• 한국방재학회:학술대회논문집
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• 한국방재학회 2007년도 정기총회 및 학술발표대회
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• pp.181-185
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• 2007

A free-surface correction(FSC) method is presented to solve the 3-D shallow water equations. Using the mode splitting process, FSC method can simulate shallow water flows under the hydrostatic assumption. For the hydrostatic pressure calculation, the momentum equations are firstly discretized using a semi-implicit scheme over the vertical direction leading to the tri-diagonal matrix systems. A semi-implicit scheme has been adopted to reduce the numerical instability caused by relatively small vertical length scale compare to horizontal one. and, as the free surface correction step the final horizontal velocity fields are corrected after the final surface elevations are obtained. Finally, the vertical final velocity fields can be calculated from the continuity equation. The numerical model is applied to the calculation of the simulation of flow fields in a rectangular open channel with the tidal influence. The comparisons with the analytical solutions show overall good agreements between the numerical results and analytical solutions.

• International Journal of Railway
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• 제1권1호
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• pp.6-11
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• 2008

This paper presents a performance characteristic analysis methodology for a linear induction motor used for a lightweight train. In general, an analytical method cannot provide accurate results in a linear motor because of large airgap, end effect, transverse edge effect, 3-dimensional configurations, large leakage, and so on. Besides, a numerical method requires lots of memory and solving time for transient analysis. However, the suggested methodology which is a kind of hybrid solution with an analytical method and a numerical method is very fast and accurate. Based on the methodology, 3-D FEM analyses for various design schemes of the secondary reaction plate have been done and from the analysis results, the best configuration for an urban railway transit is chosen.

• Structural Engineering and Mechanics
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• 제65권4호
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• pp.381-388
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• 2018

Dynamic behaviour of beam carrying masses has attracted attention of many researchers and engineers. Many studies on the analytical solution of beam with concentric tip mass have been published. However, there are limited works on vibration analysis of beam with an eccentric three dimensional object. In this case, bending and torsional deformations of beam are coupled due to the boundary conditions. Analytical solution of equations of motion of the system is complicated and lengthy. Therefore, in this study, Differential Transform Method (DTM) is applied to solve the relevant equations. First, the Timoshenko beam with 3D tip attachment whose centre of gravity is not coincident with beam end point is considered. The beam is assumed to undergo bending in two orthogonal planes and torsional deformation about beam axis. Using Hamilton's principle the equations of motion of the system along with the possible boundary conditions are derived. Later DTM is applied to obtain natural frequencies and mode shapes of the system. According to the relevant literature DTM has not been applied to such a system so far. Moreover, the problem is modelled by Ansys, the well-known finite element method, and impact test is applied to extract experimental modal data. Comparing DTM results with finite element and experimental results it is concluded that the proposed approach produces accurate results.

• Steel and Composite Structures
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• 제25권2호
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• pp.127-139
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• 2017

In this paper, an exact analytical solution for simply supported sandwich plate which considers the permeation effect of adhesives is presented. The permeation layer is described as functionally graded material (FGM), the elastic modulus of which is assumed to be graded along the thickness following the exponential law. Based on the exact three-dimensional (3-D) elasticity theory, the solution of stresses and displacements for each layer is derived. By means of the recursive matrix method, the solution can be efficiently obtained for plates with many layers. The present solution obtained can be used as a benchmark to access other simplified solutions. The comparison study indicates that the finite element (FE) solution is close to the present one when the FGM layer in the FE model is divided into a series of homogeneous layers. However, the present method is more efficient than the FE method, with which the mesh division and computation are time-consuming. Moreover, the solution based on Kirchhoff-Love plate theory is greatly different from the present solution for thick plates. The influence of the thickness of the permeation layer on the stress and displacement fields of the sandwich plate is discussed in detail. It is indicated that the permeation layer can effectively relieve the discontinuity stress at the interface.

• 분석과학
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• 제32권5호
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• pp.163-172
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• 2019

Methamphetamine (MA) is currently the most abused illicit drug in Korea and its major metabolite is amphetamine (AP). As MA exist as two enantiomers with the different pharmacological properties, it is necessary to determine their respective amounts in a sample. Thus a chiral stationary phase liquid chromatography-tandem mass spectrometric (LC-MS/MS) method was developed for identification and quantification of d-MA, l-MA, d-AP, and l-AP in human urine. Urine sample ($200{\mu}L$) was diluted with pure water and purified using solid-phase extraction (SPE) cartridge. A $5-{\mu}L$ aliquot of SPE treated sample solution was injected into LC-MS/MS system. Chiral separation was carried out on the Astec Chirobiotic V2 column with an isocratic elution for each enantiomer. Identification and quantification of enantiomeric MA and AP was performed using multiple reaction monitoring (MRM) detection mode. Linear regression with a $1/x^2$ as the weighting factor was applied to generate a calibration curve. The linear ranges were 25-1000 ng/mL for all compounds. The intra- and inter-day precisions were within 3.6 %, while the intra- and inter-day accuracies ranged from -5.4 % to 11.8 %. The limits of detection were 2.5 ng/mL (d-MA), 3.5 ng/mL (l-MA), 7.5 ng/mL (d-AP), and 7.5 ng/mL (l-AP). Method validation parameters such as selectivity, matrix effect, and stability were evaluated and met acceptance criteria. The applicability of the method was tested by the analysis of genuine forensic urine samples from drug abusers. d-MA is the most common compound found in urine and mainly used by abusers.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2015년도 제46회 하계학술대회
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• pp.744-745
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• 2015

This paper deals with magnetic characteristic analysis of axial flux permanent magnet coupling according to overload using analytical method. When magnet coupling has a slip, the eddy current induced in PM with conductivity. This eddy current make a distorted flux density. In this paper, we analyze the distorted flux density. The analytical results are validated extensively by comparing with 3d finite element analysis.

• 분석과학
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• 제8권4호
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• pp.511-517
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• 1995

A cationic water soluble porphyrin (5,10,15,20-tetrakis (l-methyl-pyridinium-4-yl)porphyrin, $H_2tmpyp^{4+}$) and its metalloporphyrins (MP) were easily extracted into acetonitrile separated by addition of sodium chloride ($4mol\;dm^{-3}$) in the presence of sodium perchlorate, where M denotes $Zn^{2+}$, $Cu^{2+}$, $Co^{3+}$, $Fe^{3+}$, and $Mn^{3+}$ and $P^{2-}$ is porphyrinate ion. The extracted ion-pair complexes were completely dissociated to $[MP(ClO_4)_3]^+$, and $[MP(ClO_4)_2]^{2+}$. The extraction and the dissociation constants were determined by taking into account of the partition constant of sodium perchlorate ($K_D=1.82{\pm}0.01$). The chemical properties of the separated acetonitrile phase as $E_{T(30)}$ and $D_{II,I}$ were determined and compared with other water miscible solvents (acetone, actonitrile, 1,4-dioxane, tetrahydrofuran, 1-propanol and 2-propanol). Furthermore, a sensitive and selective method was proposed for the determination of a subnanogram amount of copper(II) in natural water samples by using the present salting-out method and the porphyrins.

• 한국산학기술학회논문지
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• 제19권6호
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• pp.677-682
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• 2018

관계분석형 R&D 포트폴리오 방법은 중점기술의 선정기준이 독립적일 경우 각 선정기준의 고유한 목적과 특성을 반영하여 중점기술을 선정하는 방법이다. 본 연구는 중점기술을 도출하기 위한 방법으로 관계분석형 R&D 포트폴리오 방법을 제시하고 선정기준과 분석지표간의 상관관계 분석하는 1단계, 각 선정기준에 최적으로 부합하는 포트폴리오 매트릭스를 구성하는 2단계, 중점기술을 도출하는 3단계로 나누어 방법론을 적용하는 과정을 서술하였다. 본 연구에서는 중점기술을 선정하기 위한 4대 선정기준과 기술수준, 경제성, 기술성을 파악하기 위한 분석지표간의 상관관계를 HoQ를 응용한 표로 작성하였다. 상관관계표를 바탕으로 각 선정기준을 최적으로 만족하기 위해 고려해야 할 분석지표를 도출하였으며, 도출된 분석지표와 선정기술을 두 축으로 포트폴리오 매트릭스를 구성하였다. 4대 기준을 모두 충족하는 충족형 포트폴리오 P0와 4대 선정기준의 고유한 특성을 반영하여 각 선정기준을 효과적으로 충족하는 포트폴리오 P1~P4를 구성하여 중점기술을 도출하였다. 선정된 중점기술은 명세기반의 키워드 분석 등의 과정을 거쳐 미래 안보환경에 대응하기 위한 중점분야 선정에 활용될 수 있다.

• Mass Spectrometry Letters
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• 제10권1호
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• pp.38-42
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• 2019

Damaurone D belongs to the genus Rosa and is a traditional medicinal product used for the treatment of depression, inflammation, and infectious diseases. The purpose of this study was to develop a simple liquid chromatography-tandem mass spectrometry method for the detection of damaurone D in rat plasma and to demonstrate its application in pharmacokinetic studies. Damaurone D and berberine (internal standard) were extracted with acetonitrile using a protein precipitation method. Mass transition was monitored in multiple reaction monitoring mode at m/z $323.2{\rightarrow}267.0$ for damaurone D and m/z $336.1{\rightarrow}320.0$ for berberine in positive ion mode. Analytical validation was conducted by evaluating the specificity, linearity, accuracy, precision, matrix effect, extraction recovery, and stability. The calibration curves were linear over 2-1000 ng/mL. The intra- and inter-day precision and accuracy of quality control samples were 4.79-13.33% and 86.23-102.75%, respectively. The matrix effect and extraction recovery were 96.11-98.47% and 96.11-102.25%, respectively. In the pharmacokinetic study after intravenous administration of damaurone D at a dose of 3 mg/kg in rats, the area under the curve and clearance of damaurone D in rat plasma were $16750.26{\pm}2676.10min{\cdot}ng/mL$ and $182.44{\pm}31.36mL/min/kg$, respectively.

• 분석과학
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• 제7권3호
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• pp.349-359
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• 1994

천연가스 중의 부취제 농도를 분석하기 위한 기체 크로마토그래피 방법에 대하여 연구하였다. TBM(tertiarybutylmercaptan) 및 THT(tetrahydrothiophene)를 포함한 8종의 부취제를 OV-101 컬럼상에서 거의 완전히 분리하였다. 수소 유속, 공기 유속 및 검출기 온도와 같이 FPD의 응답에 영향을 미치는 몇 가지 상호 관련된 파라미터들의 최적 조건을 구하였다. TBM과 THT의 검정곡선을 투과한 장치를 이용하여 작성하였다. 이러한 분석방법을 천연가스 공급관 내의 혼합 부취제인 TBM과 THT를 정량하는 데 적용하였다. 부취수준과 부취제 농도와의 상관관계를 구하기 위한 냄새 측정기의 유용성에 대하여 알아보았다.