• 한국주조공학회지
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• 제15권6호
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• pp.604-615
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• 1995

Austenitic stainless steel castings using expandable polystylene(referred to hereafter as EPS) patterns are often affected by distinctive defects associated with incomplete decomposition of the EPS as the molds are filled with metal. The quality of the castings, with particular reference to carbon pick-up in austenitic stainless steel is further influenced to a significant extent by such factors as reduced pressure, the additive by adding $Na_2CO_3$ in coating. The steel composition and microstructure were examined at the surface layer of castings, at depths of 1mm, by taking successive layers of swarf and analysis. In experiments, the carburizing atmosphere was neutralized, showing that the coating performed efficiently by decomposing almost instantly on heating and liberating $CO_2$. The upper parts of castings obtained using EPS patterns were slightly higher in carbon pick-up than other parts. Comparing the 316L and 304 stainless steel castings, qualitative and quantative differences could be found between the carbon pick-up behaviours as influence of the carbon content and alloying elements. Carbide former such as Cr makes carbon more soluble in the steel. This must make carbon pick-up in the surface layer but at the same time richer in carbon especially in the 304 stainless steel castings.

• 한국표면공학회지
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• 제33권2호
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• pp.93-100
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• 2000

Effects of Ti content and Ti underlayer on the pitting behavior of TiN coated AISI 304 stainless steel have been studied. The stainless steel containing 0.1~1.0wt% Ti were melted with a vacuum melting furnace and heat treated at $1050^{\circ}C$ for 1hr for solutionization. The specimen were coated with l$\mu\textrm{m}$ and 2$\mu\textrm{m}$ thickness of Ti and TiN by E-beam PVD method. The microstructure and phase analysis were conducted by using XRD, XPS and SEM with these specimen. XRD patterns shows that in TiN single-layer only the TiN (111) Peak is major and the other peaks are very weak, but in Ti/TiN double-layer TiN (220) and TiN (200) peaks are developed. It is observed that the surface of coating is covered with titanium oxide (TiO$_2$) and titanium oxynitride ($TiO_2$N) as well as TiN. Corrosion potential on the anodic polarization curve measured in HCl solution increase in proportion to the Ti content of substrate and by a presence of the Ti underlayer, whereas corrosion and passivation current densities are not affected by either of them. The number and size of pits decrease with increasing Ti content and a presence of the coated Ti film as underlayer in the TiN coated stainless steel.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2007년도 춘계학술발표회 초록집
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• pp.118-119
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• 2007

오스테나이트계 스테인리스 AISI304L강을 저온 플라즈마 분위기에서 표면에 C와 N을 주입하면 내식성의 저하 없이 표면경도를 증가 시킬 수 있다. 이 공정에서 온도에 따른 영향을 조사하기위해 $380^{\circ}C{\sim}430^{\circ}C$의 온도 범위에서 20시간 동안 실시하였다. 경화층의 두께는 $7{\sim}16\;{\mu}m$정도였으며, N의 농도가 높은 영역과 C의 농도가 높은 영역으로 나뉘어 형성되었고, N이 풍부한 영역이 표면층에 형성되고 그 아래에 C의 농도 높은 영역이 형성되었다. 표면층은 질소에 의해 확장된 오스테나이트(${\gamma}_N$)상을 가지며 고온에서 처리한 경우 석출물이 형성되었다. 표면경도는 약 $900\;HV_{0.01}{\sim}1200\;HV_{0.01}$로 측정되었다.

• Journal of Welding and Joining
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• 제2권1호
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• pp.49-57
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• 1984

The influence of weld defect, residual stress and microstructure on the Low Cycle Fatigue(L. C. F.) behaviour of AISI 304L austenitic stainless steel weldment has been studied. The specimens were welded by shielded metal are welding process, post weld heat treated(PWHT) at 900.deg.C for 1.5hrs, and tested under total strain controlled condition at room temperature. The results of the experiment showed that weld defect affected the L.C.F. behaviour of weldment deleteriously compared to the residual stress or microstructure, and it reduced the L.C.F. life about 70-80%. The PWHT exhibited beneficial effect on the L.C.F. behaviour and increased the L.C.F. life about 120%. This enhancement by PWHT was attributed to the removal of residual stress and recovery of weld metal ductility. The cyclic stress flow of as welded specimens showed intermediate cyclic softening, whereas those of heat treated specimens showed continuous cyclic hardening, and this difference was explained in terms of the residual stress removal and dislocation behaviour. Scanning electron microscopy studies of fatigue fracture surface showed that weld defects of large size and near weld surface were detrimental to the L.C.F. behaviour of weldment.

• Journal of Welding and Joining
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• 제25권5호
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• pp.64-71
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• 2007

The aim of this paper is to investigate the effects of welding parameters on the weld shape in seal-welding of STS304L capsule for manufacturing a radioisotope source which is widely used in nondestructive testing of metal structures using gamma ray. Pulsed gas tungsten arc (Pulsed GTA) welding is performed for thin cross sectional area of the capsule. Seven welding parameters including current waveform parameters and arc length etc. are selected as main process parameters using design of experiment. The weld shape such as bead width, penetration depth, weld area, aspect ratio and area rate is investigated to assess the effects of welding parameters. As results, the combination of pulse duty/welding speed largely affects on bead width, penetration depth, area and aspect ratio. Finally, it is concluded that the key parameters are the combination of pulse duty/welding speed, base current and arc length, and their optimal conditions are 50%/1.77mm/s, 6.4A and 1 mm.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2008년도 제35회 하계학술대회 초록집
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• pp.320-320
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• 2008

• Journal of Advanced Marine Engineering and Technology
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• 제36권8호
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• pp.1069-1075
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• 2012

레이저는 고밀도 열원으로써, 입열을 최소화하면서 고속용접이 가능한 장비이다. 특히 최근 상업화된 고출력 파이버 레이저는 특유의 발진원리 때문에 높은 빔품질과 소형화된 시스템이 가능하다. 이러한 장점들로 인해 파이버 레이저는 LNG 카고탱크에 대해 선박 내부에서 용접이 가능한 가장 적합한 열원이라고 판단된다. 따라서 본 연구에서는 선박산업에 레이저 용접기술을 적용하기 위해 파이버 레이저를 이용하여 LNG 선용 스테인리스강의 용접을 진행하였다. 연구에서 사용한 재료는 카고탱크에 사용되고 있는 오스테나이트계 스테인리스강인 두께 1.2mm의 STS304L였다. 레이저 출력 및 용접속도를 변화시켜가면서 겹치기 및 맞대기 용접을 실시한 후 용입특성을 분석하여 최적의 접합조건을 도출하였다. 그 결과 용접부에서 모재보다 우수한 기계적 성질을 얻을 수 있었다.

• Journal of Welding and Joining
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• 제5권2호
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• pp.35-43
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• 1987

The effect of post weld heat treatment (P.W.H.T) on the propagation rate of stress corrosion cracking(S.C.C) and threshold stress intensity factor ($K_{IC}.c.c$) for stress corrosion cracking of 304 stainless steel has been investigated in boiling 45% $MgCl_2$ solutions with W.O.L specimens. Specimens were precracked by turning a pair of Cr-Mo steel bolts into a machined slot at the end of the specimen. The fracture surface was examined fractographically by Scanning Electron Microscope(S.E.M.)

• 한국산학기술학회:학술대회논문집
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• 한국산학기술학회 2006년도 춘계학술발표논문집
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• pp.184-187
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• 2006

Nickel was plated electrolessly on 304L stainless steel powder. To obtain uniform coating and dispension of powder, the bath was continuously agitated with magnetic stirrer. The various pH and bath temperatures were studied. The conditions were in the range of $pH4{\sim}10$ and $45{\sim}65^{\circ}C$, respectively. The coating morphologies were examined by SEM/EDS tests. The optimum condition was pH9 at $55^{\circ}C$.

• Journal of Advanced Marine Engineering and Technology
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• 제13권2호
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• pp.43-63
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• 1989

Various kinds of corrosion prevention methods have been developed. It is known that the method of electrochemical protection is more effective and economical than any other method on the large scale metal structures in corrosive solutions. Strong acid solutions such as nitric and sulfuric acid solutions are often used in industries, and the expensive stainless steel is almost exclusively used for the equipment that comes in contact with such acid solutions. However, it is more reasonable that carbon steel is used rather than stainless steel depending upon concentration of those acid solutions from the economical viewpoint. In this study, the typical strong acid solution such as nitric and sulfuric acid solutions are chosen for the experiment and the selected materials of specimen are the stainless steels of SUS 304L and SUS 316L, the carbon steels of SS 41, SM 50 and RA 32, and highly pure lead. Electrochemical protection diagrams can be drawn with data from the external cathodic and anodic polarization curves of SUS 304L, SUS 316L and SM 50 steels in 5-60% nitric acid solutions and from those polarization curves of SS 41, RA 32, SM 50 and SUS 316L steels, and highly pure lead in 2.5-98% sulfuric acid solutions at the slow scanning rate. The data obtained with using the determination method of the optimum cathodic protection potential, the Tafel extrapolation method and the characteristics of anodic polarization curves. The main results obtained from the diagrams are as follows: 1) In nitric acid solution : (1) Corrosion potentials exist in each of those corrosion zones on the stainless steels in the lower concentration than about 12% solutions and on the high tensile strength steels in the lower concentration than about 30% solutions, but the corrosion current (density) in each zone is small on the above mentioned former steels and large on the latter ones. (2) The stainless steels can be self-passivated in the higher concentration than 15% solutions, and the high tensile strength steels gives rise to the same phenomenon in the higher concentration than 35% solutions. (3) The stainless steels in the lower concentration than 60% solutions and the high tensile strength steels in the higher concentration than 35% solutions can be used without protection, but the latter steels must ve protected anodically in the lower conccentration than about 30% solutions. 2) In sufuric acid solution : (1) The carbon steels can be self-passivated in the higher concentration than 45% solutions, and the SUS 316L steel in higher concentration than 75% solutions and the lead in all concentration solutions also gives rise to the same phenomenon. (2) The lead in the lower concentration than 80% solutions and the SUS 316L steel in the higher concentration than 80% solutions can be used without protection. (3) The carbon steels in the higher concentration than 50% solutions also can be used without protecting economically, but the SUS 316L steel in the 20-70% solutions are considerably corrosive without protecting anodically.