• Journal of Ocean Engineering and Technology
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• v.25 no.4
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• pp.66-71
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• 2011

The flexural strength of $MoSi_2$ based composites reinforced with Nb sheets has been investigated, based on the detailed examination of their microstructure and fractured surface. Both sintered density and porosity of Nb/$MoSi_2$ composites were also examined. Nb/$MoSi_2$ composites were fabricated by different conditions such as temperature, applied pressure and its holding time, using a hot-press device. The volume fraction of Nb sheet in this composite system was fixed as 10%. The characterization of Nb/$MoSi_2$ composites were investigated by means of optical microscopy, scanning electron microscope and three point bending test. Nb/$MoSi_2$ composites represented a dense morphology at the interfacial region, accompanying the creation of two types of reaction layer by the chemical reaction of Nb and $MoSi_2$. Nb/$MoSi_2$ composites possessed an excellent density at the fabricating temperature of $1350^{\circ}C$, corresponded to about 95% of theoretical density. The flexural strength of Nb/$MoSi_2$ romposites were greatly affected by the pressure holding time at the same fabricating temperature, owing to the large suppression of porosity in the microstructure. Especially, Nb/$MoSi_2$ composites represented a good flexural strength of about 310 MPa at the fabricating condition of $1350^{\circ}C$, 30MPa and 60min, accompanying the pseudo-ductile fracture behavior by the deformation of Nb sheet and the interfacial delamination.

• The Journal of Advanced Prosthodontics
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• v.6 no.4
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• pp.266-271
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• 2014

PURPOSE. The purpose of this study was to compare the fracture strength of the metal and the bond strength in metal-ceramic restorations produced by selective laser sintering (SLS) and by conventional casting (CAST). MATERIALS AND METHODS. Non-precious alloy (StarLoy C, DeguDent, Hanau, Germany) was used in CAST group and metal powder (SP2, EOS GmbH, Munich, Germany) in SLS group. Metal specimens in the form of sheets ($25.0{\times}3.0{\times}0.5mm$) were produced in accordance with ISO 9693:1999 standards (n=30). To measure the bond strength, ceramic was fired on a metal specimen and then three-point bending test was performed. In addition, the metal fracture strength was measured by continuing the application of the load. The values were statistically analyzed by performing independent t-tests (${\alpha}=.05$). RESULTS. The mean bond strength of the SLS group (50.60 MPa) was higher than that of the CAST group (46.29 MPa), but there was no statistically significant difference. The metal fracture strength of the SLS group (1087.2 MPa) was lower than that of the CAST group (2399.1 MPa), and this difference was statistically significant. CONCLUSION. In conclusion the balling phenomenon and the gap formation of the SLS process may increase the metal-ceramic bond strength.

• The Journal of Korean Academy of Prosthodontics
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• v.34 no.4
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• pp.823-832
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• 1996

The purpose of this study was to assess the effect of 1) the diameter(0.7,1.0,1.2mm) and number(1,2,3) of commonly available orthodontic metal wires embedded in self-curing orthodontic acrylic resin specimens($64{\times}10{\times}3mm$) and 2) the use of chemical adhesive system(Silicoater, Metalprimer) to prevent slipping at the interface between the resin and the metal wire on reinforcement by using three-point bending test. From this study, the following results were obtained. 1. No statistically significant difference was found among the transverse strengths for the control without reinforcement, one 0.7mm wire, two 0.7mm wires, three 0.7mm wires, and one 1.0mm wire groups(P>.05). 2. In the groups with 1.0 or 1.2mm wires, the transverse strength increased in proportion to the increase of number of wires(P<.05). 3. In the groups with 0.7 or 1.0mm wires, neither of Silicoater and Netalprimer increased the transverse strength significantly(P>.05). 4. No statistically significant difference was found in transverse strength between Silicoater groups and Metalprimer groups with same diameter of wires(P.>05). From these result, it is concluded that diameter of wires is a primary considering factor to reinforce the acrylic resin effectively and, when this requirement is satisfied, increased number of wires or chemical adhesive systems can be expected to produce the additional reinforcing effect.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.16 no.11
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• pp.7244-7249
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• 2015

In this study, in order to asses the structural performance of trapezoidal PSC girder using a socket joint system and it is possible to calculate the optimized cross-section of the web element tests were carried out for each specimens. we conducted a socket joint performance test, web bending and shear performance tests and all tests were performed at 4 point loading method. The initial crack load of socket joint specimen was significantly lower than the reference specimen but post peak behavior was no significant differences. And the length of the loop joint of the reinforcing bars had no significant effect on the maximum load. As a web shear tests, to obtain a maximum load of the specimen has a prestressing rod reinforced at tension side. As a web flexural tests, to obtain higher diagonal cracking load in specimen of reinforced using prestressing rod than reference specimen.

• Steel and Composite Structures
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• v.29 no.4
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• pp.527-544
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• 2018

The paper presents the study on a change in modal parameters and structural stiffness of cable-stayed Fiberline Bridge made entirely of Glass Fiber Reinforced Polymer (GFRP) composite used for 20 years in the fjord area of Kolding, Denmark. Due to this specific location the bridge structure was subjected to natural aging in harsh environmental conditions. The flexural properties of the pultruded GFRP profiles acquired from the analyzed footbridge in 1997 and 2012 were determined through three-point bending tests. It was found that the Young's modulus increased by approximately 9%. Moreover, the influence of the temperature on the storage and loss modulus of GFRP material acquired from the Fiberline Bridge was studied by the dynamic mechanical analysis. The good thermal stability in potential real temperatures was found. The natural vibration frequencies and mode shapes of the bridge for its original state were evaluated through the application of the Finite Element (FE) method. The initial FE model was created using the real geometrical and material data obtained from both the design data and flexural test results performed in 1997 for the intact composite GFRP material. Full scale experimental investigations of the free-decay response under human jumping for the experimental state were carried out applying accelerometers. Seven natural frequencies, corresponding mode shapes and damping ratios were identified. The numerical and experimental results were compared. Based on the difference in the fundamental natural frequency it was again confirmed that the structural stiffness of the bridge increased by about 9% after 20 years of service life. Data collected from this study were used to validate the assumed FE model. It can be concluded that the updated FE model accurately reproduces the dynamic behavior of the bridge and can be used as a proper baseline model for the long-term monitoring to evaluate the overall structural response under service loads. The obtained results provided a relevant data for the structural health monitoring of all-GFRP bridge.

• Structural Engineering and Mechanics
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• v.76 no.4
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• pp.465-477
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• 2020

This paper presents an investigation on the dynamic behavior of SRC columns with built-in cross-shaped steels under impact load. Seven 1/2 scaled SRC specimens were subjected to low-speed impact by a gravity drop hammer test system. Three main parameters, including the lateral impact height, the axial compression ratios and the stirrup spacing, were considered in the response analysis of the specimens. The failure mode, deformation, the absorbed energy of columns, as well as impact loads are discussed. The results are mainly characterized by bending-shear failure, meanwhile specimens can maintain an acceptable integrity. More than 33% of the input impact energy is dissipated, which demonstrates its excellent impact resistance. As the impact height increases, the flexural cracks and shear cracks observed on the surface of specimens were denser and wider. The recorded time-history of impact force and mid-span displacement confirmed the three stages of relative movement between the hammer and the column. Additionally, the displacements had a notable delay compared to the rapid changes observed in the measured impact load. The deflection of the mid-span did not exceed 5.90mm while the impact load reached peak value. The impact resistance of the specimen can be improved by proper design for stirrup ratios and increasing the axial load. However, the cracking and spalling of the concrete cover at the impact point was obvious with the increasing in stiffness.

• Journal of the Korea institute for structural maintenance and inspection
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• v.28 no.1
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• pp.90-97
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• 2024

In this study, we employed Highly Ductile Cement Composite (HDCC) to evaluate the flexural performance of a RC slab that simulates the laminating structure of a seashell. To evaluate flexural performance, we produced conventional RC slab specimens, HDCC slab specimens, and HDCC-M slab specimens which biomimics a seashell's layered structure by inserting PE mesh inside the slab made of HDCC. A series of 4-point bending tests were conducted. Experimental results shows the flexural strength of the HDCC-M slab specimen was 1.7 times and 1.2 times higher than that of the RC and HDCC slab specimens, respectively. Furthermore, the ductility was evaluated using the ratio of yield deflection to maximum deflection, and it was confirmed that the HDCC slab test specimen exhibited the best ductility. This is most likely due to the fact that the inserted PE mesh separates the layers and increases ductility, while the HDCC passing through the mesh prevents the loss of load carrying capacity due to layer separation.

• Korean Chemical Engineering Research
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• v.45 no.5
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• pp.466-472
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• 2007

A technology platform for wafer-level three-dimensional integration circuits (3D-ICs) is presented, and that uses wafer bonding with low-k polymeric adhesives and Cu damascene inter-wafer interconnects. In this work, one of such technical platforms is explained and characterized using a test vehicle of inter-wafer 3D via-chain structures. Electrical and mechanical characterizations of the structure are performed using continuously connected 3D via-chains. Evaluation results of the wafer bonding, which is a necessary process for stacking the wafers and uses low-k dielectrics as polymeric adhesive, are also presented through the wafer bonding between a glass wafer and a silicon wafer. After wafer bonding, three evaluations are conducted; (1) the fraction of bonded area is measured through the optical inspection, (2) the qualitative bond strength test to inspect the separation of the bonded wafers is taken by a razor blade, and (3) the quantitative bond strength is measured by a four point bending. To date, benzocyclobutene (BCB), $Flare^{TM}$, methylsilsesquioxane (MSSQ) and parylene-N were considered as bonding adhesives. Of the candidates, BCB and $Flare^{TM}$ were determined as adhesives after screening tests. By comparing BCB and $Flare^{TM}$, it was deduced that BCB is better as a baseline adhesive. It was because although wafer pairs bonded using $Flare^{TM}$ has a higher bond strength than those using BCB, wafer pairs bonded using BCB is still higher than that at the interface between Cu and porous low-k interlevel dielectrics (ILD), indicating almost 100% of bonded area routinely.

• The Journal of Korean Academy of Prosthodontics
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• v.47 no.2
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• pp.191-198
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• 2009

Statement of problem: Ceramics have been important materials for the restoration of teeth. The demands of patients for tooth-colored restorations and the availability of various dental ceramics has driven the increased use of new types of dental ceramic materials. Improved physical properties of theses materials have expanded its use even in posterior crowns and fixed partial dentures. However, ceramic still has limitation such as low loading capability. This is critical for long-span bridge, because bridge is more subject to tensile force. Purpose: The wire reinforced ceramic was designed to increase the fracture resistance of ceramic restoration. The purpose of this study was to evaluate the fracture resistance of wire reinforced ceramic. Material and methods: Heat pressed ceramic(ingot No.200 : IPS Empress 2, Ivoclar Vivadent, Liechtenstein) and Ni-Cr wire(Alfa Aesar, Johnson Matthey Company, USA) of 0.41 mm diameter were used in this study. Five groups of twelve uniform sized ceramic specimens(width 4 mm, thickness 2 mm, length 15 mm) were fabricated. Each group had different wire arrangement. Wireless ceramic was used as control group. The experimental groups were divided according to wire number and position. One, two and three strands of wires were positioned on the longitudinal axis of specimen. In another experimental group, three strands of wires positioned on the longitudinal axis and five strands of wires positioned on the transverse axis. Three-point bending test was done with universal testing machine(Z020, Zwick, Germany) to compare the flexural modulus, flexural strength, strain at fracture and fracture toughness of each group. Fractured ceramic specimens were cross-sectioned with caborundum disc and grinded with sandpaper to observe interface between ceramic and Ni-Cr wire. The interface between ceramic and Ni-Cr wire was analyzed with scanning electron microscope(JSM-6360, JEOL, Japan) under platinum coating. Results: The results obtained were as follows: 1. The average and standard deviation in flexural modulus, flexural strength and fracture toughness showed no statistical differences between control and experimental groups. However, strain was significantly increased in wire inserted ceramics(P<.001). 2. Control group showed wedge fracture aspects across specimen, while experimental groups showed cracks across specimen. 3. Scanning electron microscopic image of cross-sectioned and longitudinally-sectioned specimens showed no gap at the interface between ceramic and Ni-Cr wire. Conclusion: The results of this study showed that wire inserted ceramics have a high strain characteristic. However, wire inserted ceramics was not enough to use at posterior area of mouth in relation to flexural modulus and flexural strength. Therefore, we need further studies.

• Journal of the Korea Concrete Institute
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• v.22 no.2
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• pp.199-208
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• 2010

In order to substitute FRP bar for steel bar in new structures, it is necessary to establish a reliable design code. But relatively little research has been conducted on the material in Korea. So, a total of 22 beam specimens (18 GFRP reinforced concrete and 4 conventional steel reinforced concrete) were constructed and tested. In the first phase of the experiment, it was carried out to observe flexural behavior, and collect deflection and crack data. In order to eliminate of the uncertainty by the shear reinforcements and induce flexural failure mode, any stirrup were not used and only shear span-depth ratio were adjusted. However, almost beams were broken by shear and the ACI 440.1R, CSA S806, which were used to design test beams, showed considerable deviation between prediction and test results of shear strengths. Therefore in the second phase of the study, shear failure modes and behavior were observed. A standard specimen had dimensions of 3,300 mm long ${\times}$ 800 mm wide ${\times}$ 200 mm effective depth. Clear span and shear span were 2,800 mm, 1,200 mm respectively. Control shear span-depth ratio was 6.0. Four-point bending test over simple support was conducted. Variables of the specimens were concrete compressive strength, type and elastic modulus of reinforcement, shear span-depth ratio, effective reinforcement ratio, the effect of bundle placing method and cover thickness.