• Korean Journal of Materials Research
• /
• v.32 no.7
• /
• pp.326-331
• /
• 2022

AZ31 magnesium alloy was used to manufacture a thin plate using a melt drag method. The effects of roll speed, molten metal temperature, and molten metal height, which are the basic factors of the melt drag method, on the surface shape, the thickness of the thin plate, Vickers hardness, and microstructure of the thin plate were investigated. It was possible to manufacture AZ31 magnesium alloy thin plate at the roll speed range of 1 to 90 m/min. The thickness of the thin plate, manufactured while changing only the roll speed, was about 1.8 to 8.8 mm. The shape of the solidified roll surface was affected by two conditions, the roll speed and the molten metal height, and the Vickers hardness of the manufactured magnesium alloy thin plate value ranged from Hv38~Hv60. The microstructure of the thin plate produced by this process was an equiaxed crystal and showed a uniform grain size distribution. The grain size was greatly affected by the contact state between the molten metal and the solidification roll, and the amount of reactive solids and liquids scraped at the same time as the thin plate. The average grain size of the thin plate fabricated in the range of these experimental conditions changed to about 50-300 ㎛.

• Journal of Welding and Joining
• /
• v.26 no.6
• /
• pp.54-58
• /
• 2008

Laser welding with AZ61 filler wire was carried out to improve formability though reduction of porosity and formation of under fill bead. Optimum welding condition and mechanical properties of butt joint for $400{\times}500{\times}1.3mm$ magnesium sheets were studied. Optimal welding conditions of laser power, welding speed, and defocusing length are 1000W, 3m/min, and 2mm, respectively. Results of tensile test indicated that both tensile strength and elongation of specimens welded with filler wire were improved at room temperature because of reduction of porosity and under-filled bead formation in addition to the precipitation hardening and microstructure refinement by Al-Mn and Mg-Al-Zn precipitates. At elevated temperature of $200{\sim}350^{\circ}C$, fracture location of tensile specimen was shifted from weld metal to base metal, indicating less softening of weld metal than base metal.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2008.10a
• /
• pp.66-70
• /
• 2008

In this study, the formability of AZ31B magnesium alloy sheets was investigated by the analytical and experimental approaches. Tensile tests and limit dome height tests were rallied out at several temperatures between $25^{\circ}C$ and $300^{\circ}C$ to obtain the mechanical properties and forming limit diagram (FLD). The FLD-based criterion considering the strain-path and the blank temperature was used to predict the forming limit in a deep-drawing process of cross-shaped cup by finite element analysis. This criterion proved to be very useful in determining the optimal process conditions such as blank shape, punch velocity, minimum comer radius, fillet size, and so on, through the comparison between FEA and experimental data. In particular, the temperature of each tool that provided the best formability of the blank was determined by coupled temperature-deformation analyses. A practical method that can greatly reduce the forming time by increasing the punch speed during the forming process was suggested.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2006.05a
• /
• pp.63-66
• /
• 2006

The effect of warm rolling under various conditions on the microstructure and mechanical property was investigated using an AZ31 Mg alloy sheet. Several processing parameters such as initial thickness, thickness reduction by a single pass rolling, rolling temperature, roll speed, and roll temperature were varied to elicit an optimum condition for the warm rolling process of AZ31 Mg alloy. Microstructure and mechanical properties were measured for specimens subjected to rolling experiments of various conditions. Warm rolling of 30% thickness reduction per pass was possible without any side-crack at temperatures as low as $200^{\circ}C$ under the roll speed of 30 m/min. The initial microstructure before rolling was the mixed one consisting of partially recrystallized and cast structures. Grain refinement was found to occur actively during the warm rolling, producing a very fine grain size of 7 mm after 50% reduction in single pass rolling at $200^{\circ}C$. Yield strength of 204MPa, tensile strength of 330MPa and uniform elongation of 32% have been obtained in warm rolled sheets.

• Journal of Surface Science and Engineering
• /
• v.44 no.6
• /
• pp.239-245
• /
• 2011

Magnesium alloys is the lightest by structural metals, but it is not good corrosion resistant because of pit, void. Particularly, AZ31B magnesium alloy sheets that have slag, scratch by rolling process indicate some defects. The objective of this research is to perform uniform plating on AZ31B by studying etching and zincate process. Especially, zincate treatment by zinc salt and pyrophosphate is the most important in the decoration plating. Dissolution of magnesium is reduced by the formation of uniform zinc conversion layer during strick and post process, which decreases defects for plating process.

• Journal of Surface Science and Engineering
• /
• v.47 no.4
• /
• pp.147-154
• /
• 2014

Formation behavior of PEO (Plasma Electrolytic Oxidation) films on AZ31 Mg alloy was studied in aqueous solutions containing various concentrations of hydroxide ion ($OH^-$) and silicate ion ($SiO_3{^{2-}}$) by voltage-time curves, and corrosion resistance of the PEO film-covered specimen was investigated by immersion test in 0.5 M NaCl solution. From the analyses of the voltage-time curves, it is suggested that two different types of anions are essentially needed for the formation of PEO films on AZ31 Mg alloy: film formation agent and local film breakdown agent. $SiO_3{^{2-}}$ ion acts only as a film formation agent but $OH^-$ ion acts not only as a film formation agent but also film breakdown agent. The PEO films prepared on AZ31 Mg alloy in alkaline silicate solution showed very good corrosion resistance without any pitting or filiform corrosions up to 480 h of immersion in 0.5 M NaCl.

• Transactions of Materials Processing
• /
• v.15 no.3 s.84
• /
• pp.232-240
• /
• 2006

Magnesium alloys are expected to be widely used fur the parts of structural and electronic appliances due to their lightweight and EMI shielding characteristics. While the die casting has been mainly used to manufacture the parts from the magnesium alloys, the press forming is considered as an alternative to the die casting for saving the manufacturing cost and improving the structural strength of the magnesium alloy parts. However, the magnesium alloy has low formability at room temperature and therefore, in many cases, forming at elevated temperatures is necessary to obtain the required material flow without failure. In the present study, square cup deep drawing tests using the magnesium alloy AZ31 sheet were experimentally conducted at various elevated temperatures as well as room temperature, and the corresponding finite-element simulations, which calculated the damage evolution based on the Oyane's criterion, were conducted using the stress-strain relations from the tensile tests at various temperatures. The formability predictability by the finite-element analysis was investigated by comparing the predicted damage distributions over the deformed AZ31 sheet at elevated temperatures with the corresponding experimental deformations with failures.

• Journal of Surface Science and Engineering
• /
• v.43 no.2
• /
• pp.73-79
• /
• 2010

A chromium-free conversion coating for AZ31 magnesium alloy has been obtained by using a permanganatephosphate solution, which has been developed with acid pickling. Examination have been carried out on the conversion coatings for morphology, composition and corrosion resistance. The morphology of the conversion-coated layer was observed using optical microscope and SEM. It was shown that the conversion coatings are relatively uniform and continuous, with thickness 1.8 to 2.7 ${\mu}m$. The chemical composition of conversion coating was mainly consisted of Mg, O, P, K, Al and Mn by EDS analysis. It was found that the corrosion resistance of the AZ31 magnesium alloy has been improved by the permanganate-phosphate conversion treatment from electrochemical polarization.

• Transactions of Materials Processing
• /
• v.16 no.6
• /
• pp.447-451
• /
• 2007

The springback characteristics of AZ31B magnesium alloy sheet was investigated in OSU draw/bend test Springback is the elastically-driven change of shape of a part after forming and it should be estimated and controlled to manufacture more precise products in sheet forming. Magnesium alloy sheets have unique mechanical properties such as high in-plane anisotropy/asymmetry of yield stress and hardening response. So, there will be a difference in the prediction of springback with symmetric mechanical properties for magnesium alloy sheets. In this work, the Strip draw/bend tests were conducted with various conditions - die radius, sheet thickness and controlled tensile force and the tendency of springback angle was observed from the tests.

• Transactions of Materials Processing
• /
• v.27 no.3
• /
• pp.160-164
• /
• 2018

The success of warm forming of Mg alloy sheets is very dependent on its frictional behavior at elevated temperatures. The effects of contact pressure and sliding length on the frictional characteristics of AZ31B Mg alloy sheet were investigated at elevated temperature and at room temperature. The contact pressure range for the friction test was determined through FE analysis of the roof panel which is a candidate for Mg alloy application. According to the experimental results, the frictional behavior of the Mg alloy sheet is equally highly influenced by both sliding length and contact pressure at room temperature. At elevated temperatures, however, the sliding length has a more dominant influence on the frictional characteristics of the Mg alloy sheet than the contact pressure, if the contact pressure is lower than a certain level.