequency component included in the propagated ultrasonic wave signal. However, its application In field inspection is not easy at the present stage because no standard methodology has yet been made to accurately estimate this parameter. Thus, the aim of this paper is to propose an advanced signal processing technique for the precise estimation of a nonlinear ultrasonic parameter, which is based on power spectral and bispectral analysis. The method of estimating power spectrum and bispectrum of the pulse-like ultrasonic wave signal used in the commercial SAM (scanning acoustic microscopy) equipment is especially considered in this study The usefulness of the proposed method Is confirmed by experiments for a Newton ring with a continuous air gap between two glasses and a real semiconductor sample with local delaminations. The results show that the nonlinear parameter obtained tv the proposed method had a good correlation with the delamination.

The Characteristics of the Wafer Bonding between InP Wafers and $\textrm{Si}_3\textrm{N}_4$/InP (Direct Wafer Bonding법에 의한 InP 기판과 $\textrm{Si}_3\textrm{N}_4$/InP의 접합특성)

  • Kim, Seon-Un;Sin, Dong-Seok;Lee, Jeong-Yong;Choe, In-Hun
    • Korean Journal of Materials Research
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    • v.8 no.10
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    • pp.890-897
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    • 1998
  • The direct wafer bonding between n-InP(001) wafer and the ${Si}_3N_4$(200 nm) film grown on the InP wafer by PECVD method was investigated. The surface states of InP wafer and ${Si}_3N_4$/InP which strongly depend upon the direct wafer bonding strength between them when they are brought into contact, were characterized by the contact angle measurement technique and atomic force microscopy. When InP wafer was etched by $50{\%}$ HF, contact angle was $5^{\circ}$ and RMS roughness was $1.54{\AA}$. When ${Si}_3N_4$ was etched by ammonia solution, RMS roughness was $3.11{\AA}$. The considerable amount of initial bonding strength between InP wafer and ${Si}_3N_4$/InP was observed when the two wafer was contacted after the etching process by $50{\%}$ HF and ammonia solution respectively. The bonded specimen was heat treated in $H^2$ or $N^2$, ambient at the temperature of $580^{\circ}C$-$680^{\circ}C$ for lhr. The bonding state was confirmed by SAT(Scannig Acoustic Tomography). The bonding strength was measured by shear force measurement of ${Si}_3N_4$/InP to InP wafer increased up to the same level of PECVD interface. The direct wafer bonding interface and ${Si}_3N_4$/InP PECVD interface were chracterized by TEM and AES.

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Cell-cultivable ultrasonic transducer integrated on glass-coverslip (세포 배양 가능한 커버슬립형 초음파 변환자)

  • Keunhyung Lee;Jinhyoung Park
    • The Journal of the Acoustical Society of Korea
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    • v.42 no.5
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    • pp.412-421
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    • 2023
  • Ultrasound brain stimulation is spot-lighted by its capability of inducing brain cell activation in a localized deep brain region and ultimately treating impaired brain function while the efficiency and directivity of neural modulation are highly dependent on types of stimulus waveforms. Therefore, to optimize the types of stimulation parameters, we propose a cell-cultivable ultrasonic transducer having a series stack of a spin-coated polymer piezoelectric element (Poly-vinylidene fluoride-trifluorethylene, PVDF-TrFE) and a parylene insulating layer enhancing output acoustic pressure on a glass-coverslip which is commonly used in culturing cells. Due to the uniformity and high accuracy of stimulus waveform, tens of neuronal cell responses located on the transducer surface can be recorded simultaneously with fluorescence microscopy. By averaging the cell response traces from tens of cells, small changes to the low intensity ultrasound stimulations can be identified. In addition, the reduction of stimulus distortions made by standing wave generated from reflections between the transducers and other strong reflectors can be achieved by placing acoustic absorbers. Through the proposed ultrasound transducer, we could successfully observe the calcium responses induced by low-intensity ultrasound stimulation of 6 MHz, 0.2 MPa in astrocytes cultured on the transducer surface.

The Electrical Properties and Resonant Frequency of Pt/Pb(Zr,Ti)$O_3$/Pt Films (Pt/Pb(Zr,Ti)$O_3$/Pt 박막의 전기적 특성과 공진주파수에 관한 연구)

  • Park, Young;Lee, Ki-Won;Jang, Dong-Uk;Park, Hyun-June;Park, Gi-Yub;Choi, Won-Seok;Song, Joon-Tae
    • Proceedings of the KIEE Conference
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    • 2004.07c
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    • pp.1552-1554
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    • 2004
  • The modeled resonant frequency and electrical properties of Pb(Zr, Ti)$O_3$ (PZT) film with various thicknesses have been investigated in film bulk acoustic wave resonators (FBARs). PZT films and Pt electrodes were fabricated by rf-magnetron sputtering. Fabrication process of electrodes and PZT were patterned by simple lift-off process and then back side of silicon was etched by 45wt% KOH. The crystal structure of PZT films with 0.5, 1 and 2 ${\mu}m$ thickness was investigated by x-ray deflection (XRD) and scanning electron microscopy (SEM). The dielectric constant and performance characteristics of PZT FBAR strongly depended on the film thickness. The resonant frequency of PZT films decreased with increasing film thickness. These sputtered PZT FBAR with simple lift-off process enable us to fabricate high Q values with resonant frequencies. (0.71 - 1.48 GHz).

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CNT-PDMS Composite Thin-Film Transmitters for Highly Efficient Photoacoustic Energy Conversion

  • Song, Ju Ho;Heo, Jeongmin;Baac, Hyoung Won
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.297.2-297.2
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    • 2016
  • Photoacoustic generation of ultrasound is an effective approach for development of high-frequency and high-amplitude ultrasound transmitters. This requires an efficient energy converter from optical input to acoustic output. For such photoacoustic conversion, various light-absorbing materials have been used such as metallic coating, dye-doped polymer composite, and nanostructure composite. These transmitters absorb laser pulses with 5-10 ns widths for generation of tens-of-MHz frequency ultrasound. The short optical pulse leads to rapid heating of the irradiated region and therefore fast thermal expansion before significant heat diffusion occurs to the surrounding. In this purpose, nanocomposite thin films containing gold nanoparticles, carbon nanotubes (CNTs), or carbon nanofibers have been recently proposed for high optical absorption, efficient thermoacosutic transfer, and mechanical robustness. These properties are necessary to produce a high-amplitude ultrasonic output under a low-energy optical input. Here, we investigate carbon nanotube (CNT)-polydimethylsiloxane (PDMS) composite transmitters and their nanostructure-originated characteristics enabling extraordinary energy conversion. We explain a thermoelastic energy conversion mechanism within the nanocomposite and examine nanostructures by using a scanning electron microscopy. Then, we measure laser-induced damage threshold of the transmitters against pulsed laser ablation. Particularly, laser-induced damage threshold has been largely overlooked so far in the development of photoacoustic transmitters. Higher damage threshold means that transmitters can withstand optical irradiation with higher laser energy and produce higher pressure output proportional to such optical input. We discuss an optimal design of CNT-PDMS composite transmitter for high-amplitude pressure generation (e.g. focused ultrasound transmitter) useful for therapeutic applications. It is fabricated using a focal structure (spherically concave substrate) that is coated with a CNT-PDMS composite layer. We also introduce some application examples of the high-amplitude focused transmitter based on the CNT-PDMS composite film.

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Critical Cleaning Requirements for Flip Chip Packages

  • Bixenman, Mike;Miller, Erik
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2000.04a
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    • pp.43-55
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    • 2000
  • In traditional electronic packages the die and the substrate are interconnected with fine wire. Wire bonding technology is limited to bond pads around the peripheral of the die. As the demand for I/O increases, there will be limitations with wire bonding technology. Flip chip technology eliminates the need for wire bonding by redistributing the bond pads over the entire surface of the die. Instead of wires, the die is attached to the substrate utilizing a direct solder connection. Although several steps and processes are eliminated when utilizing flip chip technology, there are several new problems that must be overcome. The main issue is the mismatch in the coefficient of thermal expansion (CTE) of the silicon die and the substrate. This mismatch will cause premature solder Joint failure. This issue can be compensated for by the use of an underfill material between the die and the substrate. Underfill helps to extend the working life of the device by providing environmental protection and structural integrity. Flux residues may interfere with the flow of underfill encapsulants causing gross solder voids and premature failure of the solder connection. Furthermore, flux residues may chemically react with the underfill polymer causing a change in its mechanical and thermal properties. As flip chip packages decrease in size, cleaning becomes more challenging. While package size continues to decrease, the total number of 1/0 continue to increase. As the I/O increases, the array density of the package increases and as the array density increases, the pitch decreases. If the pitch is decreasing, the standoff is also decreasing. This paper will present the keys to successful flip chip cleaning processes. Process parameters such as time, temperature, solvency, and impingement energy required for successful cleaning will be addressed. Flip chip packages will be cleaned and subjected to JEDEC level 3 testing, followed by accelerated stress testing. The devices will then be analyzed using acoustic microscopy and the results and conclusions reported.

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The Ultrasonic Image Processing by Peak Value, Time Average and Depth Profile Technique in High Frequency Bandwidth (고주파대역에서 피크값, Time Average 및 Depth Profile 초음파 영상처리)

  • 이종호
    • Journal of the Korean Institute of Telematics and Electronics T
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    • v.35T no.3
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    • pp.120-127
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    • 1998
  • In this paper, ultrasonic images of 25MHz bandwidth were acquired by applying peak value variation, time average and depth profile algorithm to acoustic microscopy and its performance was compared and analysed with each other. In the time average algorithm, total reflecting pulse wave from a spot on the coin was converted to digital data in time domain and average value of the converted 512 data was calculated in computer. Time average image was displayed by gray levels colour of acquired N x N matrix average data in the scanning area on the sample. This technique having smoothing effects in time domain make developed an ultrasonic image on a highly scattering area. In depth profile technique, time difference between the reference and the reflected signal was detected with minimum resolution performance of 2ns, thus we can acquired real 3 dimensional shape of the scanning area in accordance with relative magnitude. Through these experiments, peak value, time average and depth profile images were analysed and advantages of each algorithm were proposed.

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An experimental study on triaxial failure mechanical behavior of jointed specimens with different JRC

  • Tian, Wen-Ling;Yang, Sheng-Qi;Dong, Jin-Peng;Cheng, Jian-Long;Lu, Jia-wei
    • Geomechanics and Engineering
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    • v.28 no.2
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    • pp.181-195
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    • 2022
  • Roughness and joint inclination angle are the important factors that affect the strength and deformation characteristics of jointed rock mass. In this paper, 3D printer has been employed to make molds firstly, and casting the jointed specimens with different joint roughness coefficient (JRC), and different joint inclination angle (α). Conventional triaxial compression tests were carried out on the jointed specimens, and the influence of JRC on the strength and deformation parameters was analyzed. At the same time, acoustic emission (AE) testing system has been adopted to reveal the AE characteristic of the jointed specimens in the process of triaxial compression. Finally, the morphological of the joint surface was observed by digital three-dimensional video microscopy system, and the relationship between the peak strength and JRC under different confining pressures has been discussed. The results indicate that the existence of joint results in a significant reduction in the strength of the joint specimen, JRC also has great influence on the morphology, quantity and spatial distribution characteristics of cracks. With the increase of JRC, the triaxial compressive strength increase, and the specimen will change from brittle failure to ductile failure.

Dual-mode diagnosis system for water quality and corrosion in pipe using convolutional neural networks (CNN) and ultrasound (합성곱 신경망과 초음파 기반 상수도관 수질 및 부식 분석용 이중모드 진단 시스템)

  • So Yeon Moon;Hyeon-Ju Jeon;Yeongho Sung;Min-Seo Kim;Daehun Kim;Jaeyeop Choi;Junghwan Oh;O-Joun Lee;Hae Gyun Lim
    • Proceedings of the Korea Information Processing Society Conference
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    • 2023.11a
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    • pp.685-686
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    • 2023
  • 상수도관의 수질 및 부식도 검사에는 파이프에 손상을 입히지 않고 지속적인 방법이 필요하다. 초음파는 이를 만족하면서 상태를 확인할 수 있고 주파수가 높을수록 해상도가 좋아져 정밀한 측정이 가능하다는 장점이 있다. 이러한 특성을 이용해 상수도관 모니터링 시스템으로 초음파 기반의 Scanning Acoustic Microscopy(SAM)과 Convolutional Neural Network(CNN)을 사용하는 새로운 방법을 제안한다. 기존의 Non-Destructive Testing(NDT)방식의 단점을 보완하면서 더 높은 해상도로 상수도관을 점검하는 방식으로, SAM 을 이용하여 부식으로 인한 파이프 두께 변화와 부유물의 여부 및 수질을 동시에 감지하고 얻은 데이터를 CNN 으로 분석했다. CNN 의 높은 정확도 결과로 이 시스템의 파이프 부식도 및 수질 모니터링에 대한 적합성을 보여주었다.