• Title/Summary/Keyword: 한국용출실험

Search Result 537, Processing Time 0.038 seconds

Solvent Leaching Characteristics of Dark Brownish Pigment from Activated Charcoal used in Decolorization of Crude Polysaccharide from Auricularia auricula (흑목이 버섯 다당류의 탈색에 사용된 활성탄으로부터 흑갈색 색소의 용매 침출 특성)

  • Kim, Hyeon-Min;Hur, Won;Lee, Shin-Young
    • Food Engineering Progress
    • /
    • v.13 no.4
    • /
    • pp.262-268
    • /
    • 2009
  • A dark brownish pigment in the crude polysaccharide from Auricularia auricula was adsorbed by activated charcoal. The leaching of the pigment adsorbed on activated charcoal and regeneration of activated charcoal used was investigated with eight kinds of solvents. The highest leaching capacity was obtained with the alkaline solution (KOH). The optimum volume of 1 M KOH solution per activated carbon was 45 mL/g, and the treatment for 10 min during single stage leaching was sufficient to achieve the leaching equilibrium. Second-order kinetic model provided the best fitting for the pigment leaching. The pigment leaching capacity of 88.9% was obtained by seven times of treatment with 1 M KOH solution at 25$^{\circ}C$, while at 95$^{\circ}C$, leaching capacity of 82.6% was achieved with single stage alone showing the significant increase of leaching capacity with increasing temperature. The regenerated activated charcoal was nearly as effective as fresh activated charcoal in pigment adsorption of crude polysaccharide from Auricularia auricula.

Long-term teaching Characteristics of Hexavalent Chromium Contaminated Soils Treated with Phosphate and Chromium Reducing Agent (크롬환원제와 인산염으로 처리된 6가 크롬 오염토양의 장기용출 특성)

  • Lee Eui-Sang
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.7 no.3
    • /
    • pp.448-452
    • /
    • 2006
  • This study was performed to evaluate the long-term teachability of the stabilized hexavalent chromium contaminated soils treated with chromium reducing agent and soluble phosphate. The study shows that $Cr^{6+}$ in the leachate was little detected and the remaining $PO_4-P$ concentration kept below 0.1 mg/L due to the formation of geochemically stable hexavalent chromium phosphate minerals from the reactions of labile soil $Cr^{6+}$ forms with the added soluble phosphate salt and chromium reducing agent. The results provide evidence for the potential use of the immobilization technique for the hexavalent chromium contaminated soil remediation in the near future.

  • PDF

남해안의 해수 및 해저퇴적물 용출액과 적조생물 성장과의 관계 연구

  • Lee, Sam-Geun;Lee, Yeong-Sik;Im, Wol-Ae;Jo, Eun-Seop
    • Proceedings of the Korean Environmental Sciences Society Conference
    • /
    • 2007.05a
    • /
    • pp.447-449
    • /
    • 2007
  • 유해성 적조생물인 C. polykrikoides에 대한 해역별 적조잠재력 평가를 위하여 유해성 적조가 자주 발생하는 남해안의 소리도 부근해역, 광양만, 남해도 주변해역, 거제만, 부산연안의 해수 및 해저퇴적물을 채집하여 배양실험을 실시하였다. 실험을 위한 기본배지는 f/2배지에서 배양조건은 온도 $20^{\circ}C$, 염분 34, 조도 2000Lux, 그리고 실험생물은 대수증식기의 C. polykrikoides를 $300cells/m{\ell}$접종하였다. 해역별 해수에 대한 적조생물 성장은 광양만에서 가장 높아 적조발생 잠재력이 가장 높았고, 다음은 부산 기장, 거제, 남해연안 순서로 성장이 높게 나타났으며, 질산성 질소 농도는 $0.35{\sim}24.74{\mu}M$ 범위로 적조생물의 성장과 같은 순서를 나타내었다. 한편 해저 퇴적물 용출액은 적조생물의 성장을 현저히 촉진시켰으며, 남해도 미조연안의 해저 퇴적물 용출액에서 적조발생 잠재력이 가장 높았고, 부산 형제도연안, 광양만, 거제만, 소리도연안의 해저퇴적물 순서로 적조생물의 성장을 촉진시키는 결과를 나타내었다. 그리고 적조생물의 성장은 인산염의 농도에 의해서 성장이 결정되었던 것으로 추정되며, 용출된 인산염의 농도 $1.59{\sim}10.39{\mu}M$ 범위로 남해 미조연안, 부산 형제도 연안, 광양만, 거제만, 소리도 연안 순서로 C. polykrikoides의 성장과 같은 순서로 나타났다.

  • PDF

Leaching Behavior of Heavy Metals from an Ore Containing High Concentration as Utilizing Acidithiobacillus ferrooxidans and Acidithiobacillus thiooxidans (Acidithiobacillus ferrooxidans와 Acidithiobacillus thiooxidans를 활용한 고농도 비소 함유 광석 내 중금속 용출 거동 연구)

  • Kim, Gahee;Kim, Rina;Kim, Kwanho;You, Kwang-suk
    • Resources Recycling
    • /
    • v.30 no.2
    • /
    • pp.14-23
    • /
    • 2021
  • To investigate the potential for leaching of heavy metals by bacteria from ores stacked on actual mining sites, leaching tests of a complex metallic ore (Pb-Zn-As ore) were conducted over 60 days using acidophile bacteria Acidithiobacillus ferrooxidans and Acidithiobacillus thiooxidans under initial acidic conditions. Initially, a small amount of heavy metals was leached due to the initial acidic conditions. After 20 days, when A. thiooxidans in the reactor was adapted to the ore, the amount of leached heavy metals rapidly increased; the concentrations of leached arsenic, iron, and zinc reached a maximum of 2800, 3700, and 2500 mg/L, respectively. On the other hand, in the presence of A. ferrooxidans or in the control test without bacteria, heavy metals, except zinc, were barely detected in leaching. Through this study, it was confirmed that (i) bacteria could leach heavy metals at mining sites under acidic conditions and (ii) leaching of heavy metals from a high arsenic-containing ore by A. thiooxidans was more significant than that by A. ferrooxidans.

Bioleaching of Galena by Indigenous Bacteria at Room Temperature (상온에서 토착박테리아를 이용한 방연석의 용출 특상)

  • Park, Cheon-Young;Kim, Soon-Oh;Kim, Bong-Ju
    • Journal of the Mineralogical Society of Korea
    • /
    • v.23 no.4
    • /
    • pp.331-346
    • /
    • 2010
  • This study was carried out to leach valuable metals from galena using indigenous bacteria with no optimum pH conditions at room temperature. Even in these conditions, the rod-shaped indigenous bacteria, ranging from $0.4{\times}0.2{\mu}m$ to $0.5{\times}1.7{\mu}m$, were attached to the surface of the galena. For the 19 days of the bioleaching experiment, the content of Ph, Fe, Zn ions was found to be 347, 222 and 1.7 times higher than that of the control leaching agent, respectively. Numerous hexagonal column crystals were observed on the surface of galena. Those crystals may be formed from the biooxidation of galena by the indigenous bacteria. XRD analysis showed the peaks of anglesite observed in the bioleached galena. It is expected that more valuable elements can be leached out of the galena, if the bacteria is used under optimum pH and temperature conditions in future bioleaching experiments.

Comparative Study of Dissolution Properties of Immediate-release and Controlled-release Type Vitamin C Tablets (속방형 및 용출조절형 비타민 C 정제의 용출 특성 비교 분석)

  • Yang, Hyo-Jin;Ryu, Na-Hee;Yang, Joo-Hong;Hong, Sun-Ho;Lee, Yeonkyung;Cho, Yang-Hee
    • Journal of Food Hygiene and Safety
    • /
    • v.37 no.2
    • /
    • pp.114-120
    • /
    • 2022
  • In this study, a comparative dissolution experiment was conducted between an immediate-release and a controlled-release vitamin C tablet applied with a technology to control the dissolution of vitamin C to maintain the vitamin C level in the human body. In order to confirm the dissolution rate (%) of vitamin C tablets, HPLC determination was conducted based on the dissolution test methods in the 'Korean Pharmacopoeia (No. 2020-88),' 'Guidelines on Specifications of Dissolution Tests for Oral dosage Forms,' and 'Standard and Specifications for Health Functional Foods (No. 2020-63)' from Ministry of Food and Drug Safety (MFDS). In addition, the dissolution pattern between the immediate-release tablet and the controlled-release tablet was comparatively analyzed. The analysis result confirmed that the immediate-release vitamin C tablet was 100% dissolved after 45 minutes, while the controlled-release vitamin C tablet was 100% dissolved after 480 minutes (8 hours). Furthermore, the dissolution rate (%) at 60 minutes was slower than that of the immediate-release vitamin C tablet. Based on these results, this study confirmed that the dissolution rate (%) test and development of controlled-release tablets containing vitamin C as the main component a re possible.

Studies of Egg-Shell Calcium (I) - The Effects of Elution Condition of Egg-Shell Calcium on Elution Quantity and Ionization Rate - (난각칼슘에 관한 연구(I) - 난각칼슘의 용출 조건이 용출량과 이온화율에 미치는 영향 -)

  • 이숙경;박종호
    • Journal of Food Hygiene and Safety
    • /
    • v.17 no.4
    • /
    • pp.183-187
    • /
    • 2002
  • This study was performed to investigate the utility of egg-shell calcium with calcium soak egg-shell in the vinegar. We compared examination eluted quantity with ionization rate in each condition. The results were as follows. 1 The degree of elution and ionization of calcium was proportional to the amount of vinegar and added acetic acid in the vinegar for elution. And ionization rate was the most high in case of 200 ml vinegar volume. 2. fluted quantity were increased in the rank order to 4$0^{\circ}C$ > 3$0^{\circ}C$ > 2$0^{\circ}C$ by temperature but the rank order of ionization of calcium was 3$0^{\circ}C$ > 2$0^{\circ}C$ > 4$0^{\circ}C$ by temperature. The occurrence of unacceptable flavor resulting from the immersion at 4$0^{\circ}C$ was another obstacle to adopt. 3. Eluted quantity and ionization rate of the egg-shell calcium were appeared excellent in case of the brewage vinegar at ventilation condition. The case of brown rice vinegar did not show a considerable difference, but eluted quantity and ionization rate were appeared the most excellent to the other sample. 4. The optimum condition for elution and ionization of the egg-shell calcium was appeared Immersing egg-shells in the brewed rice-bran vinegar at 3$0^{\circ}C$ for three days.

The Mineralogical and Chemical Characteristics of Slag from Kazakhstan and Leaching of Cu and Fe (카자흐스탄 구리 슬래그의 광물학적, 화학적 특성 및 구리와 철의 용출 특성)

  • Kim, Bong-Ju;Cho, Kang-Hee;Shin, Seung-Han;Choi, Nag-Choul;Park, Cheon-Young
    • Journal of the Mineralogical Society of Korea
    • /
    • v.28 no.1
    • /
    • pp.17-28
    • /
    • 2015
  • In order to study the mineralogical and chemical characteristics of copper slag, optical microscopy, SEM/EDS, EPMA, AAS and XRD analyses were carried out. In addition, sulfuric acid leaching experiments were performed to investigate the potential of the slag as a copper resource. It was confirmed that fayalite, chromite, bornite and chalcopyrite were contained in the slag. The slag mainly consisted of acicular fayalite and skeletal lath -euhedral chromite crystals. Also a very large amount of bornite and chalcopyrite grains were contained in the slag. The content of Fe and Cu in the slag was 18.37% and 0.93%, respectively. As a result of sulfuric acid leaching experiments, the leaching rates of Cu and Fe were increased through decreasing the slag particle size, increasing the sulfuric acid concentration and the leaching temperature. The maximum efficiency of Cu and Fe leaching were obtained under the conditions of particle size of 32 mesh, sulfuric acid concentration of 2.0 M, and leaching temperature of $60^{\circ}C$. Accordingly, it is expected that the slag could be available as a potential and alternative resource of metallic copper.

Evaluation for Contents of Contaminants and Leaching Characteristics of Bottom Ash (바텀애쉬의 유해물질 함량 측정 및 용출특성 평가연구)

  • Koh, Taehoon;Lee, Sungjin;Shin, Minho;Kim, Byongsuk;Lee, Jeakeun;Lee, Taeyoon
    • Journal of the Korean GEO-environmental Society
    • /
    • v.11 no.6
    • /
    • pp.77-83
    • /
    • 2010
  • In this study, we tried to determine any detrimental effects on water quality when bottom ash obtained from a coal-fired power plant intended to be used as a fill material in construction sites. Physical-chemical properties of bottom ash were determined using proximate analysis, elemental analysis, XRD, and XRF. Classification of bottom ash as a waste material and soil contamination due to the use of bottom ash were performed by Korea waste standard leaching test and soil toxicity test, respectively. Results of leaching tests were compared to the regulations for water quality and groundwater quality and no harmful effects on water quality were found. Most of heavy metals in leachate were below detection limits but trace amount of $Cr^{6+}$ was found. However, concentration of $Cr^{6+}$ was below the regulation criteria. Column leaching tests indicated that concentrations of Pb and Zn were slightly higher than regulations but below regulations within 1 PVE, but concentrations of sulfate were 10 times higher than regulation and thus, the required time to reach regulation was almost 8 PVE.

pH변화에 따른 광미와 오염된 토양에 함유된 중금속 용출특성

  • 이평구;강민주;최상훈
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
    • /
    • 2003.04a
    • /
    • pp.141-144
    • /
    • 2003
  • 청양 및 서보광산에서 채취한 광미 및 오염된 토양에 대한 산성비를 고려한 용출실험 결과, 아연, 카드뮴 및 망간 pH 6.2-5.8, 철 pH 5.2-3.2, 코발트 pH 4.4-3.2, 구리 pH 3.2-3.0, 납과비소 pH3.0-3.5의 용출조건에서 최초로 각 원소의 용출이 발생하였다. 반응용액의 최종 pH5.0-1.5사이에서 용출되는 중금속은 이온교환형태 및 탄산염광물형태와 수반된 것이 용해된 것이다. 반응용액의 최종 pH1.5이하에서 용출되는 중금속은 철과 밀접하게 수반된 것으로 해석되었다. 청양광산과 서보광산의 광미가 pH2.0이하로 유지되는 경우가 발생한다면, 청양광산은 비소(최대 6,006$\mu\textrm{g}$/g), 아연(최대 2,503$\mu\textrm{g}$/g) 및 납(최대 29,638$\mu\textrm{g}$/g), 서보광산은 납(최대 2,258$\mu\textrm{g}$/g)과 111소(최대 874$\mu\textrm{g}$/g)의 오염확산이 크게 우려되며, 이 결과는 광미에 대한 환경복원이 필요한 것을 지시한다. 서보광산의 오염된 토양은 pH3.0까지의 산성비와 반응하는 경우에는 중금속의 오염확산이 거의 우려되지 않으며, pH3.0이하의 강산 용액과 반응한다면 아연의 오염확산이 우려된다.

  • PDF