• Title/Summary/Keyword: 합성 ferrite

Search Result 119, Processing Time 0.031 seconds

Microwave Absorption of Ferrite Powders by Wet-Direct Synthesis (습식직접합성 Ferrite 분말의 전파흡수능)

  • 남경호;이경희;이병하
    • Journal of the Korean Ceramic Society
    • /
    • v.28 no.11
    • /
    • pp.843-850
    • /
    • 1991
  • There is a growing demend for absorptive electromagentic shielding materials for wide band frequency application. In this study, the absorber which consists of a rubber plus Ni-Zn ferrite which have been prepared by direct-wet method. A rubber ferrite composite for electromagnetic shielding, it is most importan facter the homogeneous ultra fine size and high dispersitive ferrite powder. Direct-wet method and solid-solid reaction method for preparing of ultra fine ferrite powder was used. It has been experimentally verified that the powder which prepared by direct-wet method was very fine and almost same size spherical powder, the composite ferrite have excellent electromagnetic wave absorption in X-band.

  • PDF

Effects of $SiO_2$ and Seed on Ba-ferrite Synthesized by Molten Salt (용융염법으로 합성한 Ba-ferrite의 $SiO_2$ 및 Seed 첨가 효과)

  • 김영근;이승관;김현식;오영우
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1996.11a
    • /
    • pp.326-329
    • /
    • 1996
  • In order to synthesize Ba-ferrite fine particles by molten salt method and inhibit the abnormal grain growth of sintered specimen, KCI anti NaCl were added to basic composition to 50% by weight, and added 1 male% of $SiO_2$ to control the shape of Ba-ferrite particles. $H_{c}$ and $M_{r}$ were decreased when F $e^{3+}$ was substituted with $Co_{2+}$ and $Ti_{4+}$ from x=0 to x=1.0 in $BaFe_{12-2x}$ $Ti_{x}$ $Co_{x}$ $O_{19}$ , and 1 mole% $SiO_2$ increased the size but shortened c-axis of hexagonal ferrite. Seeds added in Ba-ferrite particle effected inhibition of abnormal grain growth during sintering.ing.g.

  • PDF

Magnetic Characteristics of BaFe12-2xCoxTixO19 Particles Prepared by Sol-gel Synthesis (졸-겔 합성에 의한 BaFe12-2xCoxTixO19 미립자의 자기적 특성)

  • 최현승;정지형;박효열;김태옥
    • Journal of the Korean Ceramic Society
    • /
    • v.40 no.1
    • /
    • pp.62-68
    • /
    • 2003
  • Ba-ferrite particles added with Co and Ti, which were known well the additives for the control in coercivity, were synthesized by sol-gel method. In the range 90 to 120 minute reaction time, a stable sol solution which showed no change with temperature, pH, viscosity and aging time. After dried and heat treatment of sol solution, Ba-ferrite phase formed at $700^{\circ}C$ with Differential Thermal Analysis(DTA) and X-Ray Diffractometer(XRD) measurement. The crystallinity became to be better with increasing the temperature. It were showed by Scanning Electron Microscopy(SEM) that Ba-ferrite increased to particle sizes as increasing heating temperature and obtained of narrow particles size distribution. Also, magnetic characteristics of Ba-ferrite powders Co and Ti added were observed by a Vibrating Sample Magnetometer(VSM). Saturation magnetization$(M_s)$ was not much changed, however. the coercivity$(H_c)$dramatically dropped with addition of Co and Ti.

Preparation of Ultrafine Mn-Zn Ferrite by Direct-Wet Synthesis and a Study of Magnetic Properties (습식직접 합성에 의한 초미분 Mn-Zn Ferrite의 합성과 자성특성에 관한 연구)

  • 이경희;이병하;허원도;황우연
    • Journal of the Korean Ceramic Society
    • /
    • v.28 no.10
    • /
    • pp.757-766
    • /
    • 1991
  • These powder properties were investigated and prepared of ultrafine Mn-Zn ferrite powder by Direct-wet process from variation of oxidation condition. H2O2 oxidation the products were ultrafine spherical particles of about 400${\AA}$ in diameter and superparamagnetics. H2O2 and Air oxidation, Coexistance ultrafine spherical particles of about 400${\AA}$ and cubic particles of about 1000${\AA}$. The products were constructed of superparamagnetic and ferromagnetic particles, and Magnetization were about 30 emu/g. Air Oxidation, Above 6 hr Air 120 ι/hr and 4 hr of Air 180 ι/hr were uniform cubic particles of above 1000${\AA}$. The products were ferromagnetic particles and Magnetization of above 45 emu/g.

  • PDF

Conditions for the Formation of Ba-Ferrite by Hydrothermal Synthesis (수열합성에 의한 Ba-Ferrite의 형성조건)

  • 이경희;이병하;윤갑중
    • Journal of the Korean Ceramic Society
    • /
    • v.22 no.5
    • /
    • pp.61-65
    • /
    • 1985
  • This stud deals with the conditions for the Formation of Ba-Ferrite by Hydrothemal synthesis Suspensions Containing either iron(III) hydroxide or hydroxide oxide and barium ians were subjected to autoclavings at various temperatures from 150 to 30$0^{\circ}C$. A ferromagnetic precipitate BaO.$6Fe_2O_3$ consisting of hexagonal plate-like particle was obtained by suitable combination of temperature and concentration of KOH

  • PDF

Stepwise Production of Syngas and Hydrogen from Methane on Ferrite Based Media Added with YSZ (YSZ 첨가 페라이트 매체상에서 메탄으로부터 합성 가스 및 수소의 단계적 생산)

  • Je, Han-Sol;Cha, Kwang-Seo;Kim, Hong-Soon;Lee, Young-Seak;Park, Chu-Sik;Kim, Young-Ho
    • Journal of Hydrogen and New Energy
    • /
    • v.21 no.1
    • /
    • pp.50-57
    • /
    • 2010
  • Stepwise production of syn-gas and hydrogen from methane on ferrite based media added with yttria-stabilized zirconia (YSZ) was carried out using a fixed bed infrared reactor. In this study, all M-ferrite (M=Co, Cu, Mn and Ni) media were prepared by co-precipitation method, and there the YSZ was added as a binder to improve thermal stability, reactivity, and resistance against carbon deposition. Most of the ferrite media containing YSZ showed the good redox property for temperature programmed reduction/oxidation (TPR/O) tests. Notably, the Cu-substituted ferrite medium with YSZ showed the great resistance against carbon deposition as well as the good reactivity for the stepwise production of syngas and hydrogen. Furthermore, it also showed the good durability without significant deactivation during five repeated cyclic tests.

Preparation of Zeolite Coated with Metal-Ferrite and Adsorption Characteristics of Cu(II) (금속 페라이트가 코팅된 제올라이트의 제조와 Cu(II)의 흡착 특성)

  • Baek, Sae-Yane;Nguyen, Van-Hiep;Kim, Young-Ho
    • Applied Chemistry for Engineering
    • /
    • v.30 no.1
    • /
    • pp.54-61
    • /
    • 2019
  • In this study, a magnetic adsorbent was synthesized by growing ferrite nanoparticles substituted with metals (Me = Co, Mn, Ni) on zeolite 4A for the efficient separation of waste adsorbents present in the solution after the adsorption of Cu(II). The metal ferrite grown on the surface of zeolite was prepared by solvothermal synthesis. Characteristics of the magnetic adsorbent were analyzed by X-ray diffractometer (XRD), scanning electron microscopy (SEM) and physical property measurement system (PPMS). The saturation magnetization of the A type zeolite coated with Co-ferrite (CFZC) was the highest at 5 emu/g and the Cu(II) adsorption performance was also excellent. The adsorption results of Cu(II) on CFZC were well fitted by the Langmuir model at 298 K. Also, the adsorption of Cu(II) on CFZC follows a pseudo-second order kinetic. The Gibbs free energy values (${\Delta}G^0$) ranging from -4.63 to -5.21 kJ/mol indicates that the Cu(II) adsorption is spontaneous in the temeprature range between 298 and 313 K.