• 제목/요약/키워드: Acidity, Measurement

검색결과 87건 처리시간 0.025초

THE NONDESTRUCTIVE MEASUREMENT OF THE SOLUBLE SOLID AND ACID CONTENTS OF INTACT PEACH USING VIS/NIR TRANSMITTANCE SPECTRA

  • Hwang, I.G.;Noh, S.H.;Lee, H.Y.;Yang, S.B.
    • 한국농업기계학회:학술대회논문집
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    • 한국농업기계학회 2000년도 THE THIRD INTERNATIONAL CONFERENCE ON AGRICULTURAL MACHINERY ENGINEERING. V.II
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    • pp.210-218
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    • 2000
  • Since the SSC(soluble solid contents) and titratable acidity of fruit are highly concerned to the taste, the need for measuring them by non-destructive technology such as NIR(Visual and Near-infrared) spectroscopy is increasing. Specially, in order to grade the quality of each fruit with a sorter at sorting and packing facilities, technologies for online measurement satisfying the tolerance in terms of accuracy and speed should be developed. Many researches have been done to develop devices to measure the internal qualities of fruit such as SSC, titratable acidity, firmness, etc. with the VIS(Visual)/NIR(Near Infrared) reflectance spectra. The distributions of the SSC, titratable acidity, firmness, etc. are different with respect to the position and depth of fruit, and generally the VIS/NIR light can interact with fruit in a few millimeters of pathlength, and it is very difficult to measure the qualities of inner flesh of fruit. Therefore, to measure the average concentrations of each quality factor such as SSC and titratable acidity with the reflectance-type NIR devices, the spectra of fruit at several positions should be measured. Recently, the interest about the transmittance-type VIS/NIR devices is increasing. NIR light can penetrate through the fruit about 1/10-1/1,000,000 %. Therefore, very intensive light source and very sensitive sensor should be adopted to measure the transmitted light spectra of intact fruit. The ultimate purpose of this study was to develop a device to measure the transmitted light spectra of intact fruit such as apple, pear, peach, etc. With the transmittance-type VIS/NIR device, the feasibility of measurement of the SSC and titratable acidity in intact fruit cultivated in Korea was tested. The results are summarized as follows; A simple measurement device which can measure the transmitted light spectra of intact fruit was constructed with sample holder, two 500W-tungsten halogen lamps, a real-time spectrometer having a very sensitive CCD array sensor and optical fiber probe. With the device, it was possible to measure the transmitted light spectra of intact fruit such as apple, pear and peach. Main factors affecting the intensity of transmitted light spectra were the size of sample, the radiation intensity of light source and the integration time of the detector. Sample holder should be designed so that direct light leakage to the probe could be protected. Preprocessing method to the raw spectrum data significantly influenced the performance of the nondestructive measurement of SSC and titratable acidity of intact fruit. Representative results of PLS models in predicting the SSC of peach were SEP of 0.558 Brix% and R2 of 0.819, and those in predicting titratable acidity were SEP of 0.056% and R2 of 0.655.

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한지의 산성도 측정을 위한 비파괴적 방법의 적용 (The application of a nondestructive method to measure the acidity of Korean papers)

  • 이혜윤;정용재;이규식;한성희
    • 보존과학연구
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    • 통권20호
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    • pp.21-47
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    • 1999
  • According to damage of papers by the chemical cause, papers become to acidify. Among the 3 kinds of method measuring the acidity of paper, one was nondestructive method measuring the surface of the paper by flat type electrode and the others were destructive methods measuring directly by cold water extract method and hot water extract method. In case of the cellulolytic cultural properties, the latter methods were not applied because those methods must bedissociated papers. To measure the paper acidity nondestructively, we investigated the correlation of the nondestructive method and the destructive methods. The conclusions are as follows. 1) In the relationship of the cold water extract method and the hot water extract method, It was indicated that the pH measured by the hot water extract method was high quality printing paper 0.08, rough printing paper 0.13, and Korean paper 0.29 higher than that by the cold water extract method.2) In the relationship of the cold water extract method and the surface measurement method, It showed that the pH value measured by the cold water extract method was high quality printing paper 1.86, rough printing paper 0.80,and Korean paper 0.58 higher than value that by the surface measurement.3) In the relationship of the hot water extract method and the surface measurement method, It showed that the pH value measured by the hot ABSTRACT water extract method was high quality printing paper 1.78, rough printing paper 0.66, and Korean paper 0.29 higher than that by the surface measurement. From the above-mentioned results, the pH value measured by the surface measurement was need to high about 1.78∼1.86 in high quality printing paper, 0.66-0.80 in rough printing paper, and 0.29∼0.58 in Korean paper and the surface measurement with flat type electrode was very available to measure the acidity of Korean papers actually.

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雨水採取機가 雨水成分에 미치는 影響 (Effects of Rain Water Sampler on the Results of Analysis)

  • 李敏熙;韓義正;辛燦基;韓振錫
    • 한국대기환경학회지
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    • 제3권2호
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    • pp.53-61
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    • 1987
  • Automatic and manual rain smaplers wre installed at the roof of National Institute of Environmental Research (NIER), and the rain sampling and measurement were conducted during the period April to August 31, 1987. The rain sampling and measurement were carried out in the following manners: The 1st : Acidity and conductivity were measured entirely by automatic rain sampler (continuous measurement) The 2nd : Acidity and conductivity wrer measured in the laboratory with the sample that was taken out of automatic rain sampler. The 3rd : Acidity and conductivity were measured in the laboratory with the sample that was taken out of manual rain sampler. Afterwards, those different measurement values were compared each other and the following conclusions were obtained: 1) The pH of the continous measurement by the automatic sampler was lower than that of the laboratory measurement, and it was reversed in case of the conductivity. 2) The significance was recognized at 5% risk ratio for the population mean of difference of the measurement values of the pH and conductivity from both samples. 3) The significance was not recognized at 5% risk ratio by the analysis of variance by one way layout for the pH and conductivity. 4) The significance was recognized at 5% risk ratio by the analysis of variance by two way layouts for the pH conductivity. 5) The significance was recognized at 5% rrisk ratio for the differences of the pH values obtained by oboth samplers, and no significance was recognized for conductivity. 6) In comparison of the measurement values from the two samplers were shown a good correlation for pH; correlation coefficient (r) = 0.63, and regression equation Y = 0.53X + 2.78. For conductivity, the correlation was also excellent; correlation coefficient (r) = 0.53 and regression equation Y = 0.63X + 5.65.

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발굴현장 수습 유물 보존처리 (On-site conservation of a gilt bronze crown)

  • 유재은
    • 보존과학연구
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    • 통권20호
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    • pp.49-64
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    • 1999
  • According to damage of papers by the chemical cause, papers become to acidify. Among the 3 kinds of method measuring the acidity of paper, one was nondestructive method measuring the surface of the paper by flat type electrode and the others were destructive methods measuring directly by cold water extract method and hot water extract method. In case of the cellulolytic cultural properties, the latter methods were not applied because those methods must bedissociated papers. To measure the paper acidity nondestructively, we investigated the correlation of the nondestructive method and the destructive methods. The conclusions are as follows. 1) In the relationship of the cold water extract method and the hot water extract method, It was indicated that the pH measured by the hot water extract method was high quality printing paper 0.08, rough printing paper 0.13, and Korean paper 0.29 higher than that by the cold water extract method.2) In the relationship of the cold water extract method and the surface measurement method, It showed that the pH value measured by the cold water extract method was high quality printing paper 1.86, rough printing paper 0.80,and Korean paper 0.58 higher than value that by the surface measurement.3) In the relationship of the hot water extract method and the surface measurement method, It showed that the pH value measured by the hot ABSTRACT water extract method was high quality printing paper 1.78, rough printing paper 0.66, and Korean paper 0.29 higher than that by the surface measurement. From the above-mentioned results, the pH value measured by the surface measurement was need to high about 1.78∼1.86 in high quality printing paper, 0.66-0.80 in rough printing paper, and 0.29∼0.58 in Korean paper and the surface measurement with flat type electrode was very available to measure the acidity of Korean papers actually.

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수종 치과용 시멘트 경화시 초기 산도측정에 관한 실험적 연구 (AN EXPERIMENTAL STUDY ON THE MEASUREMENT OF THE INITIAL ACIDITY OF DENTAL CEMENTS)

  • 이명종
    • Restorative Dentistry and Endodontics
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    • 제16권2호
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    • pp.189-196
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    • 1991
  • The purpose of this study was to observe the inital acidity of zinc phosphate cements(Confit and Super Cem), poly carboxylate cement(Unident and Poly F), zinc oxide engenol cement(Stailine Super EBA) and g1ass ionomer cement(Fuji ionomer) Each cement was manuplated in accordance with each manufacturer's direction. All cements were mixed at the room temperature of $23^{\circ}{\pm}$, $5^{\circ}C$, and the electrode of pH meter(Ionanalyzer) was inserted in the mixed cement, and the acidity of cement were measured for 20 minutes from begining of cement mixing at $23^{\circ}C$ and $37^{\circ}C$ Results were as follows 1. The acidity of all cements ranges from pH 3, 5 to 4, 5 at 2 minutes after the start of mixing 2. The value of pH at $23^{\circ}C$ was higher than the value of pH at $37^{\circ}C$ in all cements. 3. As the time elapsed, the pH in all cements rose. The 20 minutes after the start of mixing the range of acidity was from pH 5 to pH 6 except Poly F. 4. In polycarboxylate cement, the different value of acidity at $23^{\circ}C$ and $37^{\circ}C$ was greatest. 5. The curve pattern of acidity in Unident was similar to that in Poly F cement The pH value of Unident was higher then that of Poly F, and value of pH in the curve pattern of acidity in Confit were similar to those in Super cement.

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타액검사기의 신뢰도 평가 (Evaluation of the Reliability of Salivary Testing Instrument)

  • 한금아;이준행
    • 대한소아치과학회지
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    • 제45권3호
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    • pp.363-369
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    • 2018
  • 타액검사기는 방법이 간단하고 단시간 내에 검사를 할 수 있는 장점이 있다. 하지만 타액 채취가 용이하고 장치의 사용이 간단하나 그 결과의 신뢰성에 영향을 미치는 요인에 대해서는 검증해 볼 필요가 있다. 이번 연구는 타액검사기의 측정 결과에 영향을 미칠 수 있는 요인 중 외부변수인 시간적 요인을 분석하기 위해 측정 시간에 따른 검사 결과의 차이를 비교하였다. 또한 내부변수를 파악하기 위해 타액검사기 측정값 사이의 관련성을 분석하였다. 나이, 성별, 질환의 유무에 상관없이 무작위적으로 선정한 20명의 사람들을 대상으로 하여 타액을 채취하였다. 평균 나이는 46.6세였고, 남자 10명, 여자 10명이었다. 채취한 타액을 바로 타액검사기로 측정한 것을 I군으로 하였다. 또한 채취한 타액을 종이컵에서 10분간 공기중에 방치한 후 타액검사기로 측정한 것을 III군으로 하였다. 그리고 I군으로 사용한 것을 30분 후 재 측정하여 II군으로, III군으로 사용한 것을 30분 후 재 측정한 것을 IV군으로 하였다. 실험 결과 cariogenic bacteria, acidity, buffer capacity, blood, leukocyte, protein and ammonia 중 buffer capacity만 제외하고 나머지는 모두 II, IV군에서 유의한 변화가 있었다. 또한 측정값 중 cariogenic bacteria는 leukocyte, protein과 상호관련성이 있었고 buffer capacity는 acidity, protein과, 그리고 protein은 buffer capacity, leukocyte와 연관성이 있었다. 결론적으로 외부변수인 측정 시간에 따른 측정결과 값의 차이는 각각 다르게 나타났으며, 이는 타액검사 시 시간요인의 중요성을 의미하는 것이다. 또한 내부변수인 측정값 간의 상호관계를 이용하여 임상적으로 접근할 경우 그 연관성에 대한 고려가 필요하다.

대기중의 산성도(H+) 측정 (Measurement of Aerosol Acidity ($H^+$) in Ambient Air)

  • 이학성
    • 한국환경과학회지
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    • 제4권1호
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    • pp.53-62
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    • 1995
  • 대기중의 산성도($H^+$)를 측정하기 위하여 디누더 시스템(Annula Denuder System)을 이용하였다. 산성도 측정은 1990년 4월 부터 1001년 3월 까지 미국 시카고에서 81개 샘플을 12시간 동안 낮과 밤을 구분하여 측정하였다. 본 연구를 통하여 대기중의 산성도 측정은 디누더 시스템을 이용하면 보다 정확한 결과를 얻을 수 있을음 알 수 있었다. 여과지에 포집된 산성도($H^+$)를 추출해 낼때 사용하는 $HCIO_4$용액은 $10^{-5}N$의 농도를 사용하는 것이 $10^{-4}N$의 농도보다 더 정확한 결과를 얻을 수 있다. 보다 정확한 산성도를 측정하기 위해서는 에어로졸이 여과지에 포집되기 전에 가스 상태의 $NH_3$가 먼저 제거되어야 한다. 산성도는 계절에 따라 변하였고 여름에 가장 높은 농도를 나타냈다. $SO_4^{2+}$NH_4^+$, 그리고 $SO_4^{2+}$H^+$의 상관관계는 높은 것으로 나타났다.

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동결농축법을 이용한 고산도 복분자 농축식초 제조에 관한 연구 (A Study on High-acidity Rubus coreanus Concentrated Vinegar Production Using Freeze Concentration Method)

  • 성지연;이익희
    • 한국융합학회논문지
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    • 제12권11호
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    • pp.419-426
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    • 2021
  • 최근까지 고산도 식초 제조를 위한 다양한 연구가 진행되어 왔으나 식초의 농축공정에 대한 연구는 거의 없었다. 본 연구에서는 고품질의 고산도 식초 제조를 위해 동결농축법의 도입 가능성을 알아보았다. 총산도가 서로 다른 3종류(7.53, 5.43, 및 3.72)의 복분자 발효식초를 동결 및 융해시켜 얻은 동결농축식초분획을 대상으로 총산도, 산도pH, 비중 및 포도당 농도를 측정하였다. 총산도, 비중 및 포도당 농도 모두 최초식초의 15%가 융해되었을 때 가장 높은 것으로 나타났다. 산도pH는 최초식초의 15%가 융해되었을 때 가장 낮은 것으로 나타났다. 누적산도 측정결과 최초식초의 20%가 융해되었을 때 9.32로 가장 높았는데 이는 최초식초보다 3.89높은 수치였다. 본 연구에서는 동결농축법을 이용하여 식초를 효과적으로 농축할 수 있을 뿐 만 아니라 융해비율 조정으로 원하는 총산도의 식초를 효과적으로 얻을 수 있음을 확인하였다. 그러나 고산도 농축식초 제조공정에 동결농축법의 도입여부를 판단하기 위해서는 유기산 및 아미노산 분석 등의 연구가 필요할 것으로 사료된다.

가시광 및 근적외선 분광기법을 이용한 방울토마토의 내부품질 예측에 관한 연구 (Study on Prediction of Internal Quality of Cherry Tomato using Vis/NIR Spectroscopy)

  • 김대용;조병관;모창연;김영식
    • Journal of Biosystems Engineering
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    • 제35권6호
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    • pp.450-457
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    • 2010
  • Although cherry tomato is one of major vegetables consumed in fresh vegetable market, the quality grading method is mostly dependant on size measurement using drum shape sorting machines. Using Visible/Near-infrared spectroscopy, apparatus to be able to acquire transmittance spectrum data was made and used to estimate firmness, sugar content, and acidity of cherry tomatoes grown at hydroponic and soil culture. Partial least square (PLS) models were performed to predict firmness, sugar content, and acidity for the acquired transmittance spectra. To enhance accuracy of the PLS models, several preprocessing methods were carried out, such as normalization, multiplicative scatter correction (MSC), standard normal variate (SNV), and derivatives, etc. The coefficient of determination ($R^2_p$) and standard error of prediction (SEP) for the prediction of firmness, sugar, and acidity of cherry tomatoes from green to red ripening stages were 0.859 and 1.899 kgf, with a preprocessing of normalization, 0.790 and $0.434^{\circ}Brix$ with a preprocessing of the 1st derivative of Savitzky Golay, and 0.518 and 0.229% with a preprocessing normalization, respectively.

해염성분에 의한 에어로솔 물성변화 모사연구 (A Modeling Study on Aerosol Property Changes due to Sea-Salts)

  • 김용표
    • 한국대기환경학회지
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    • 제16권2호
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    • pp.113-120
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    • 2000
  • Effects of sea-salts on the properties of aerosol collected in a coastal region were studied by applying a gas-particle equilibrium model SCAPE to the measurement data from Korea Cheju Island in summer 1994. It was found that the observed higher ammonium concentrations in fine particles (PM2.5) than in TSP were caused by forced evaporation of ammonium in coarse fraction of aerosol by sea-salts and the degree of evaporation was quantified through an application of SCAPE. By subtracting the sea-salt fraction from the measured concentra-tions the changes of aerosol property were also studied. The concentrations of nitrate at both TSP and PM2.5 decreased when alkaline sea-salt fraction was removed from the measured data. Estimates of aerosol acidity increased for most samples with sea salt loadings, However in some cases with high mass fractions of sea-salt components the aerosol acidity of PM2.5 decreased slightly. This is though to be related with the formation of solid salt with the removal of sea-salts.

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