• Title/Summary/Keyword: 2-Phase

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A study on the grain growth mechanism in dual-phase high Cr-steel (고크롬 (α+γ) 2상강의 결정립 성장기구)

  • Wey, Myeong-Yong
    • Journal of the Korean Society for Heat Treatment
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    • v.11 no.4
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    • pp.324-332
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    • 1998
  • The grain growth characteristics of dual-phase (${\alpha}+{\gamma}$) containing high Cr-steel have investigate using ${\alpha}$-, ${\gamma}$-single phases and (${\alpha}+{\gamma}$)dual-phase of 12%Cr Steel. The heat treatment has performed at $1000-1200^{\circ}C$ for 1-100hr. The results are as follows : 1) The grain growth rate in (${\alpha}+{\gamma}$) dual phase was substantially slower than that of single grain. 2) The relation between mean grain radius $\bar{{\gamma}}$ and annealing time t is, in general, described as following equation : $$(\bar{{\gamma}})^n-(\bar{{\gamma}_o})^n=K_n{\cdot}t{\cdots}{\cdots}(1)$$ i) In the case of single phase of high Cr steel, Eq.(1) is described as $(\bar{{\gamma}})^2-(\bar{{\gamma}_o})^2=K_2{\cdot}t$ and the grain growth is controlled by boundary migration. ii) In dual phase, the grain growth needs diffusion of alloying elements because the chemical composition of ${\alpha}$- and ${\gamma}$- phases differs from each other. When the volume fraction of ${\alpha}$-, ${\gamma}$-phase was almost equal and ${\gamma}$-phase in the case of 80 and $90%{\gamma}$. Eq.(1) is described as $(\bar{{\gamma}})^3-(\bar{{\gamma}_o})^3=K_3{\cdot}t$ because the grain growth is controlled by volume diffusion iii) In the case of ${\gamma}$-rich phase (80 and $90%{\gamma}$), the grain growth of minor phase (10 and $20%{\alpha}$) is described as $(\bar{{\gamma}})^4-(\bar{{\gamma}_o})^4=K_4{\cdot}t$ because the boundary diffusion is predominent rather than volume diffusion.

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Formation of Phases and Mechanical Properties of YSZ-Based Thermal Barrier Coating Materials Doped with Rare Earth Oxides (희토류 산화물이 첨가된 YSZ 기반의 열차폐 코팅용 소재의 상 형성 및 기계적 특성)

  • Yong Seok Choi;Gye Won Lee;Sahn Nahm;Yoon suk Oh
    • Journal of Powder Materials
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    • v.30 no.5
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    • pp.402-408
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    • 2023
  • This study focused on improving the phase stability and mechanical properties of yttria-stabilized zirconia (YSZ), commonly utilized in gas turbine engine thermal barrier coatings, by incorporating Gd2O3, Er2O3, and TiO2. The addition of 3-valent rare earth elements to YSZ can reduce thermal conductivity and enhance phase stability while adding the 4-valent element TiO2 can improve phase stability and mechanical properties. Sintered specimens were prepared with hot-press equipment. Phase analysis was conducted with X-ray diffraction (XRD), and mechanical properties were assessed with Vickers hardness equipment. The research results revealed that, except for Z10YGE10T, most compositions predominantly exhibited the t-phase. Increasing the content of 3-valent rare earth oxides resulted in a decrease in the monoclinic phase and an increase in the tetragonal phase. In addition, the t(400) angle decreased while the t(004) angle increased. The addition of 10 mol% of 3-valent rare-earth oxides discarded the t-phase and led to the complete development of the c-phase. Adding 10 mol% TiO2 increased hardness than YSZ.

Inhibitory Effect of Bojungbangam-tang Kakambang on Cisplatin-Induced G2/M Phase Arrest in Human Renal Proximal Tubular HK-2 Cells (보정방암탕가감방(保正防癌湯加減方)이 cisplatin으로 유도된 인간 근위세뇨관 HK-2세포의 G2/M phase arrest에 미치는 영향)

  • Park, Sung-Cheul;Lee, Su-Kyung;Yeom, Seung-Ryong;Kwon, Young-Dal;Song, Yung-Sun
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.21 no.6
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    • pp.1555-1563
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    • 2007
  • To idenifty effect of Bojungbangam-tang kakambang on Cisplatin-Induced G2/M Phase Arrest in Human Renal Proximal Tubular HK-2 Cells. Cytotoxicity of cisplatin was detected in HK-2 cells and the value of IC50 is about $25\;{\mu}M$. The treatment of cisplatin to HK-2 showed the G2/M phase cell cycle arrest. The ethanol extract of Bojungbangam-tang kakambang (EBTKB), a new herbal prescription composed of ten crude herbs, inhibited cisplatin-induced G2/M phase arrest in HK-2 cells. EBTKB increased G0/G1 peak in cisplatin-treated HK-2 cells. p53, p21 and p27 expression were increased in cisplatin-treated HK-2 cells. Inhibitory effect of EBTKB on cisplatin-induced G2/M phase arrest was accomplished through inhibition of p53, p21 and p27 expression. Also, reduced CDK2 and cyclin A expression by cisplatin were increased by EBTKB, but cyclin E was not changed. Reduction of ERK activation and increment of p38 activation by cisplatin were increased ERK activation and decreased p38 activation by EBTKB. Cisplatin had no effect on JNK activation, but EBTKB increased JNK activation. These results can suggest that EBTKB inhibits cisplatin-induced G2/M phase arrest in HK-2 cell through reduction of p53-dependent p21 and p27 protein, ERK activation and p38 inactivation.

Variation of Dielectric Constnat with Grain Size of Pyrochlore Phase in the PMN-Pyrochlore Diphasic Mixtrues (Pyrochlore상의 입자크기에 따른 PMN-Pyrochlore 2상 혼합체의 유전율 변화)

  • 허강일;김정주;조상희
    • Journal of the Korean Ceramic Society
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    • v.30 no.5
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    • pp.365-372
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    • 1993
  • Variation of dielectric constant in PMN-Pyrochlore diphasic mixtures were investigated with grain size of pyrochlore phase. Size of pyrochlore phase was controlled by the numbers of calcining and sedimentation method during powder processing. When grain size of pyrochlore phase is large in the sintered specimen, dielectric constant slowly decreased with increase of amount of pyrochlore phase. On the contary, grain size of pyrochlore phase is small, dielectric constant drastically decreased. It was thought that small sized pyrochlore grains more easily surrounded high dielectric phase (perovskite PMN) than large ones with addition of pyrochlore phase.

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Design of Ku-Band Phase Locked Harmonic Oscillator (Ku-Band용 위상 고정 고조파 발진기 설계)

  • Lee Kun-Joon;Kim Young-Sik
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.16 no.1 s.92
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    • pp.49-55
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    • 2005
  • In this paper, the phase locked harmonic oscillator(PLHO) using the analog PLL(Phase Locked Loop) is designed and implemented for a wireless LAN system. The harmonic oscillator is consisted of a ring resonator, a varactor diode and a PLL circuit. Because the fundamental fiequency of 8.5 GHz is used as the feedback signal for the PLL and the 2nd harmonic of 17.0 GHz is used as the output, a analog frequency divider for the phase comparison in the PLL system can be omitted. For the simple PLL circuit, the SPD(Sampling Phase Detector) as a phase comparator is used. The output power of the phase locked harmonic oscillator is 2.23 dBm at 17 GHz. The fundamental and 3rd harmonic suppressions are -31.5 dBc and -29.0 dBc, respectively. The measured phase noise characteristics are -87.6 dBc/Hz and -95.4 dBc/Hz at the of offset frequency of 1 kHz and 10 kHz from the carrier, respectively.

Phase Transformation and Dielectric Properties of <001> 0.7Pb(Mg1/3Nb2/3)O3-0.3PbTiO3 Single Crystals (<001> 0.7Pb(Mg1/3Nb2/3)O3-0.3PbTiO3 단결정의 상변화 및 유전 특성)

  • Lee, Eun-Gu;Lee, Jae-Gab
    • Korean Journal of Materials Research
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    • v.21 no.7
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    • pp.391-395
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    • 2011
  • The structure and dielectric properties of poled <001>-oriented 0.7Pb($Mg_{1/3}Nb_{2/3})O_3-0.3PbTiO_3$ (PMN-0.3PT) crystals have been investigated for orientations both parallel and perpendicular to the [001] poling direction. An electric field induced monoclinic phase was observed for the initial poled sample. The phase remained stable after the field was removed. A quite different temperature dependence of dielectric constant has been observed between heating and cooling due to an irreversible phase transformation. The results of mesh scans and temperature dependence of the dielectric constant demonstrate that the initial monoclinic phase changes to a single domain tetragonal phase at 370K and to a paraelectric cubic phase at 405K upon heating. However, upon subsequent cooling from the unpoled state, the cubic phase changes to a poly domain tetragonal phase and to a rhombohedral phase. In the ferroelectric tetragonal phase with a single domain state, the dielectric constant measured perpendicular to the poling direction was dramatically higher than that of the parallel direction. A large dielectric constant implies easier polarization rotation away from the polar axis. This enhancement is believed to be related to dielectric softening close to the morphotropic phase boundary and at the phase transition temperature.

Convective Boiling Two-phase Flow in Trapezoidal Microchannels : Part 1-Pressure Drop Characteristics (사다리꼴 미세유로의 대류비등 2상유동 : 1부-압력강하 특성)

  • Kim, Byong-Joo;Kim, Geon-Il
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.23 no.1
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    • pp.87-94
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    • 2011
  • Characteristics of two-phase pressure drop in microchannels were investigated experimentally. The microchannels consisted of 9 parallel trapezoidal channels with each channel having $205\;{\mu}m$ of bottom width, $800\;{\mu}m$ of depth, $3.6^{\circ}$ of sidewall angle, and 7 cm of length. Pressure drops in convective boiling of Refrigerant 113 were measured in the range of inlet pressure 105~195 kPa, mass velocity $150{\sim}920\;kg/m^2s$, and heat flux $10{\sim}100\;kW/m^2$. The total pressure drop generally increased with increasing mass velocity and/or heat flux. Two-phase frictional pressure drop across the microchannels increased rapidly with exit quality and showed bigger gradient at higher mass velocity. A critical review of correlations in the literature suggested that existing correlations were not able to match the experimental results obtained for two-phase pressure drop associated with convective boiling in microchannels. A new correlation suitable for predicting two-phase friction multiplier was developed based on the separated flow model and showed good agreement with the experimental data.

Characteristics of Ag-added Ge2Sb2Te5 Thin Films and the Rapid Crystallization (Ag-첨가 Ge2Sb2Te5 박막의 물성 및 고속 결정화)

  • Kim, Sung-Won;Song, Ki-Ho;Lee, Hyun-Yong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.7
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    • pp.629-637
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    • 2008
  • We report several experimental data capable of evaluating the amorphous-to-crystalline (a-c) phase transformation in $(Ag)_x(Ge_2Sb_2Te_5)_{1-x}$ (x = 0, 0.05, 0.1) thin films prepared by a thermal evaporation. The isothermal a-c structural phase changes were evaluated by XRD, and the optical transmittance was measured in the wavelength range of $800{\sim}3000$ nm using a UV-vis-IR spectrophotometer. A speed of the a-c transition was evaluated by detecting the reflection response signals using a nano-pulse scanner with 658 nm laser diode (power P = $1{\sim}17$ mW, pulse duration t = $10{\sim}460$ ns). The surface morphology and roughness of the films were imaged by AFM. It was found that the crystallization speed was so enhanced with an increase of Ag content. While the sheet resistance of c-phase $(Ag)_x(Ge_2Sb_2Te_5)_{1-x}$ was similar to that of c-phase $Ge_2Sb_2Te_5$ (i.e., $R_c{\sim}10{\Omega}/{\square}$), the sheet resistance of a-phase $(Ag)_x(Ge_2Sb_2Te_5)_{1-x}$ was found to be lager than that of a-phase $Ge_2Sb_2Te_5$, $R_a{\sim}5{\times}10^6{\Omega}{/\square}$. For example, the ratios of $R_a/R_c$ for $Ge_2Sb_2Te_5$ and $(Ag)_{0.1}(Ge_2Sb_2Te_5)_{0.9}$ were approximately $5{\times}10^5$ and $5{\times}10^6$, respectively.

Influence of air pressure, temperature, humidity and CO$_{2}$ concentration on optical phase changes in thin films

  • Kim, Moon-Hwan;Tachikawa, Yoshihiko;Ogita, Eiji;Ueda, Toshitsugu
    • 제어로봇시스템학회:학술대회논문집
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    • 1989.10a
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    • pp.799-804
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    • 1989
  • A new method for measuring optical phase changes of reflection beam from optical mirror is proposed. The optical phase change is liable to change with varying atmosphere conditions. This optical phase changes are measured against air pressure, temperature, humidity and CO$\_$2/ concentration variations. It is clarified that the optical phase changes are most effected by humidity change.

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Numerical Simulation of Two-Phase Flow for Gas-Solid Particles (가스와 입자가 혼합된 2상 유동에 관한 수치해석적 연구)

  • Jung H.;Choi J. W.;Park C. G.
    • Journal of computational fluids engineering
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    • v.6 no.4
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    • pp.8-14
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    • 2001
  • The phenomena of two-phase suspension flows appear widely in nature and industrial processes. Hence, it is of great importance to understand the mechanism of the gas-solid two-phase flows. In the present study, the numerical simulation has been approached by utilizing the Eulerian-Lagrangian methodology for describing the characteristics of the fluid and particulate phases in a vertical pipe and a 90°square-sectioned bend. The continuous phase(gas phase) is described by the Eulerian formulation and a κ-ε turbulence model is employed to find mean and turbulent properties of the gas phase. The particle properties(velocity and trajectory) are then described by a Lagrangian approach and computed using the mean velocity and turbulent fluctuating velocity of the gas phase. The predictions are compared with measurements by laser-Doppler velocimeter for the validation. As a result, the calculated results show good agreements.

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