• Title/Summary/Keyword: 희석제

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X-Ray Spectrometric Analysis of $Ta_2O_5$,$Nb_2O_5$ and $SnO_2$in Tin Slags using Standard Addition and Dilution Method (표준물첨가 및 희석법을 이용한 주석 슬랙중$Ta_2O_5$,$Nb_2O_5$$SnO_2$의 X-선 분광분석)

  • Young-Sang Kim;Dong-Hui Lee
    • Journal of the Korean Chemical Society
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    • v.27 no.6
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    • pp.424-482
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    • 1983
  • Determination for $Ta_2O_5$,$Nb_2O_5$ and $SnO_2$ in tin slags was investigated by X-ray spectrometric method. Standard addition-dilution method was attempted and showed a comparable accuracy with standard calibration curve method. Pure chemicals($Ta_2O_5$,$Nb_2O_5$ and $SnO_2$) were added to the samples and diluted with silica or ferric oxide. For the determination of $Ta_2O_5$and$SnO_2$ , silica was more suitable than ferric oxide while the latter was more preferable than the former for $Nb_2O_5$.

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The Predilution Effect of Al-based Liquid Coagulants for the Optimal Efficacy (최적 응집 효율을 위한 Al계 액상 응집제의 희석 효과)

  • Heo, Jae-Yong;Lee, Sang-Wha
    • Applied Chemistry for Engineering
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    • v.17 no.1
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    • pp.37-43
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    • 2006
  • The coagulation efficacy of Al-based coagulants (such as Alum, PACS, and PACC) was investigated to ascertain removal efficiencies of turbidity and phosphate with variation of solution pH, coagulant dosages, and pre-dilution ratios. The efficacy of Al-based coagulants was maximized in the pH range of 6~9. Under the initial condition of pH 8, $10mg/L\;{PO_4}^{3-}$, and 20 NTU, Al-based coagulants exhibited a similar efficacy in the removal of turbidity, whereas the removal efficiency of phosphate was clearly dependent on the basicity of coagulants: Alum (0%) > PACS (45~50%) > PACC (70%). At high initial turbidity of 100 NTU, polymeric coagulants, such as PACS and PACC, exhibited a higher removal efficiency of turbidity compared to Alum. In comparison to direct injection of coagulants at low initial turbidity (20 NTU), 500~2000 times pre-diluted Alum, exhibited reduced coagulation efficacy; however, removal efficiencies of turbidity and phosphate increased with the increase of retention time. Pres-diluted PACC exhibited the enhanced coagulation efficacy followed by silght decrease of the removal efficiencies with increase of the retention time. At high initial turbidity of 100 NTU, pre-diluted Alum and PACC exhibited higher removal efficiencies of turbidity and phosphate.

Absorption characteristic of carbon dioxide in Ionic Liquids based sulfite anion in the pre-combustion condition (연소 전 조건에서 음이온이 Sulfite계인 이온성 액체의 CO2 흡수 특성)

  • Baek, Geun Ho;Jang, Hyun Tae;Cha, Wang Seog
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.22 no.3
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    • pp.763-769
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    • 2021
  • In this study, ionic liquids were synthesized to remove carbon dioxide (CO2) on a laboratory scale. The vapor-liquid absorption equilibrium device (VLE) was used to investigate the carbon dioxide absorption capacity. In the regeneration study, the absorption capacity after regeneration was reduced by approximately 7% for all ionic liquids, in which the anion was sulfite-based, showing excellent regeneration. Ethyl sulfite showed the highest absorption capacity of CO2 among the ionic liquids based on the sulfite anion. In particular, the absorption capacity of [beim] ethyl sulfite was 1.1 mol CO2 / mol IL at an absorption equilibrium pressure of 22 bar. In the regeneration study, the absorption capacity after regeneration was reduced by approximately 7% for all ionic liquids, in which the anion was sulfite-based, from which regeneration is outstanding. After the absorption experiment, the viscosity of the sample tended to decrease by approximately 8% compared to that before the absorption experiment. On the other hand, the absorbent was synthesized in the first step. Moreover, the raw material used is also inexpensive and has excellent reproducibility and highly stable absorbent capacity.

Void Formation Mechanism of Thermoset (열경화성 수지의 기공 생성 원인)

  • 강길호;박상윤
    • Polymer(Korea)
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    • v.28 no.1
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    • pp.35-40
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    • 2004
  • The formation mechanism of void defect which deteriorate composite's property is various according to each composite process. In this paper, void formation and growth mechanism is analyzed by thermal analysis and GC/MS. We made a vacuum chamber for observing pressure effect. Thermal analysis has been done in various condition. Elements of volatiles during resin curing were turned out by GC/MS. The most of volatiles of polyester were composed of styrene (over 80%) and a small quantity of toluene. In case epoxy resin, butyl glycidyl ether was the main element of volatiles (over 90%). We concluded that the original sites of void growth existed in resin and they were eliminated by vacuum and heating process. And the growth of void was influenced by water, diluents, solvent, and reactants in resin.

BTX의 폭발특성에 관한 연구

  • 김종복;오규형;이성은;류창하
    • Proceedings of the Korean Institute of Industrial Safety Conference
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    • 2000.11a
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    • pp.140-145
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    • 2000
  • BTX는 석유화학곧업에서 생산되는 방향족탄화수소 화합물의 주요 생산품목인 Benzene, Toluene, Xylene을 일컫는 말로서 석유화학공정에서 간단히 줄여서 쓰는 용어이다. 벤젠, 톨루엔, 크실렌 등은 페인트 희석제로 쓰이는 유기용매의 주성분들이며, 인체에 중독성을 나타내는 유해물질이기도 하며 소방법상에서는 인화성액체인 4류 위험물로 취급하고 있다.(중략)

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Effect of Diluent Size on Aluminum Nitride Prepared by Using Self-Propagating High-Temperature Synthesis Process (희석제 입도가 고온자전연소법에 의한 질화알루미늄 합성에 미치는 영향)

  • Lee, Jae-Ryeong;Lee, Ik-Kyu;Shin, Hee-Young;Chung, Hun-Saeng
    • Journal of the Korean Ceramic Society
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    • v.42 no.1
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    • pp.69-75
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    • 2005
  • To investigate the morphological effect on synthesis of aluminum nitride by SHS Process, two type of Al Powder (granular and flacky shape) with the mean size of 34 $\mu$m and the diluent AIN powders of four different mean sizes.0.12, 9.7, 39.3, 50.5 $\mu$m, were used to prepare green compact. The packing density was fixed to $35 TD\%. The initial pressure of $N_{2}$ and diluent fraction was varied in the range of $1\~10 MPa,\;0.4\~0.7$, respectively. AlN with high purity of $98\% or over and large particle size of about several tens fm can be synthesized by SHS reaction as a consequence of adjusting particle size of AlN dilutent similarly to that of Al reactant. This may be caused by improvement of $N_{2}$ gas permeation to compact after passing the propagation wave. In the case of flaky-shape aluminum used as reactant, instead of granular Al-powder, unstable combustion would be occurred. As the result, irregular propagation of combustion wave and falling-off of maximum temperature would be observed during the reaction.

A Study of The Correlation of The Area Dose with Residual CT Contrast Media and MRI Contrast Media during The Use of General Imaging Automatic Exposure Control System (일반촬영 자동노출제어장치 사용 시 잔존 CT 조영제와 MRI 조영제에 따른 면적선량의 상관성 연구)

  • Hong, Chan-Woo;Park, Jin-Hun;Lee, Jung-Min;Seo, Young-Deuk
    • Journal of the Korean Society of Radiology
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    • v.10 no.8
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    • pp.619-627
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    • 2016
  • The purpose of this study is to investigate the effect of CT contrast agent and MRI contrast agent on the area dose in the body when using automatic exposure control system in general radiography. After making rectangular holes in the center of the abdominal thickness paraffin phantom, CT contrast agent and MRI contrast agent were respectively diluted with physiological saline solution for contrast medium dilution ratio of 10:0, 9:1, 8:2, 7:3, 6:4, 5:5, 4:6, 3:7, 2:8, 1:9, 0:10%. Each experiment was set to 78 kVp, 320 mA, which is the proper condition for KUB photography, and thereafter a total of 30 inspections were made for each dilution ratio using an automatic exposure control device, and the area dose corresponding to the dilution ratio of each contrast agent, Average comparison and correlation analysis were performed on the exposure index. As a result, the CT contrast agent and the MRI contrast agent appeared different in area dose according to the dilution ratio(p<0.05), and as the dilution ratio increased, the area dose increased for CT contrast agent and MRI contrast agent(P<0.05). In each test, the exposure index showed the manufacturer's recommendation of 200-800 EI value, and the exposure index and area dose increased as the area dose increased(p<0.05). In conclusion, CT contrast agent and MRI contrast agent confirmed to increase the area dose by general imaging test using all automatic exposure control device. Therefore, it is considered that it is necessary to perform it after the contrast medium has been excreted sufficiently when using usual imaging test after using the contrast agent in CT and MRI examination.