• Title/Summary/Keyword: AM materials

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Confocal Microscopy of Colloidal Suspensions

  • Kim, Jin Young;Weon, Byung Mook
    • Applied Microscopy
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    • v.44 no.1
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    • pp.30-33
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    • 2014
  • Colloidal systems or colloids consist of microparticles or nanoparticles (solute) uniformly suspended in a liquid (solvent), also called colloidal suspensions. They can mimic and exhibit microscopic or atomic aspects of molecular and atomic systems. They have been increasingly studied because of their similarity with atomic systems. They can be microscopically observed by optical microscopes because they are large enough in size and slow in motion to be monitored; microscopic methods are very useful and powerful in research on colloidal systems. Recently, confocal laser microscopy has been known as a powerful tool to obtain information of real-space and real-time behaviors of colloidal suspensions. In particular, it is possible to exactly track individual colloids in three dimensions with confocal microscopy. In this article, we briefly discuss the usefulness of confocal microscopy in colloidal systems that are currently used as model systems to resolve important questions in materials science.

The electrochemical properties of $TiO_2$ photoanode using SBM co-polymer binders (SBM 고분자중합 바인더가 사용된 $TiO_2$ 광전극의 전기화학적 특성)

  • Jin, En-Mei;Park, Kyung-Hee;Gu, Hal-Bon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.360-361
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    • 2008
  • A new kind of SBM co-polymer binder as styrene, n-butyl acrylate, and methacrylic acid (SBM) monodisperse co-polymer binder materials basted on $TiO_2$ pastes was synthesized and this $TiO_2$ pastes were applied of dye-sensitized solar cells (DSSCs). The SBM co-polymer binder was prepared by soap-free emulsion copolymerization using a PEG-EEM macromonomer. The photoanodes were characterized by morphology investigated from field emission scanning electron microscopy (FE-SEM). The photoelectrochemical properties of the thin films and the performance of DSSCs were measured by photovoltaic-current density. DSSC based on the emulsion co-polymer binder was obtained conversion efficiency of 7.1% under irradiation of AM 1.5($100mWcm^{-2}$).

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AC Plasma Power Supply with Variable Voltage and Variable Frequency (가변전압 가변주파수(VVVF) 교류 플라즈마 전원장치)

  • Shin Wan-Ho;Yun Kee-Pok;Jeoung Hwan-Myoung;Choi Jae-Ho
    • Proceedings of the KIEE Conference
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    • summer
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    • pp.1205-1207
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    • 2004
  • AC plasma power supply is used to control a ozone generator and a air pollution gas. AC plasma power supply is composed of power semiconductor switch devices and control board adapted SHE(Selected Harmonic Elimination) PWM method. AC plasma power supply with sinusoidal VVVF(variable voltage and variable frequency) is realized. Its output voltage range is from 0 [V] to 20[kV] and output frequency range is from 8[kHz] to 20[kHz]. Using proposed system, AC high voltage and high frequency discharge is tested in the DBD(dieletric barrier discharge) reactor, and the space distribution of a its non-thermal plasma is observed. In spite of the increasement of voltage and frequency, the proposed system have a stable operation characteristics. It is verified by the experimental results.

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A Study on Web Document's Efficient Browsing

  • Kim, Dong-Hyun;Song, Seung-Heon;Kim, Eung-Kon
    • Journal of information and communication convergence engineering
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    • v.1 no.2
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    • pp.88-92
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    • 2003
  • Most document consists of primary content and supporting material, such as footnotes, detailed explanations, and illustrations, and the related supporting materials are linked as hypertext on web document. However, the content of hypertext links is appeared in the new windows on present web browser. Then the user will leave the primary material, may lose the entire context, and must have some difficulties to return to the primary context when the interest disappears. Using the technique for fluid links, we can solve these problems easily. If the mouse is putted on the link, the related material is presented in between lines or at margin maintaining the context of primary material. In this paper, we introduce the various browsing techniques using fluid links, analyze the forms and the features, and then we propose the way to implement in Java.

A Design of the Thickness Gauge Using the Compton Gamma-ray Backscattering

  • B.S. Moon;Kim, Y.K.;Kim, J.Y.;Kim, J.T.;C.E. Chung;S.B. Hong
    • Nuclear Engineering and Technology
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    • v.32 no.5
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    • pp.457-464
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    • 2000
  • In this paper, we describe the results of various calculations performed for a design of the thickness gauges that use the gamma-ray backscattering method. The radiation source is assumed to be the $_{24}$1Am(60keV gamma-ray) and the detector is a single crystal scintillator in a cylindrical form. The source is located at the center of the detector with the collimator of a cylindrical shape. First, when gamma-rays are incident on a material with a constant angle, we compute the variations of the spectrum for the photons scattered into different angular intervals. Next, we compute for an optimal size for the collimator cylinder for a fixed detector size and an optimal distance from the detector to the material. Finally, we compute the number of observed photons for different thickness of two different materials, a plastic film and an Al foil.

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Experimental and FE Analysis to Improve the Accuracy of Springback Prediction on Sheet Metal Forming (판재 성형품의 탄성회복예측 정밀도 향상을 위한 실험 및 해석)

  • Lee Y. S.;Kim M. C.;Kwon Y, N.;Lee J. H.
    • Transactions of Materials Processing
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    • v.13 no.6 s.70
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    • pp.490-496
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    • 2004
  • Springback comes from the release of external loads after forming. The control of phenomenon is especially important in the sheet metal forming since there are no other practical methods available to correct the dimensional inaccuracy from springback. Therefore the accurate prediction before the die machining has been a long goal in the field of sheet metal forming. The am of the present study is to enhance the prediction capability of finite element (FE) analysis for the springback phenomenon. For this purpose FE analysis for V-bending has been carried out with the commercial programs, LS-DYNA. The FE analysis results have been validated through the comparison of experimental. The experimental results measured directly by the strain gauge have given the confidence to FEA.

Physical Properties of MoS2

  • Lee, Chang-Gu
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.100-100
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    • 2013
  • Among recently discovered 2-dimensional materials, molybdenum disulfide has fascinating physical properties. It is atomically thin and is a semiconductor with with a similar level of bandgap with silicon. Especially, its properties get interesting when it becomes thinner. Its bandgap goes through bandgap transition from indirect to direct gap. Also its gap size increases as its thickness decreases. In this talk, I am going to present our recent work on characterization of its electrical and optical properties. We used Raman and PL spectroscopy to observe its property dependence on thickness. We fabricated electrical devices to study optimal condition for MoS2 devices. Also we synthesized large-area MoS2 films for devices applications.

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Fabrication of enzymatic biosensor based on the poly(3-thiophenecarboxylic acid-co-thiophene) polymer as electron-transfer materials

  • Kim, Soo-Yeoun;Jo, Hyeon-Jin;Choi, Seong-Ho
    • Journal of the Korean Applied Science and Technology
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    • v.36 no.1
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    • pp.269-278
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    • 2019
  • We fabricated glucose oxidase (GOx)-modified biosensor for detection of glucose by physical immobilization of GOx after electrochemical polymerization of the conductive mixture monomers of the 3-thiophenecarboxylic acid (TCA) and thiophene (Th) onto ITO electrode in this study. We confirmed the successfully fabrication of GOx-modified biosensor via FT-IR spectroscopy, SEM, contact angle, and cyclic voltammetry. The fabricated biosensor has the detection limit of $0.1{\mu}M$, the linearity of 0.001-27 mM, and sensitivity of $38.75mAM^{-1}cm^{-2}$, respectively. The fabricated biosensor exhibits high interference effects to dopamine, ascorbic acid, and L-cysteine, respectively. From these results, the fabricated GOx-modified biosensor with long linearity and high sensitivity could be used as glucose sensor in human blood sample.

New Liquid Crystal-Embedded PVdF-co-HFP-Based Polymer Electrolytes for Dye-Sensitized Solar Cell Applications

  • Vijayakumar, G.;Lee, Meyoung-Jin;Song, Myung-Kwan;Jin, Sung-Ho;Lee, Jae-Wook;Lee, Chan-Woo;Gal, Yeong-Soon;Shim, Hyo-Jin;Kang, Yong-Ku;Lee, Gi-Won;Kim, Kyung-Kon;Park, Nam-Gyu;Kim, Suhk-Mann
    • Macromolecular Research
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    • v.17 no.12
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    • pp.963-968
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    • 2009
  • Liquid crystal (LC; E7 and/or ML-0249)-embedded, poly(vinylidenefluoride-co-hexafluoropropylene) (PVdF-co-HFP)-based, polymer electrolytes were prepared for use in dye-sensitized solar cells (DSSCs). The electrolytes contained 1-methyl-3-propylimidazolium iodide (PMII), tetrabutylammonium iodide (TBAI), and iodine ($I_2$), which participate in the $I_3^-/I^-$ redox couple. The incorporation of photochemically stable PVdF-co-HFP in the DSSCs created a stable polymer electrolyte that resisted leakage and volatilization. DSSCs, with liquid crystal(LC)-embedded PVdF-co-HFP-based polymer electrolytes between the amphiphilic ruthenium dye N719 absorbed to the nanocrystalline $TiO_2$ photoanode and the Pt counter electrode, were fabricated. These DSSCs displayed enhanced redox couple reduction and reduced charge recombination in comparison to that fabricated from the conventional PVdF-co-HFP-based polymer electrolyte. The behavior of the polymer electrolyte was improved by the addition of optimized amounts of plasticizers, such as ethylene carbonate (EC) and propylene carbonate (PC). The significantly increased short-circuit current density ($J_{sc}$, $14.60\;mA/cm^2$) and open-circuit voltage ($V_{oc}$, 0.68 V) of these DSSCs led to a high power conversion efficiency (PCE) of 6.42% and a fill factor of 0.65 under a standard light intensity of $100\;mW/cm^2$ irradiation of AM 1.5 sunlight. A DSSC fabricated by using E7-embedded PVdF-co-HFP-based polymer electrolyte exhibited a maximum incident photon-to-current conversion efficiency (IPCE) of 50%.

Effect of Magnetic Field Annealing on Microstructure and Magnetic Properties of FeCuNbSiB Nanocrystalline Magnetic Core with High Inductance

  • Fan, Xingdu;Zhu, Fangliang;Wang, Qianqian;Jiang, Mufeng;Shen, Baolong
    • Applied Microscopy
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    • v.47 no.1
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    • pp.29-35
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    • 2017
  • Transverse magnetic field annealing (TFA) was carried out on $Fe_{73.5}Cu_1Nb_3Si_{15.5}B_7$ nano-crystalline magnetic core with the aim at decreasing coercivity ($H_c$) while keeping high inductance ($L_s$). The magnetic field generated by direct current (DC) was applied on the magnetic core during different selected annealing stages and it was proved that the nanocrystalline magnetic core achieved lowest $H_c$ when applying transverse field during the whole annealing process (TFA1). Although the microstructure and crystallization degree of the nanocrystalline magnetic core exhibited no obvious difference after TFA1 compared to no field annealing, the TFA1 sample showed a more uniform nanostructure with a smaller mean square deviation of grain size distribution. $H_c$ of the nanocrystalline magnetic core annealed under TFA1 decreased along with the increasing magnetic field. As a result, the certain size nanocrystalline magnetic core with low $H_c$ of 0.6 A/m, low core loss (W at 20 kHz) of 1.6 W/kg under flux density of 0.2 T and high $L_s$ of $13.8{\mu}H$ were obtained after TFA1 with the DC intensity of 140 A. The combination of high $L_s$ with excellent magnetic properties promised this nanocrystalline alloy an outstanding economical application in high frequency transformers.