• Title/Summary/Keyword: 3-point flexural strength test

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Evaluation of Flexural Strength of 3D Printing Resin According to Post-Curing Equipment and Time (후경화기와 경화시간에 따른 3D 프린팅 레진의 굴곡강도 평가)

  • Hae-Bom Kim;Jae-Won Choi
    • Journal of the Korean Society of Industry Convergence
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    • v.26 no.4_2
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    • pp.629-637
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    • 2023
  • This study aimed to evaluate the effect of post-curing equipment and time on the flexural strength of 3D printing resins produced by a liquid crystal display(LCD) printer. The three 3D printing resins(DENTCA Denture Teeth, DT; C&B 5.0 hybrid, CH; C&B Permanent A2, CP) were divided into four groups according to post-curing time(10 min and 30 min) and equipment with or without vacuum treatment. For the three-point flexural strength test and biaxial strength test were prepared by method according to ISO 10477, ISO 6872, respectively. Flexural strength was measured with universal testing machine. Comparison between post-curing time of each post-curing equipment was analyzed by independent sample t-test and Mann-Whitney U test(α=.05), and comparison between groups according to each 3D printing resin was performed by Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(α=.05). The flexural strength of the resin post-curing under vacuum was higher than that of the resin post-curing in air. In the comparison according to the post-curing time, in the case of the post-curing equipment without vacuum, the 30 minute curing time showed significantly higher flexural strength than the 10 minute curing time, except for the biaxial flexural strength of CH(P<.05). In the post-curing equipment with vacuum, the three-point flexural strength of all 3D printing resins(DT, CH, and CP) showed a higher value at 30 minute curing time than at 10 minute curing time.

An Experimental Study on Strength Properties, Size Effect, and Fatigue Behaviour of Concrete under Biaxial Flexural Stress State (이방향 휨응력상태의 콘크리트 강도 특성, 크기효과 및 피로거동에 관한 실험적 연구)

  • Zi, Goangseup;Kim, Jihwan
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.33 no.3
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    • pp.901-907
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    • 2013
  • In this study, flexural strength properties of concrete under biaxial stress state were experimentally investigated. Tests for size effect and fatigue behaviour of concrete under biaxial stress were carried out by the ASTM C 1550 and the biaxial flexure test(BFT). The results given by the biaxial tests were compared to those by the third-point bending test. Test results showed that biaxial flexural strengths obtained from the ASTM C 1550 and the biaxial flexure test are greater than the strength by the third-point bending test. As the size increases, the uniaxial and biaxial flexural strength decreases. However, the slope of the size effect of the biaxial strength was greater than that of the uniaxial strength. Finally, the fatigue response of concrete under the biaxial stress state was similar with that for uniaxial stress state.

The effect of short and long duration sintering method on microstructure and flexural strength of zirconia (단시간과 장시간의 소결방법에 따른 지르코니아의 굴곡 강도와 미세구조의 변화)

  • Lee, Ha-Bin;Lee, Tae-Hee;Kim, Ji-Hwan
    • Journal of Technologic Dentistry
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    • v.42 no.2
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    • pp.73-79
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    • 2020
  • Purpose: The aim of this study was to investigate the influence of short and long duration sintering on microstructure and flexural strength of zirconia. Methods: To conduct three-point bending test, Zirconia specimens are milled according to ISO 6872 guidelines(N=18, n=9 per group). Two specimens group(n=8) is sintered for 10 hours(Standard schedule) and 3 hours(Speed schedule) at the peak temperature of 1550℃ with silicon carbide sintering furnace. Flexural strength of specimens are measured by instron. After coating each specimen(n=1), microstructure of specimens is observed using Scanning Electron Microscope(SEM). T-test was utilized to statistically assess the data. Results: The mean and standard deviation value of the flexural strength for standard schedule group are 578.15±57.48Mpa, that of speed schedule are 465.9±62.34Mpa. T-test showed significant differences in flexural strength between two zirconia specimen group which applied standard schedule and speed schedule respectively(p<0.05). Conclusion: The result of this study showed that the increase in sintering time led to increased grain size, and also to a positive effect on the flexural strength.

Flexural properties of a light-cure and a self-cure denture base materials compared to conventional alternatives

  • Mumcu, Emre;Cilingir, Altug;Gencel, Burc;Sulun, Tonguc
    • The Journal of Advanced Prosthodontics
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    • v.3 no.3
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    • pp.136-139
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    • 2011
  • PURPOSE. A new light curing urethane dimethacrylate and a cold curing resin with simpler and faster laboratory procedures may have even improved flexural properties. This study investigated the 3-point flexural strengths and flexural moduli of two alternate base materials. MATERIALS AND METHODS. A cold curing resin (Weropress) and a light curing urethane dimethacrylate base material (Eclipse). Along with Eclipse and Weropress, a high impact resin (Lucitone199) and three conventional base materials (QC 20, Meliodent and Paladent 20) were tested. A 3-point bending test was used to determine the flexural strengths and flexural moduli. The mean displacement, maximum load, flexural modulus and flexural strength values and standard deviations for each group were analyzed by means of one-way analysis of variance (ANOVA) (with mean difference significant at the 0.05 level). Post hoc analyses (Scheffe test) were carried out to determine the differences between the groups at a confidence level of 95%. RESULTS. Flexural strength, displacement and force maximum load values of Eclipse were significantly different from other base materials. Displacement values of QC 20 were significantly different from Lucitone 199 and Weropress. CONCLUSION. The flexural properties and simpler processing technique of Eclipse system presents an advantageous alternative to conventional base resins and Weropress offers another simple laboratory technique.

Flexural and shear behavior of large diameter PHC pile reinforced by rebar and infilled concrete

  • Bang, Jin-Wook;Lee, Bang-Yeon;Kim, Yun-Yong
    • Computers and Concrete
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    • v.25 no.1
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    • pp.75-81
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    • 2020
  • The purpose of this paper is to provide an experimental and analytical study on the reinforced large diameter pretensioned high strength concrete (R-LDPHC) pile. R-LDPHC pile was reinforced with infilled concrete, longitudinal, and transverse rebar to increase the flexural and shear strength of conventional large diameter PHC (LDPHC) pile without changing dimension of the pile. To evaluate the shear and flexural strength enhancement effects of R-LDPHC piles compared with conventional LDPHC pile, a two-point loading tests were conducted under simple supported conditions. Nonlinear analysis on the basis of the conventional layered sectional approach was also performed to evaluate effects of infilled concrete and longitudinal rebar on the flexural strength of conventional LDPHC pile. Moreover, ultimate strength design method was adopted to estimate the effect of transverse rebar and infilled concrete on the shear strength of a pile. The analytical results were compared with the results of the bending and shear test. Test results showed that the flexural strength and shear strength of R-LDPHC pile were increased by 2.3 times and 3.3 times compared to those of the conventional LDPHC pile, respectively. From the analytical study, it was found that the flexural strength and shear strength of R-LDPHC pile can be predicted by the analytical method by considering rebar and infilled concrete effects, and the average difference of flexural strength between experimental results and calculated result was 10.5% at the ultimate state.

A study of the changes in the strength and microstructure of the zirconia crown surface by the glazing number (Glazing 횟수가 전장지르코니아에 미치는 굴곡강도와 표면 미세구조의 변화)

  • Oh, Seon Mi
    • Journal of Technologic Dentistry
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    • v.43 no.2
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    • pp.35-41
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    • 2021
  • Purpose: This study aimed to investigate the flexural strength and surface microstructure of the zirconia crown according to the number of glazing zirconia prostheses. Methods: The specimens were made as follows. A specimen without glazing: 1ea, first glazed specimens (group B): 10ea, second glazed specimens (group C): 10ea, third glazed specimens (group D): 10ea. Three-point measuring strength equipment and electron microscopes were used for strength measurement and microstructure observation. As for statistical analysis, one-way ANOVA and t-test (level of significance level=5%) were used to determine the difference in the change in flexural strength according to the number of glazing zirconia prostheses. Results: ANOVA analysis of groups B (1st glazing), C (2nd glazing), and D (3rd glazing) revealed that the change in strength between the groups is statistically significant (p=0.023). The Mann-Whitney test for each group revealed that the difference in flexural strength between groups B and C was not statistically significant (z=-0.302, p=0.762) while that between groups C and D was statistically significant (z=-0.257, p=0.01). Microstructure observation revealed 3 changes in the microstructure of the surface of the glaze powder were observed. Conclusion: According to the number of glazing zirconia prostheses, it was found that the difference in strength between groups was statistically significant, and changes in the microstructure were observed.

Effect of Washing Solvent and Washing Method on Flexural Strength of 3D-Printed Temporary Resin Material (세척 용액 및 세척 방법이 3D 프린팅 임시수복용 레진의 굴곡강도에 미치는 영향)

  • Hae-Bom Kim;Jae-Won Choi
    • Journal of the Korean Society of Industry Convergence
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    • v.27 no.2_2
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    • pp.389-395
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    • 2024
  • The purpose of this study was to evaluate the effect of different washing solvents and washing methods on the flexural strength of 3D printed temporary resin. A bar(25 × 2 × 2 mm) was produced with a layer thickness of 50 ㎛ using an LCD-type 3D printer and divided into 15 groups(n = 10, each) according to washing solution(IPA; 99% isopropyl alcohol, TPM; 93% Tripropylene glycol monomethylether, ETL; Ethanol, TWC; Twin 3D Cleaner, and DNC; DIO navi Cleaner) and washing method(Dip; Dip washing, Ultra; Ultrasonic washing, and Auto; Automated washing). All groups were washed for 5 minutes, and post-cured for 5 minutes using a UV LED light curing machine. The Flexural strength was measured using a three-point bending test using a universal testing machine. For statistical analysis, one-way ANOVA, Tukey HSD post hoc test, Kruskal-Wallis test and post-hoc by Bonferroni-Dunn test(𝛼=.05) were performed depending on whether the normality test was satisfied. In all washing solvents except TPM and DNC, the Dip group showed the lowest flexural strength values, while the Auto group showed the highest flexural strength values except for DNC. Additionally, the washing solution showed completely different flexural strength values depending on the washing method.

The effect of different fiber reinforcements on flexural strength of provisional restorative resins: an in-vitro study

  • Kamble, Vaibhav Deorao;Parkhedkar, Rambhau D.;Mowade, Tushar Krishnarao
    • The Journal of Advanced Prosthodontics
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    • v.4 no.1
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    • pp.1-6
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    • 2012
  • PURPOSE. The aim of this study was to compare the flexural strength of polymethyl methacrylate (PMMA) and bis-acryl composite resin reinforced with polyethylene and glass fibers. MATERIALS AND METHODS. Three groups of rectangular test specimens (n = 15) of each of the two resin/fiber reinforcement were prepared for flexural strength test and unreinforced group served as the control. Specimens were loaded in a universal testing machine until fracture. The mean flexural strengths (MPa) was compared by one way ANOVA test, followed by Scheffe analysis, using a significance level of 0.05. Flexural strength between fiber-reinforced resin groups were compared by independent samples t-test. RESULTS. For control groups, the flexural strength for PMMA (215.53 MPa) was significantly lower than for bis-acryl composite resin (240.09 MPa). Glass fiber reinforcement produced significantly higher flexural strength for both PMMA (267.01 MPa) and bis-acryl composite resin (305.65 MPa), but the polyethylene fibers showed no significant difference (PMMA resin-218.55 MPa and bis-acryl composite resin-241.66 MPa). Among the reinforced groups, silane impregnated glass fibers showed highest flexural strength for bis-acryl composite resin (305.65 MPa). CONCLUSION. Of two fiber reinforcement methods evaluated, glass fiber reinforcement for the PMMA resin and bis-acryl composite resin materials produced highest flexural strength. Clinical implications. On the basis of this in-vitro study, the use of glass and polyethylene fibers may be an effective way to reinforce provisional restorative resins. When esthetics and space are of concern, glass fiber seems to be the most appropriate method for reinforcing provisional restorative resins.

Influence of airborne-particle abrasion on flexural strength of fiber-reinforced composite post (미세입자 분사마모 표면처리가 Fiber-Reinforced Composite 포스트의 굴곡 강도에 미치는 영향)

  • Sim, Eun-Ju;Kim, Jin-Woo;Cho, Kyung-Mo;Park, Se-Hee
    • Journal of Dental Rehabilitation and Applied Science
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    • v.32 no.1
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    • pp.24-31
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    • 2016
  • Purpose: Many studies have shown that airborne-particle abrasion of fiber post can improve the bonding strength to resin cement. But, airborne-particle abrasion may influence the property of fiber post. The purpose of this study is to evaluate the influence of airborne-particle abrasion on flexural strength of fiber post. Materials and Methods: Two fiber-reinforced posts; DT Light Post Size 2 (1.8 mm diameter, Bisco Inc) and RelyX Fiber Post Size 3 (1.9 mm diameter, 3M ESPE); were used in this study. Each group was divided into 3 subgroups according to different surface treatments; without pretreatment: $50{\mu}m$ aluminum oxide (Cobra$^{(R)}$, Renfert): and $30{\mu}m$ aluminum oxide modified with silica (Rocatec Soft$^{(R)}$, 3M ESPE). After airborne-particle abrasion procedure, three-point bending test was done to determine the flexural strength and flexural modulus. The diameter of each posts was measured to an accuracy of 0.01 mm using a digital micrometer. There was no diameter change before and after airborneparticle abrasion. The mean flexural moduli and flexural strengths calculated using the appropriate equations. The results were statistically analyzed using One-way ANOVA and Scheffe's post-hoc test at 95% confidencial level. Results: There was no significant difference on flexural strength between groups. Conclusion: In the limitation of this study, flexural strength and flexural modulus of fiber post are not affected by airborne-particle abrasion.

Thermal shock behavior of alumina ceramics by ball-on-3 ball test (Ball-on-3 ball test에 의한 알루미나 세라믹스의 열충격 거동)

  • 이중현;박성은;한봉석;이홍림
    • Journal of the Korean Ceramic Society
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    • v.36 no.10
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    • pp.1062-1068
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    • 1999
  • The flexural strength distribution of alumina ceramics was observed using ball-on-3 ball test after thermal shock into the distilled water of 25$^{\circ}C$ Crack distribution was also observed by dye-penetration after thermal shock test. Fracture probability of alumina ceramics by ball-on-3 ball test was studied and compared with that by 3-point bending test. The crack distance from the center of thespecimen showed the stronger effect on the flexural strength by ball-on-3 ball test than the crack density.

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