• Journal of the Korean Society for Heat Treatment
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• v.9 no.1
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• pp.69-77
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• 1996

The fatigue crack initiation behavior of plasma ion nitrided SACM645 steel was investigated through the rotary bending fatigue test and residual stress measurement by XRD. It was shown by XRD and EPMA that the plasma ion nitrided surface was composed of ${\gamma}^{\prime}(Fe_4N)$phase and ${\varepsilon}(Fe_{2-3}N)$phase, and that the nitrogen atoms existed in Fe matrix in diffusion layer. The OM, SEM and Auger spectroscopy showed that the depth of compound layer, mixed compound and diffusion layer, and diffusion layer was $8{\mu}m$, $30{\mu}m$ and $300{\mu}m$, respectively. However, the microhardness test showed that the depth of hardened layer was $500{\mu}m$. The tensile strength of the ion nitrided SACM645 was lower than that of the unnitrided SACM645, and the ion nitrided specimen was fractured without plastic deformation. The nitrided SACM645 showed much poorer low cycle fatigue properties than the unnitrided one. In rotary bending fatigue, the fatigue strength of the ion nitrided SACM645 was higher than that of the unnitrided specimen, and the fatigue crack initiation sites changed by applied fatigue stress levels. The XRD result showed that the ion nitrided SACM645 has the compressive residual stress from surface to $600{\mu}m$ deep and the tensile residual stress from $600{\mu}m$ to deeper site. It is thought that crack initiation takes place at the point where the total stress of residual stress and applied stress is maximum.

• The Journal of Korean Academy of Prosthodontics
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• v.42 no.2
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• pp.142-153
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• 2004

Statement of problem: Increasing demand of esthetic restorations made lots of kinds of ceramic materials. Among them, zirconia has been being focused by many dentists. But, mechanical properties of zirconia were still unclear. Purpose : The purposes of this study were to analyze the flexural strength of various zirconia ceramics which had been currently used for clinic i.e., In-Ceram Zirconia(Vita Zahnfabrik, Bad $S\"{a}ckingen$, Germany), Celay Zirconia(Vita Zahnfabrik, Bad $S\"{a}ckingen$, Germany) and CAD/CAM Zirconia (Adens Zi-Ceram. Seoul , Korea). Material and methods: The four point bending test(ASTM Cl161) was used to measure the flexural strength of a specimen before and after circular heat treatment and fatigue loading. Results : 1. The average value of flexural strengths of CAD/CAM Zirconia, Celay Zirconia, In-Ceram Zirconia in dry condition were 806.5 MPa, 669.9 MPa, 605.6 MPa, respectively. There was a statistically significant difference in strength among the types (P<0.05). 2. After thermocycling, the average flexural strengths of CAD/CAM Zirconia, Celay Zirconia, In-Ceram Zirconia were 791.2 MPa, 604.2 MPa, 605.4 MPa, respectively. CAD/CAM Zirconia showed statistically significant higher strength(P<0.05). The others showed no significant difference after thermocycling(P>0.05). 3. After fatigue loading in wet condition. the average flexural strengths of CAD/CAM Zirconia, Celay Zirconia, In-Ceram Zirconia were 806.0 MPa, 674.9 MPa, 601.7 MPa, respectively. There was a significant difference in strength among the types(P<0.05). 4. There was no statistically significant difference in strength of the specimens according to experimental methods except for before and after thermocycling in Celay Zirconia(P>0.05). Conclusion: Besides high esthetic quality, zirconia had sufficiently high mechanical strength.

• Journal of Technologic Dentistry
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• v.31 no.4
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• pp.37-43
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• 2009

This study evaluated the effect of concentration of glass fiber reinforcement on the flexural properties of auto and heat polymerized denture base resin. The test specimens($64{\times}10{\times}3.3mm$) were made of auto and heat polymerized resin(Vertex, Dentimax, Netherlands). Glass fiber(ER 270FW, Hankuk Fiber Glass, Korea) were used to reinforce the denture base resin. The 2.6%, 5.3% and 7.9% volume pre-impregnated fiber were located at the bottom of specimen. The test specimens(n=7) of each group were stored in distilled water at $37^{\circ}C$ for 50 hours before test. The flexural strength and modulus were measured by an universal testing machine(Z020, Zwick, Germany) at a crosshead speed of 5 mm/min in a three-point bending mode. The data was analyzed by one-way ANOVA and the Duncan's multiple range test(${\alpha}$=0.05). The difference of auto polymerized resin groups and heat polymerized resin groups were statistically analyzed by t-test(${\alpha}$=0.05). Glass fiber showed significant reinforcing effects on auto and heat polymerized resin. For flexural strength and modulus, auto polymerized resin was the highest in 7.9% volume, while heat polymerized resin was the highest in 5.3% volume. In this study, glass fiber at 7.9% volume ratio showed most effective reinforcing effect on auto polymerized resin and glass fiber at 5.3% volume ratio showed most effective reinforcing effect on heat polymerized resin in terms of flexural strength and flexural modulus.

• Polymer(Korea)
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• v.25 no.3
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• pp.435-440
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• 2001

The objective of this study was to examine the effect of oxidation inhibitor contents on the work of adhesion, fracture toughness, and impact strength of the unidirectional carbon-carbon composites (C/C composites). The molybdenum disilicide ($MoSi_2$) used as an oxidation inhibitor was impregnated with phenolic resins to improve the anti-oxidation properties of the composites in different concentrations of 4, 12 and 20 wt%. Based on Wilhelmy equation, the work of adhesion of C/C composites was calculated by contact angle methods. Fracture toughness and impact strength were pressured by three-point bending test for the critical intensity factor ($K_IC$) and Izod test method, respectively. As a result, the composites made with $MoSi_2$ resulted in an increasing of both fracture toughness and impact strength. Especially, the composites made with 12 wt% $MoSi_2$ content showed the highest value of London dispersive component, $W_A\;^L$, in work of adhesion, resulting from improving the interfacial adhesion force among fibers, filler, and matrix in this system.

• Textile Coloration and Finishing
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• v.28 no.4
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• pp.246-252
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• 2016

In comparison to metal alloys, braided composite features a high impact resistance and crash energy absorption potential, and also it still remained competitive stiffness and strength properties. Braiding angle is one of the most important parameters which affect the mechanical behaviors of braided composite. This paper presents transverse low velocity impact failure behavior analysis on the carbon 3D triaxial braided composite tube with the braiding angle of $20^{\circ}$, $50^{\circ}$ and $80^{\circ}$. The flexural behaviour of 3D triaxial braided composite tube under bending loads was studied by conducting quasistatic three point bending test. Also, the low velocity impact responses of the braided composite tubes were also tested to obtain load-displacement curves and energy absorption. Consequently, the increase of the braided angle, the peak load also increases owing to the bigger bending stiffness.

• Ocean Systems Engineering
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• v.11 no.4
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• pp.313-330
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• 2021

In this study, the dynamic interaction between an Arctic Spar and drifting level ice is examined in time domain using the newly developed ice-hull-mooring coupled dynamics program. The in-house program, CHARM3D, which is the hull-riser-mooring coupled dynamic simulator is extended by coupling with the open-source discrete element method (DEM) simulator, LIGGGHTS. In the LIGGGHTS module, the parallel-bonding method is implemented to model the level ice using an assembly of multiple bonded spherical particles. As a case study, a spread-moored Artic Spar platform, whose hull surface near waterline is the inverted conical shape, is chosen. To determine the breaking-related DEM parameter (the critical bonding strength), the four-point numerical bending test is used. A series of numerical simulations is systematically performed under the various ice conditions including ice drift velocity, flexural strength, and thickness. Then, the effects of these parameters on the ice force, platform motions, and mooring tensions are discussed. The simulations reveal various features of dynamic interactions between the drifting ice and moored platform for various ice conditions including the novel synchronous resonance at low ice speed. The newly developed simulator is promising and can repeatedly be used for the future design and analysis including ice-floater-mooring coupled dynamics.

• Structural Engineering and Mechanics
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• v.89 no.4
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• pp.349-362
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• 2024

High-performance fiber-reinforced cement composites (HPFRCC) are new materials created and used to repair, strengthen, and improve the performance of different structural parts. When exposed to tensile tension, these materials show acceptable strain-hardening. All of the countries of the globe currently seem to have a need for these building materials. This study aims to create a low-carbon HPFRCC (high ductility) that is made from materials that are readily available locally which has the right mechanical qualities, especially an increase in tensile strain capacity and environmental compatibility. In order to do this, the effects of fiber volume percent (0%, 0.5%, 1%, and 2%), and determining the appropriate level, filler type (limestone powder and silica sand), cement type (ordinary Portland cement, and limestone calcined clay cement or LC3), matrix hardness, and fiber type (ordinary and oxygen plasma treated polypropylene fiber) were explored. Fibers were subjected to oxygen plasma treatment at several powers and periods (50 W and 200 W, 30, 120, and 300 seconds). The influence of the above listed factors on the samples' three-point bending and direct tensile strength test results has been examined. The results showed that replacing ordinary Portland cement (OPC) with limestone calcined clay cement (LC3) in mixtures reduces the compressive strength, and increases the tensile strain capacity of the samples. Furthermore, using oxygen plasma treatment method (power 200 W and time 300 seconds) enhances the bonding of fibers with the matrix surface; thus, the tensile strain capacity of samples increased on average up to 70%.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.15 no.9
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• pp.5844-5853
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• 2014

This paper presents the results of experimental investigations on the shear failure behaviors of reinforced concrete beams using ductile fiber reinforced cementitious composite (DFRCC). Total 10 RC beams of $150{\times}300{\times}1,000mm$ size were tested by 4-point bending under the displacement control. The main parameters of the experiment are surface treatment by grinding and preloading to the cracking point in the repair process. The load-displacement curves, diagonal tension cracking load, flexural cracking load, and shear strength were obtained. The test results showed that the DFRCC can be used effectively for restoring the shear strength approximately 99% to the original value under the condition that the appropriate thickness and surface treatment like grinding are assured. For further research, the specimens taken from real deteriorated structures will need to be tested after being repaired with DFRCC.

• Restorative Dentistry and Endodontics
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• v.46 no.3
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• pp.39.1-39.12
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• 2021

Objectives: This study analyzed the physical-chemical behavior of 2 bulk fill resin composites (BFCs; Filtek Bulk Fill [FBF], and Tetric-N-Ceram Bulk Fill [TBF]) used in 2- and 4-mm increments and compared them with a conventional resin composite (Filtek Z250). Materials and Methods: Flexural strength and elastic modulus were evaluated by using a 3-point bending test. Knoop hardness was measured at depth areas 0-1, 1-2, 2-3, and 3-4 mm. The translucency parameter was measured using an optical spectrophotometer. Real-time polymerization kinetics was analyzed using Fourier transform infrared spectroscopy. Results: Flexural strength was similar among the materials, while TBF showed lower elastic modulus (Z250: 6.6 ± 1.3, FBF: 6.4 ± 0.9, TBF: 4.3 ± 1.3). The hardness of Z250 was similar only between 0-1 mm and 1-2 mm. Both BFCs had similar hardness until 2-3 mm, and showed significant decreases at 3-4 mm (FBF: 33.45 ± 1.95 at 0-1 mm to 23.19 ± 4.32 at 3-4 mm, TBF: 23.17 ± 2.51 at 0-1 mm to 15.11 ± 1.94 at 3-4 mm). The BFCs showed higher translucency than Z250. The polymerization kinetics of all the materials were similar at 2-mm increments. At 4-mm, only TBF had a similar degree of conversion compared with 2 mm. Conclusions: The BFCs tested had similar performance compared to the conventional composite when used in up to 2-mm increments. When the increment was thicker, the BFCs were properly polymerized only up to 3 mm.

• Journal of Ocean Engineering and Technology
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• v.25 no.4
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• pp.66-71
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• 2011

The flexural strength of $MoSi_2$ based composites reinforced with Nb sheets has been investigated, based on the detailed examination of their microstructure and fractured surface. Both sintered density and porosity of Nb/$MoSi_2$ composites were also examined. Nb/$MoSi_2$ composites were fabricated by different conditions such as temperature, applied pressure and its holding time, using a hot-press device. The volume fraction of Nb sheet in this composite system was fixed as 10%. The characterization of Nb/$MoSi_2$ composites were investigated by means of optical microscopy, scanning electron microscope and three point bending test. Nb/$MoSi_2$ composites represented a dense morphology at the interfacial region, accompanying the creation of two types of reaction layer by the chemical reaction of Nb and $MoSi_2$. Nb/$MoSi_2$ composites possessed an excellent density at the fabricating temperature of $1350^{\circ}C$, corresponded to about 95% of theoretical density. The flexural strength of Nb/$MoSi_2$ romposites were greatly affected by the pressure holding time at the same fabricating temperature, owing to the large suppression of porosity in the microstructure. Especially, Nb/$MoSi_2$ composites represented a good flexural strength of about 310 MPa at the fabricating condition of $1350^{\circ}C$, 30MPa and 60min, accompanying the pseudo-ductile fracture behavior by the deformation of Nb sheet and the interfacial delamination.