• Proceedings of the KWS Conference
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• 1996.10a
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• pp.176-179
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• 1996

• Corrosion Science and Technology
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• v.6 no.5
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• pp.251-256
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• 2007

Plasma nitriding is a surface treatment process which is increasingly used to improve wear, fatigue and corrosion resistance of industrial parts. Active screen plasma nitriding (ASPN) has both the advantages of the classic cold wall and the hot wall conventional dc plasma nitriding (DCPN) method and the parts to be nitrided are no longer directly exposed to the plasma. In this study, AS plasma nitriding has been used to nitride the UNS S31803 duplex stainless steel, AISI 304 and AISI 316 austenitic stainless steel, and AISI 420 martensitic stainless steel. Treated specimenswere characterized by means of microstructural analysis, microhardness measurements and electrochemical tests in NaCl aerated solutions. Hardness of the nitride cases of AISI 420 stainless steel by Knoop test can get up to 1300 HK0.1. From polarization tests, the corrosion current densities of AISI 420 and UNS S31803specimens ASPN at $420^{\circ}C$ were generally lower than those of their untreated substrates. The corrosion resistance of UNS S31803 duplex stainless steel can be enhanced by plasma nitriding at $420^{\circ}C$ Cowing to the formation of the S-phase.

• Journal of the Korean Society for Heat Treatment
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• v.24 no.6
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• pp.327-337
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• 2011

Effects of microstructural change, tensile properties and impact property according to the change of austenitizing temperature and tempering temperature of AISI 51B20 steel were examined. Regardless of austenite grain size, lath martensite with needle and packet shapes was found at tempering temperature of $300^{\circ}C{\sim}400^{\circ}C$. The needles of lath martensite changed to parallel packet at tempering temperature of $450^{\circ}C{\sim}600^{\circ}C$. As tempering temperature increased, tensile strength, yield strength and hardness decreased, while elongation, ratio of reduction area and Charpy impact energy increased. Grain size increased when quenching temperature was $930^{\circ}C$. Grain size had prominent effect on the mechanical properties of AISI 51B20 steel. Ratio of tensile strength/yield strength and yield strength autenitized at $880^{\circ}C$ followed by tempering at $350^{\circ}C{\sim}450^{\circ}C$ showed higher values than that of autenization at $930^{\circ}C$ due to fine grain size.

• Korean Journal of Metals and Materials
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• v.49 no.7
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• pp.515-521
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• 2011

Small punch creep testing has received attention due to the convenience of using smaller specimens than those of conventional uniaxial creep tests, which enables creep testing on developing or currently operational components. However, precedent studies have shown that it is necessary to consider friction between the punch and specimen when computing uniaxial equivalent stress from a finite element model. In this study, small punch creep behaviors of AISI 316L stainless steel, which is widely used in high temperature-high pressure machineries, have been compared for the two different ceramic balls such as $Si_3N_4$ and $Al_2O_3$. The optimal range of the friction coefficient is 0.4~0.5 at $650^{\circ}C$ for the best fit between experimental and simulation data of AISI 316 L stainless steel. The higher the friction coefficient, the longer the creep rupture time is. Therefore, the type of ceramic ball used must be specified for standardization of small punch creep testing.

• Korean Journal of Materials Research
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• v.33 no.7
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• pp.309-314
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• 2023

This study aimed to address the limitations of traditional plasma nitriding methods by implementing a short-term plasma oxy-nitriding treatment on the surface of AISI 420 martensitic stainless steel. This treatment involved the sequential formation of nitride and oxide layers, to enhance surface hardness and corrosion resistance, respectively. The process resulted in the formation of a 20 ㎛-thick nitride layer and a 3 ㎛-thick oxide layer on the steel surface. Initially, the hardness increased by 2.2 times after nitriding, followed by a subsequent decrease of approximately 31 % after oxidation. While the nitriding process reduced corrosion resistance, the subsequent oxidation process led to the formation of a passive oxide film, effectively resolving this issue. The pitting corrosion of the oxide passive film started at 82.6 mVssc, providing better corrosion resistance characteristics than the nitride layer. Consequently, the trade-off between surface hardness and corrosion resistance in plasma oxy-nitrided AISI 420 martensitic stainless steel is anticipated to be recognized as an innovative and comprehensive surface treatment process for biomedical components.

• Tribology and Lubricants
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• v.39 no.5
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• pp.212-215
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• 2023

Diaphragm compressors play a crucial role in safely compressing large volumes of high-purity hydrogen gas without contamination or leakage, thereby ensuring quality and reliability. Diaphragm compressors use a thin, flat, triple-layered diaphragm plate that is subjected to repetitive piston pressure for compression. They are usually made of metallic materials such as stainless steel or Inconel owing to their high-pressure resistance. However, since they are consumable components, they fail due to fatigue from repetitive pressure and vibration stress. This study aims to evaluate the scratch characteristics of diaphragms in operational environments by conducting tests on three different samples: Inconel 718, AISI 301, and Teflon-coated AISI 301. The Inconel 718 sample underwent a polishing process, the AISI 301 sample used raw material, and the Teflon coating was applied to the AISI 301 substrate at a thickness of 50 ㎛. To assess the scratch resistance, reciprocating motion friction tests were performed using a tribometer, utilizing 220 and 2000 grit sandpapers as the counter materials. The results of the friction tests suggested that the Teflon-coated sample exhibited the lowest initial friction coefficient and consistently maintained the lowest average friction coefficient (0.13 and 0.11 with 220 and 2000 grit, respectively) throughout the test. Moreover, the Teflon-coated diaphragm showed minimal wear patterns, indicating superior scratch resistance than the Inconel 718 and AISI 301 samples. These findings suggest that Teflon coatings may offer an effective solution for enhancing scratch resistance in diaphragms, thereby improving compressor performance in high-pressure hydrogen applications.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.05a
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• pp.145-146
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• 2009

크롬 도금된 AISI 316L 스테인리스강에 펄스 바이어스를 사용한 유도결합 플라즈마로 질화 처리하여 고분자 전해질 연료전지용 분리판에 적합한 물성을 확인하였다.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2009.05a
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• pp.147-148
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• 2009

스테인리스강인 AISI 316L의 질화처리를 통하여 고분자 전해질 연료전지에 분리판에 적용가능한 특성을 측정하였다. 질화처리를 통하여 면간접촉저항을 $20m{\Omega}cm^2$ 정도로 낮게 만들었으며 부식특성도 원래의 스테인리스강과 비슷한 값을 나타내었다.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.20 no.4
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• pp.419-426
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• 2011

In this study, an experimental and theoretical program were carried out to determine the cutting forces and chip formation at different cutting speeds using a 0.4mm nose radius ceramic insert and -7 rake angle for non heat-treated AISI 4140 (27HRc) and heat-treated AISI 4140 (45 HRc) steel. The results obtained were compared to show the hardness differences between the materials. The secondary deformation zone thicknesses when comparing the two materials show different physical structure but similar size. These results were also discussed in light of the heat treatment and the effects it had on the machining characteristics of the material. In addition, the Oxley Machining Theory was used to predict the cutting forces for these materials and a comparison made. The predicted cutting performances were verified experimentally and showed good agreement with experimental data.

• Journal of the Korean institute of surface engineering
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• v.28 no.1
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• pp.23-33
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• 1995

AISI 304 stainless steel has high resistance to corrosion due to the presence of a self-healing chromium oxide film on the surface, which also accounts for the difficulty in plating. Surface cleaning of this alloy is of fundamental importance in gold plating since its effectiveness puts an upper limit on the quality of the final coating. The cleaning of AISI 304 stainless steel was investigated with elimination of artificial passive oxide film and degreasing of remaining buffing wax as stearic acid. The familiar cleaning methods i.e. ultrasonic cleaning, electro-cleaning and activation treatment were fabricated in this study. Activation treatment showed best cleaning efficiency for elimination of passive oxide film among these methods, which was also confirmed by AES (Auger electron spectrometer) analysis. However, the best condition of cleaning was obtained by combining these methods. Electrocleaning time, for degreasing the stearic acid layer, was decreased with increasing amount of added KCN.