• Korean Journal of Materials Research
• /
• v.9 no.7
• /
• pp.724-734
• /
• 1999

The adhesion characteristics of the thermoplastic resins such as PE, PP PVC, PET and PS were investigated on the surfaces of conventional steel (SS41), steel (SS41P) treated with ultrasonic waves and the SS41P coated with several ceramic powders (SS41PC) by the plasma spray. Alumina (Al$_2$O$_3$), alumina titania (Al$_2$O$_3$95%, TiO$_2$ 5%) and zirconia yttria (ZrO$_2$ 95%, $Y_2$O$_3$5% ) were used for the materials plasma spray The morphologies, surface hardness, surface roughness, and contact angles on SS41, SS41P, and SS41PC were examined. The tensile shear strength and peel strength of the polymers which were attached to the surfaces of ceramics coated on SS41P also were measured. The tensile shear strength and peel strength of polymers adhered to ceramic surface coated on steel were found to be stronger than those of conventional steel. The tensile shear strength and peel strength of the polymers adhered on the surfaces of ceramics coated steel increased in the following order PE > PET > PP > PS > PVC. The high adhesion strength of PE may be attributed to the surface roughness and its anchor effect on the ceramic surface.

• Restorative Dentistry and Endodontics
• /
• v.18 no.1
• /
• pp.73-83
• /
• 1993

The purpose of this study was to evaluate the effect of various acid treatments on dentin bonding. Freshly extracted human teeth were uprightly embedded in self curing acrylic resin, and their occlusal surfaces were grinded to expose flat dentin surfaces. The specimens were divided into 4 groups. Specimens of one group were not treated so as to be a control and those of the other three groups were threated with 10% polyacrylic acid, 10% phosphoric acid, and 10-3 solution(10% citric acid/3% ferric chloride) respectively. Primer, bonding resin and composite resin were applied over the treated dentin surfaces sequentially. All specimens were stored in $37^{\circ}C$ distilled water for 24 hours, then the tensile bond strength was measured and the treated dentin surfaces and fracured dentin surfaces were examined under a scanning electron microscope. The results were as follows: Bond strengths of acid-treated groups were higher than those of the untreated group. In the acid-treated groups, bond strength was found to be the highest in the 10-3 solution group followed by the 10% phosphoric acid group and the 10% polyacrylic acid group(P<0.01). On SEM examination of dentin surfaces, the untreated dentin surface showed a remaining smear layer and closed dentinal tubules. Dentin surfaces treated with 10 % polyacrylic acid showed a clean dentin surface without the smear layer, but showed remaining smear plugs in dentinal tubules. A dentin surface treated with 10% phosphoric acid or 10-3 solution showed open dentinal tubules without the smear layer or smear plugs. On SEM observation of the fractured dentin-resin interface, the untreated group showed that failure occurred in the smear layer. The group treated with 10% polyacrylic acid showed no resin tag remained in the dentinal tubules, but resin tags in the dentinal tubules were observed in the group treated with the 10% phosphoric acid or the 10-3 solution. On the failure mode examination, the higher the bond strength of the group, the higher the frequency of cohesive failure. The coefficient between bond strength and cohesive failure rate was 0.71.

• Journal of the Society of Disaster Information
• /
• v.12 no.1
• /
• pp.54-61
• /
• 2016

The use of advanced composite materials in strengthening and repair of existing structures is increasing rapidly. This paper describes an effectiveness of a bonding of carbon fiber reinforced sheets to corroded steel members for the repair. Three types of surface treatment, what we call cleaning, of corroded plate are chosen as parameters. They are "without cleaning","removal of painting by brushing" and "complete removal of painting". From the experimental study, the following findings are obtained. 1) When the steel plate is subjected to tensile force, carbon fiber sheets adhered to the painted steel gives a higher strength against peeling compared to that of the plate without painting, 2) The grade of surface treatment, or cleaning of the corroded steel plate affects the strengthening effect.

• The korean journal of orthodontics
• /
• v.35 no.6 s.113
• /
• pp.443-450
• /
• 2005

This study was performed to compare the shear bond strength of orthodontic adhesive to amalgam according to different light sources (halogen-based light and light emitting diode (LED)) and amalgam surface treatments. Ninety extracted human premolars were randomly divided into 6 groups (4 experimental and 2 control groups) of 15 by light sources and surface treatments. Orthodontic brackets were bonded and shear bond strength was measured with an Instron universal testing machine. The findings were as follows: The bond strength of adhesive to amalgam surface was 3-5.5 MPa which was lower than that of acid-etched enamel (19 MPa) control. In the sandblasted amalgam surface, the shear bond strength of the halogen light group was higher than that of the LED group (p < 0.05) but. in the non-treated amalgam surface. there was no significant difference in the shear bond strength according to the light sources (p> 0.05). Within the same light source. sandblasting had no significant effect on the shear bond strength of the adhesive bonded to amalgam surface (p > 0.05). There was no significant difference in shear bond strength according to the light sources in acid-etched enamel control groups. This results suggest that there can be a limit in using light curing adhesives when brackets are bonded to an amalgam surface. Additional clinical studies are necessary before routine use of halogen light and LED light curing units can be recommended in bonding brackets to an amalgam surface.

• Restorative Dentistry and Endodontics
• /
• v.32 no.3
• /
• pp.198-207
• /
• 2007

The purpose of this study was to investigate the effect of calcium hydroxide on dentin bonding strength of various dentin bonding systems as a function of time in composite resin restoration. Dentin adhesives used in this study were Scotchbond Multipurpose, Single Bond, SE Bond and Prompt L-Pop. Flat dentin surfaces adjacent to pulp chamber were created, then $Ca(OH)_2$ and saline were mixed and applied on dentin surface of experimental group, then IRM was used to cover the mixture on dentin surface and the specimens were stored at $36.5^{\circ}C$ for experiment period (7 days, 30 days). After removing IRM and $Ca(OH)_2$, each dentin adhesives were treated on dentin surfaces. Composite resin (Z-250, 3M) was placed with S mm height and was light-cured for 20 seconds. After stored in distilled water for 24 hours, each dentin-composite bonded spicemen was embedded in epoxy resin and sectioned into $1.0\times1.0mm^2$ cross section composite-dentin beams. Specimen was mounted on zig of Universal testing machine and ${\mu}TBS$ test was performed. SEM analysis was performed to examine the fractured surfaces. The results suggested that applying calcium hydroxide did not show significant difference in dentin bonding strength.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
• /
• 2000.10a
• /
• pp.47-52
• /
• 2000

F.R.P specimens were made by mixture CM(chopped mat) 450-104 matrix & RC(roving clothes)570-100 Roving, the mixture ratio Resin: hardener (92:8) for tensile test. It was also made of plates by hand lay-up method and was been cured for 24 hours and then was cut tensile specimens in accordance with ASTM D638 Type 3. Knowing exact behavior of bonded area's stress and strain when the tensile test was going on, the test specimens were made of 2 plies laminae of F.R.P in each for supporting cut part in middle of specimen length. And in middle part also were covered of F.R.P plies of 1/2, 2/3 length of specimen in each as well. Also we consider shear stress in adhered area. This study reveals that as plys length is more longer, rupture stress grows remarkably larger.

• Restorative Dentistry and Endodontics
• /
• v.30 no.6
• /
• pp.450-460
• /
• 2005

The aim of this study was to evaluate the effect of cavity shape, bond quality of bonding agent and volume of resin composite on shrinkage stress developed at the cavity floor. This was done by measuring the shear bond strength with respect to iris materials (cavity shape , adhesive-coated dentin as a high C-factor and Teflon-coated metal as a low C-factor), bonding agents (bond quality: $Scotchbond^{TM}$ Multi-purpose and Xeno III) and iris hole diameters (volume; 1mm or 3mm in $diameter{\times}1.5mm$ in thickness). Ninety-six molars were randomly divided into 8 groups ($2{\times}2{\times}2$ experimental setup). In order to simulate a Class I cavity, shear bond strength was measured on the flat occlusal dentin surface with irises. The iris hole was filled with Z250 restorative resin composite in a bulk-filling manner. The data was analyzed using three-way ANOVA and the Tukey test. Fracture mode analysis was also done When the cavity had high C-factor, good bond quality and large volume, the bond strength decreased significantly The volume of resin composite restricted within the well-bonded cavity walls is also be suggested to be included in the concept of C-factor, as well as the cavity shape and bond quality. Since the bond quality and volume can exaggerate the effect of cavity shape on the shrinkage stress developed at the resin-dentin bond, resin composites must be filled in a method, which minimizes the volume that can increase the C-factor.

• Composites Research
• /
• v.24 no.6
• /
• pp.56-63
• /
• 2011

The objective of this study is to investigate appropriate bonding methods of solar cells in order to apply solar cells, which have been receiving particular attention as a renewable energy due to fossil energy depletion and environment issues, to composite structures. Back-contact solar cells with approximately 24.2% energy conversion efficiency were used in this study. Since silicon-based solar cells are mechanically fragile, the secondary-bonding methods using adhesive were examined in this study. The experiment was conducted with three kinds of bonding materials such as EVA film, Resin film and elastic adhesive. The performance of solar cells for three types of adhesives under mechanical loading on test specimens is conducted. In addition, the measuring equipment was designed to evaluate the performance of the solar cells under mechanical loading in real time and the fracture characteristics depending on bonding materials were evaluated. The reason decreasing solar cells efficiency were analyzed and considered by Fractography. The results show that the solar cell performance is largely affected by bonding techniques. Moreover, the bonding method using elastic adhesive shows best solar cell efficiency.

• Journal of the Korean Society of Clothing and Textiles
• /
• v.30 no.12 s.159
• /
• pp.1683-1689
• /
• 2006

Precedent researches on lyocell are mostly on lyocell structure, characteristics, physical properties by finishing and dyeability, and the like; there are little cases of researches on interlining for lyocell clothes production. To serve as a base information helpful to select fusible interlining and improve the efficiency of sewing process considering the characteristics of lyocell, this study performed t-est, F-test toward to the difference in the appearance-related properties and the mechanical properties of lyocell-interlining bonded fabric in accordance with the characteristics of fusible interlining and lyocell face fabric. This study reached following conclusions. Drapability and Crease recovery of lyocell-interlining bonded fabric are influenced by the structure of fusible interlining; stiffness of lyocell-interlining bonded fabric, by the structure of fusible interlining and the yam number of lyocell face fabric. WT is influenced by the mixture rate and yam number of lyocell face fabric. RT is influenced by the yam number of lyocell face fabric; G, 2HG, 2HG5, by the structure(woven and non-woven) of fusible interlining; B, HB, by the weight, structure(woven and non-woven) of fusible interlining, and yam number of lyocell face fabric; WC, by the weight, structure of fusible interlining; RC, by the structure of fusible interlining; thickness, by the weight of fusible interlining and the yarn number of lyocell face fabric; weight, by mixture rate and yam number of lyocell face fabric.

• Restorative Dentistry and Endodontics
• /
• v.35 no.2
• /
• pp.125-133
• /
• 2010

Objectives: Rapid polymerization of overlying composite resin causes high polymerization shrinkage stress at the adhesive layer. In order to alleviate the shrinkage stress, increasing the light intensity over the first 5 seconds was suggested as an exponential curing mode by an LED light curing unit (Elipar FreeLight2, 3M ESPE). In this study, the effectiveness of the exponential curing mode on reducing stress was evaluated with measuring microtensile bond strength of three adhesives after the overlying composite resin was polymerized with either continuous or exponential curing mode. Methods: Scotchbond Multipurpose Plus (MP, 3M ESPE), Single Bond 2 (SB, 3M ESPE), and Adper Prompt (AP, 3M ESPE) were applied onto the flat occlusal dentin of extracted human molar. The overlying hybrid composite (Denfil, Vericom, Korea) was cured under one of two exposing modes of the curing unit. At 48h from bonding, microtensile bond strength was measured at a crosshead speed of 1.0 mm/min. The fractured surfaces were observed under FE-SEM. Results: There was no statistically significant difference in the microtensile bond strengths of each adhesive between curing methods (Two-way ANOVA, p > 0.05). The microtensile bond strengths of MP and SB were significantly higher than that of AP (p < 0.05). Mixed failures were observed in most of the fractured surfaces, and differences in the failure mode were not observed among groups. Conclusion: The exponential curing method had no beneficial effect on the microtensile dentin bond strengths of three adhesives compared to continuous curing method.