• Title/Summary/Keyword: 화성법

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Microstructural Analysis of Anodic Oxide Layers Formed in a Boric Acid Solution for Al Electrolytic Capacitor Foils (붕산용액에서 형성된 알루미늄 전해콘덴서용 박의 화성피막 조직분석)

  • Kim, Seong-Gap;Kim, Seong-Su;O, Han-Jun;Jo, Nam-Don;Ji, Chung-Su
    • Korean Journal of Materials Research
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    • v.11 no.4
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    • pp.329-334
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    • 2001
  • Microstructures of barrier-type oxide layers on aluminum was studied by XRD, TEM and RBS. Fer formation of oxide layer. aluminum was anodized in a boric acid solution. The thickness of the oxide film subjected to applied voltage increased linearly at ratio of 1.54nm/V. For oxide layer anodized at 300V, amorphous structure of oxide layer was not transformed after heat treatment at 50$0^{\circ}C$ , while for oxide layers anodized at higher voltages the amorphous structure crystallized into a ${\gamma}$-alumina without any heat treatment. It was also found that the amorphous structure of oxide layer formed at 100V transformed into crystalline structure by electron irradiation. The structure was identified as ${\gamma}$-alumina.

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High-temperature oxidation resistance of Ti-Si-N coating layers prepared by DC magnetron sputtering method (DC magnetron sputtering법으로 제조된 Ti-Si-N코팅막의 내산화성에 관한 연구)

  • Choi, Jun-Bo;Ryu, Jung-Min;Cho, Gun;Kim, Kwang-Ho;Lee, Mi-Hye
    • Journal of Surface Science and Engineering
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    • v.35 no.6
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    • pp.415-421
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    • 2002
  • Ti-Si-N coating layers were codeposited on silicon wafer substrates by a DC reactive magnetron sputtering technique using separate titanium and silicon targets in $N_2$/Ar gas mixtures. The oxidation behavior of Ti-Si-N coating layers containing 4.0 at.%, 10.0 at.%, and 27.3 at.% Si was investigated at temperatures ranging from 600 to $960^{\circ}C$. The coating layers containing 4.0 at.% Si became fast oxidized from $600^{\circ}C$ while the coating layers containing 10.0 at.% Si had oxidation resistance up to $800^{\circ}C$. It was concluded that an increase in Si content to a level of 10.0 at.% led to the formation of finer TiN grains and a uniformly distributed amorphous Si3N4 phase along grain boundaries, which acted as efficient diffusion barriers against oxidation. However, the coating layers containing 27.3 at.% Si showed relatively low oxidation resistance compared with those containing 10.0 at.% Si. This phenomenon would be explained by the existence of free Si which was not nitrified in the coating layers containing 27.3 at.% Si.

Probing the Impact Fee Zone Boundaries Based on Stepwise Scenarios of the Population Grid Cell Buffer Formation (인구격자 셀 버퍼공간 설정에 의한 기반시설부담구역경계 검토방안 연구)

  • Choei, Nae-Young
    • Journal of Korean Society for Geospatial Information Science
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    • v.17 no.4
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    • pp.53-60
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    • 2009
  • Recently, the Korean government has amended the "National Territory Planning Act" by adding criteria to designate the Impact Fee Zone on the basis of the population increase rate. Taking the Dongtan Newtown in Hwasung City as the case, the study first tries to apply a grid analysis method to figure out the cells that exceed the legal population increase rate criteria. Then, the study, for rather a practical purpose, introduces a scenario analysis that tries to envelope the cells into a spatially contiguous groups based on their degrees of stepwise adjacency by cell buffer formation. By overlapping the selected cell groups chosen by such stepwise scenarios over the actual zoning map of land-uses for the vicinity, it seems clear that the chosen areas rationally coincide with those residential blocks and commercial areas with the high population density in the Newtown.

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Developmental Study on the Argentaffin and Argyrophile Cells in the Gastroinestinal Mucosae of Rana nigromaculata (개구리(Rana nigromaculata) 위장관 점막내의 은친화성 세포와 은호성 세포에 대한 발생학적 연구)

  • 김한화;정영화
    • The Korean Journal of Zoology
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    • v.16 no.2
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    • pp.119-126
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    • 1973
  • This experiment was performed in order to study the morphological changes of the argentaffin and argyrophile cells in the gastrointestinal mucosae of Rana nigromaclata during development. The specimens from the stomach and the small intestine at different developmental stages were fixed in neutral 10% formalin, sectioned at a thickness of 3 microns, and impregnated by Masson's method for argentaffin cells and by Bodian's method for argyrophile cells. The results of observation were as follows: 1. In the stomach, the argentaffin cells appeared at XIII stage of metamorphosis and the argyrophile cells at X stage and they rapidly increased in number at XXV stage. 2. In the small intestine, the argentaffin cells appeared at XXV stage of metamorphosis and the argyrophile cells at XVII stage and they rapidly increased in number at XXV stage. 3. The argentaffin and argyrophile cells in the gastrointestinal mucosae, appeared prior to forming gastrointestinal mucosal fold following to development of muscle layer. 4. The rapid numeral increase of the argentaffin and argyrophile cells in the last stage of metamorphosis would be due to ecological changes and differentiations of gastrointestinal mucoae in amphilbia.

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Spatial Aggregation of Contiguous Population Distribution Grid Cells Based on Stepwise Cell Grouping Scenarios (인구분포셀 연접공간 집단화를 통한 기반시설부담구역 검토 사례연구)

  • Choei, Nae-Young
    • Journal of Korean Society for Geospatial Information Science
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    • v.18 no.4
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    • pp.51-60
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    • 2010
  • In 2008, the Development Impact Fee Zoning has been newly amended and added to the existing National Territory Planning Act. Since the beginning of 2009, many local governments nationwide started to adopt the law as a powerful tool to prepare the prescirbed masterplans for the installment of adequate infrastructure and to procure the financial resources to realize the plan. The study, in this context, tried to build gridded population data and analyzed the population cells that exceed the legal criteria of population increase rate required by the law over the case area of Sooyoung-Ri in Hwasung City. The study further probed to group the selected population cells in five specified increasing steps on which the alternative impact fee zones are built. Throughout the process, the study could properly set a reasonable impact fee zone and suggested a practical examples of the final zone specification applicable by the localities.

Spark plasma sintering 소결법에 의해 제작 된 Ti-Al-Si 합금타겟의 물성과 합금타겟을 이용하여 제작한 박막에 관한 연구

  • Lee, Han-Chan;Jeong, Deok-Hyeong;Mun, Gyeong-Il;Lee, Bung-Ju;Sin, Baek-Gyun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.08a
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    • pp.237.1-237.1
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    • 2013
  • Ti 와 Al 은 금속간의 화합물이 내산화성에 우수한 성질을 가지고 있으며 낮은 밀도와 고온에도 큰 변화가 없는 성질을 가지고 있다. 그리하여 내식 및 부식 관련 연구나 고온재료를 필요로 하는 우주, 엔진 제품 등에 많은 연구가 진행되고 있다. 또한 Ti-Al-N 박막은 경도가 우수하여 고속 공구 부품에 널리 사용되고 있으며 최근 Ti-Al-N 에 Si 첨가로 인하여 40 GPa 이상의 고경도와 1,000도 이상의 산화온도를 지닌 나노 혼합물 코팅을 형성 시키는 것으로 알려져 있다. 본 연구에서는 Ti, Al, Si 원분말을 PBM (Planetary Ball Milling) 방법을 사용하여 Ti-Al-Si 혼합분말로 제조하고, 제조된 분말들은 SPS (Spark Plasma Sintering) 공정을 통하여 Ti-Al-Si 합금타겟을 제작하였다. 제작된 Ti-Al-Si 합급타겟을 사용한 Sputtering 공정을 수행하여 Ti-Al-Si 3원계 박막을 증착하였다. 그 결과 기존 Ti (82 ${\mu}m$), Al (32 ${\mu}m$), Si (16 ${\mu}m$) 크기의 원분말들이 PBM (Planetary Ball Milling) 공정 후 Ti-Al-Si (18 ${\mu}m$) 로 입도가 작아진 것을 확인 할 수 있었고, 소결 후 타겟이 99% 이상의 높은 밀도를 가졌으며 원분말의 조성과 동일한 조성을 가진 타겟이 제작되었음을 확인하였다. Ti-Al-Si 타겟의 경도는 약 1,000 Hv 이상의 값을 보였으며, Ti-Al-Si-N 박막의 경우 타겟의 조성과 동일하였고 경도는 약 35 GPa 로 높은 경도 값을 가지는 것을 확인하였다. 내산화 테스트 결과 Ti-Al-Si-N 박막은 1,000도 에서도 박막의 손상이 가지 않았다.

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Determination of the Impact Fee Zone Based on the Grid Analysis of Population Increase (인구증가 분석격자의 공간정보를 이용한 기반시설 부담구역 설정방안)

  • Choei, Nae-Young
    • Journal of the Korean Association of Geographic Information Studies
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    • v.12 no.4
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    • pp.74-83
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    • 2009
  • In September 2008, the Korean government has legally pronounced criteria to designate the Impact Fee Zone on the basis of the population increase rate. Taking the Dongtan Newtown in Hwasung City as the case, the study tries a grid analysis method to figure out the cells that exceed the legal population increase rate criteria. The study then performs scenario analyses that try to envelope the cells into spatially contiguous groups based on their degrees of stepwise adjacency either by the cell buffer or the cell distance standards. By overlapping the selected cell groups over the actual land-use map for the vicinity, it is found that the selected areas reasonably coincide with the blocks of the high population density in the Newtown.

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A Case Study on the Parameters Applied to the Estimation of the Peak Flood in a Small Watershed (소규모유역 첨두홍수량 산정시 적용된 매개변수 사례 연구)

  • Jin Keun Song;Jae Sung Jung
    • Proceedings of the Korea Water Resources Association Conference
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    • 2023.05a
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    • pp.380-380
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    • 2023
  • 기후변화와 도시화에 따른 개발사업으로 인하여 재해 위험성은 날로 증가하고 있다. 이로 인한 재해의 영향을 최소화하기 위해 각종 개발사업 시 자연재해대책법에 따라 사전에 자연재해에 따른 피해를 예방하기 위한 목적으로 재해영향평가 협의가 시행되고 있다. 재해영향평가 협의에서 홍수로 인한 재해예방을 위해 개발사업으로 인한 홍수유출 증가량 검토하고 저감 대책을 제시하게 된다. 이중 소규모 재해영향평가는 면적 5천m2 이상 5만m2 미만의 개발사업을 대상으로 실시되고 있으며, 이를 위한 첨두홍수량 산정 방법으로는 합리식, clark단위도법 등이 사용되고 있다. 소규모 유역의 첨두홍수량을 합리식, 단위도법 등으로 산정할 경우 도달시간이 매우 짧아 홍수량이 과다하게 산정된다. 이를 방지하기 위해 합리식에서는 강우지속기간을 늘리기 위해 일정 유입시간을 고려하고 있으며, 단위도법에서는 유역반응시간을 조정하고 있다. 기존의 연구에서 clark단위도법에서 저류상수 매개변수 보정을 7 ~ 10분으로 적용하도록 하고 있다. 본 연구에서는 화성, 양주, 청주지역의 소규모 재해영향평가협의 대상인 공장부지 조성사업의 홍수량 산정시 저류상수 매개변수 조정 사례를 조사하고 그 중 유역의 상황변화를 고려하지 않고 개발 후 매개변수 조정을 10분으로 적용한 10개 사업을 대상으로 선정하였다. 본 연구에서는 개발 후 매개변수 보정량을 10분을 7분으로 변경하여 홍수량을 산정하였다. 10개 사업 홍수량 산정결과 「재해영향평가등의 협의 실무지침 (2021.01, 행정안전부)」에서 제시하는 소유역 비홍수량의 범위인 25 ~ 35m3/s/km2에 8개 사업이 만족되었고, 2개 사업은 개발 후 비홍수량이 제시 범위를 다소 초과하였고, 홍수량의 증가는 4.7 ~ 16.3% 범위로 나타났다. 소규모 유역에서 저류상수 보정량이 홍수량 산정에 미치는 영향이 큰것을 감안하면 유역의 도시화등 상태변화 비율 및 소유역 면적별로 매개변수 조정량을 정량화하는 추가 연구가 필요하다.

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The Non-Appropriation Principle and Corpus Juris Spatialis (비전유원칙과 우주법(Corpus Juris Spatialis))

  • Kim, Han-Taek
    • The Korean Journal of Air & Space Law and Policy
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    • v.35 no.1
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    • pp.181-202
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    • 2020
  • The Non-Appropriation Principle was stipulated in the OST and the MA. However the MA, creating CHM in international law for the first time, attempted to further limit the prohibitions to include ownership of resources extracted from celestial bodies, its rejection by the U.S. and most of the international spacefaring community prevented it from serving as a binding international treaty. Individuals or private enterprises intending to perform space exploitation must receive approval from the nation and may not appropriate outer space or celestial bodies. In the course of this space activity, each party will be liable. Articles 6 and 7 of the OST and the Liability Convention of 1972 deal with matters concerning those problems. The CSLCA of 2015 and Luxembourg Space Resources Law of 2017 allows States to provide commercial exploration and use of space resources to their own nationals and to companies operated by other countries within their territory. These laws do not violate Article 2 of the OST. In the case of the CSLCA of 2015, the law clearly states that it cannot claim ownership, sovereignty or jurisdiction over certain celestial bodies. Even if scholars claim that the U.S. CSLCA and Luxembourg Space Resources Law violate the non-appropriation principle of the OST, they cannot prevent these two countries from extracting the space resources on "the first come, first served" basis. The legal status of outer space including the moon and other celestial bodies is res extra commercium, like the high seas, where the fishing vessels from each country catch and sell fish without occupying the sea. Major space-faring nations must push for the adoption of an international regulatory committee which will oversee applications and issue permits based on a set of robust, modern, and forward-thinking ideals that are best equipped to govern and protect outer space as individuals, businesses, and nations compete to commercialize space through mining and the extraction of space-based resources. The new Corpus Juris Spatialis on the development of space resources, whether it is a treaty or a soft law such as recommendation and declaration, in the case of the Moon and Mars, will cover a certain amount of area to develop, and the development period by the states should be specified.

In vitro evaluation of the wear resistance of provisional resin materials fabricated by different methods (제작방법에 따른 임시 수복용 레진의 마모저항성에 관한 연구)

  • Ahn, Jong-Ju;Huh, Jung-Bo;Choi, Jae-Won
    • The Journal of Korean Academy of Prosthodontics
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    • v.57 no.2
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    • pp.110-117
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    • 2019
  • Purpose: This study was to evaluate the wear resistance of 3D printed, milled, and conventionally cured provisional resin materials. Materials and methods: Four types of resin materials made with different methods were examined: Stereolithography apparatus (SLA) 3D printed resin (S3P), digital light processing (DLP) 3D printed resin (D3P), milled resin (MIL), conventionally self-cured resin (CON). In the 3D printed resin specimens, the build orientation and layer thickness were set to $0^{\circ}$ and $100{\mu}m$, respectively. The specimens were tested in a 2-axis chewing simulator with the steatite as the antagonist under thermocycling condition (5 kg, 30,000 cycles, 0.8 Hz, $5^{\circ}C/55^{\circ}C$). Wear losses of the specimens were calculated using CAD software and scanning electron microscope (SEM) was used to investigate wear surface of the specimens. Statistical significance was determined using One-way ANOVA and Dunnett T3 analysis (${\alpha}=.05$). Results: Wear losses of the S3P, D3P, and MIL groups significantly smaller than those of the CON group (P < .05). There was no significant difference among S3P, D3P, and MIL group (P > .05). In the SEM observations, in the S3P and D3P groups, vertical cracks were observed in the sliding direction of the antagonist. In the MIL group, there was an overall uniform wear surface, whereas in the CON group, a distinct wear track and numerous bubbles were observed. Conclusion: Within the limits of this study, provisional resin materials made with 3D printing show adequate wear resistance for applications in dentistry.