• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2017.05a
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• pp.843-848
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• 2017

Metal exposed to high temperature/high pressure/oxidizer-rich environment may cause rapid oxidation(ignition and combustion). In this study, a DC power supply test system that controls the temperature of specimen by supplying power to the specimen was constructed and after simulating the high temperature/stagnation/oxidizer-rich environment, the metal oxidation and ignition of STS series metal materials were evaluated. As a result, we was confirmed that the deformation (discoloration) of the selected material, the change in the surface roughness and the peeling of the metal surface were observed, and that the weight and the specimen thickness were changed. The most oxidized specimen was STS 304 and the less oxidized specimen was XM-19.

• Proceedings of the KIEE Conference
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• 2007.07a
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• pp.286-287
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• 2007

본 논문에서는 최근 유체소자 재료로써 많이 사용되고 있는 polymethyl methacrylate (PMMA)의 레이저 직접식각에 관한 특성을 나타내었다. 식각을 위한 레이저 원으로 기본파가 1064 nm, 반복율이 10 Hz인 Nd:YAG 레이저의 4고조파 성분 ($\lambda$=266 nm)을 사용하였다. X-Y-Z 축으로 이동 가능한 스테이지의 수평 이동속도를 변화시키며, 표면으로 조사되는 펄스 수를 제어하였다. 식각 후 광학현미경으로 식각 단면을 조사하여 식각 깊이와 폭을 측정하였다. 측정된 식각 깊이로부터 식각률을 계산하고, 그 값과 레이저 빔 밀도와의 관계를 알아보았다. 그 결과 시료 표면에 조사되는 레이저 빔 밀도의 로그값과 선형적인 관계를 갖는 것을 확인할 수 있었다. 또한 주사전자현미경을 이용하여 채널 형상 및 채널 내벽을 관찰하였다. 마이크로 채널 내벽에 식각 과정에서 발생한 생성물의 제거를 위해, 레이저 식각과 함께 질소가스 블로잉을 해주었다. 질소 블로잉 압력 1500 torr에서 식각 잔유물이 제거된 내벽을 볼 수 있었다. 실험결과, Nd:YAG 4고조파를 이용하여 PMMA 기판상에 유체 이동을 위한 마이크로 채널을 형성시킬 수 있었다.

• Journal of the Korean Society of Propulsion Engineers
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• v.26 no.3
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• pp.43-53
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• 2022

In this study, analysis of the flow characteristics of pintle-controlled nozzle with split-line TVC system and the thrust performance prediction was performed. The numerical computation was verified by comparing the thrust coefficient derived from the analysis results with the experimental data. By applying the same numerical analysis technique, the flow characteristics of nozzle were confirmed according to operating altitude, pintle stroke position and TVC angle with the 1/10 scale. As the TVC angle increased, thrust loss occurred and the tendency of AF was different depending on the position of the pintle stroke. Based on the analysis results, the relation of thrust coefficient was derived by applying the response surface methods. The thrust performance model with a slight difference of 1.2% on average from the analysis result was generated.

• The Journal of Engineering Geology
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• v.22 no.1
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• pp.83-94
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• 2012

Slopes are commonly formed both above and below roads located in mountainous terrain and along riversides. The Buk-sil site, a cut slope formed below the road, collapsed in October, 2010. A field investigation determined the causes of failure as improper drainage of valley water from the slope above the road and direct seepage of road-surface water. These factors may have accelerated the collapse via complex interaction between water and sub-surface structures such as bedding. Projection analysis of the site showed the possible involvement of plane, wedge, and toppling failure. Safety factors calculated by Limit Equilibrium Analysis for plane and wedge failure were below the standard for wet conditions. The wetness index, analyzed using topographic factors of the study area, was 9.0-10.5, which is high compared with the values calculated for nearby areas. This finding indicates a high concentration of water flow. We consider that water-flow control on the upper road is crucial for enhancing slope stability at the Buk-sil site.

• Journal of Conservation Science
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• v.19
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• pp.5-18
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• 2006

The Mireuksaji stone pagoda of the Iksan was built in Muwang King of Baekjae Kingdom and has maintained its present status through several rebuilding process. Recently, the structural unbalance of the pagoda has worsened, so for scientific maintenance recovery of its original pagoda form, the pagoda is under dismantling process. The original form of this pagoda is being presumed to be a plane square pagoda of nine stories, though only a portion of six stories remains until today. The destroyed part from collapse was liked in insecure pagoda form by Japanese in year of 1915. On the surface of the stone which has gone through the present time, efflorescence appeared as precipitation substance over crusted and due to this phenomenon, the structure and color of thee original stone haven't been preserved. Therefore, quantitative analysis on its kind, emitted status and contamination type of secondary inorganic contamination substance of the over crusted surface were analyzed. Also through reaction experiments, contamination type was defined and tests have been applied to find the requirements that will wash out the contaminants. The result of this study will provide the base of quantitative analysis on the kind of inorganic contamination of the surface of stone assets, and it shall also contribute to the application of scientific maintenance recovery of surface cleaner for efflorescence.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2017.05a
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• pp.162-162
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• 2017

AlCrN 코팅은 높은 경도, 낮은 표면 조도 등의 상온에서의 우수한 기계적 특성 이외에 고온에서 안정한 합금상의 형성으로 인하여 우수한 내열성을 보이는 코팅이며, Si을 첨가하여 나노복합구조를 갖는 AlCrSiN 코팅은 고경도 특성을 나타내는 나노결정립과 고내열성을 나타내는 $Si_3N_4$ 비정질이 동시에 존재함으로써 뛰어난 고온 특성까지 보유하여 공구 코팅으로의 적용 가능성이 크다. 본 연구에서는, 가혹화된 공구사용 환경 대응 하는 더욱 우수한 내마모성 및 내열성을 보이는 코팅막을 개발하기 위해 AlCrN/AlCrSiN 이중층 코팅을 합성하였다. 합성된 코팅의 구조 및 물성을 분석하기 위해 field emission scanning electron microscopy(FE-SEM), nano-indentation, atomic force microscopy(AFM) 및 ball-on-disk wear tester를 사용하였다. 내열성을 확인하기 위하여 코팅을 furnace에 넣어 500, 600, 700, 800, 900도에서 30분 동안 annealing한 후에 nano-indentation을 사용하여 경도를 측정을 하였다. 5:5, 7:3, 9:1의 두께 비율로 AlCrN/AlCrSiN 이중층 코팅을 합성하였으며 모든 코팅의 두께는 $3{\mu}m$로 제어되었다. AlCrN 코팅층의 두께가 증가할수록, 이중층 코팅의 경도 및 내마모성은 점차 향상되었지만 코팅의 밀착력은 감소하였다. 일반적으로 AlCrN 코팅은 상대적으로 높은 잔류응력을 갖고 있으므로, AlCrN 층의 두께비율이 증가함에 따라 코팅내의 잔류응력이 높아져 코팅의 경도는 증가하고 밀착특성은 낮아진 것으로 판단된다. AlCrSiN 상부층 공정시 기판 바이어스 전압을 -50 ~ -200V 로 증가시키면서 이중층 코팅을 합성하였다. XRD 분석 결과, 공정 바이어스 전압이 증가함에 따라 AlCrSiN 상부층은 점차 비정질화 되었고, 코팅의 경도와 표면 특성이 향상되는 것을 확인하였다. 이러한 특성 향상은 높은 바이어스 인가가 이온 충돌효과의 증가를 야기시켰으, 이로 인해 치밀한 코팅층 합성에 의한 결과로 판단된다. AlCrN/AlCrSiN 이중층 코팅을 어닐링 한 후 경도 분석 결과, -150, -200V에서 합성한 코팅은 900도 이상에서 26GPa 이상의 높은 경도를 보인 것으로 보아 우수한 내열성을 갖는 것으로 확인 되었다. 이는 AlCrSiN 상부층의 높은 Si 함량 (11at.%) 으로 인한 충분한 $Si_3N_4$ 비정질상의 형성과, 고바이어스 인가로 인한 AlCrN 결정상과 $Si_3N_4$ 비정질상의 고른 분배가 코팅의 내열성을 향상시키는데 기여를 한 결과로 판단된다.

• Journal of Conservation Science
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• v.36 no.5
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• pp.368-382
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• 2020

It was confirmed that a white porcelain figurine in underglaze iron was damaged after exhibition. This study analyzes the current state of salt damage on the artifact and identifies the factors contributing to its deterioration by examining the material characteristics of the artifact and exhibition environment. The analysis will thus assist in preparing a conservation scheme for artifacts. The crystallized carbonate on the surface of the white porcelain figurine is a water-soluble alkali salt with high hygroscopicity and high solubility in water. This solubility increases as the temperature increases. The figurine was low-fired at approximately 1000℃. A lead glaze was applied, and thin cracks were formed on the glazed surface, indicating poor surface properties. Our analysis suggested that the showcase used in the exhibition likely created a moist environment resulting from condensation, as it was exposed to high temperature and relative humidity, particularly in comparison to the exhibition room where the temperature was regulated using an air conditioner. In addition, the artifacts in the showcase were exposed to sudden changes in temperature and relative humidity as the air conditioner was repeatedly turned on and off. Therefore, it can be deduced that the soluble salt remaining on the white porcelain figurine moved toward the surface of the relatively weak glaze as a result of the temperature, and the crystallized salt exacerbated surface damage as the moisture evaporated in a dry environment.

• Applied Chemistry for Engineering
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• v.5 no.5
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• pp.819-824
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• 1994

A membrane-like $H_3PMo_{12}O_{40}$-polysulfone film was prepared by blending $H_3PMo_{12}O_{40}$ with polysulfone using dimethylformamide as a common solvent. SEM and EDX analysis showed that $H_3PMo_{12}O_{40}$ was uniformly and finely distributed in the film catalyst. The ESCA measurement also revealed that the oxidation state of Mo was not changed. The $H_3PMo_{12}O_{40}$-polysulfone catalyst showed lower activity for acid-catalyzed reaction and higher activity for oxidation reaction than $H_3PMo_{12}O_{40}$ in ethanol conversion reaction. The oxidation activity of the film catalyst was about 10 times higher than $H_3PMo_{12}O_{40}$. The decrease of acidic activity was due to DMF strongly adsorbed in acid sites of $H_3PMo_{12}O_{40}$, whereas the increase of oxidation activity was mainly due to uniform distribution of $H_3PMo_{12}O_{40}$. Adsorption results showed that the surface character of $H_3PMo_{12}O_{40}$ was drastically increased, while the bulk property of that was almost same after blending. It is suggested that the control of surface/bulk property as well as acid/redox property of heteropoly acid would be possible by blending it with a polymer.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.42 no.6
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• pp.815-824
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• 2022

Among the main facilities of the power plant, the circulating water used for cooling the power generation system is supplied through the Circulation Water Intake Basin (CWIB). The vortexes of various types generated in the Pump Sump (PS) of CWIB adversely affect the Circulation Water Pump (CWP) and pipelines. In particular, the free surface vortex accompanied by air intake brings about vibration, noise, cavitation etc. and these are the causes of degradation of CWP performance, damage to pipelines. Then power generation is interrupted by the causes. Therefore, it is necessary to investigate the hydraulic characteristics of CWIB through the hydraulic model experiment and apply an appropriate Anti Vortex Device (AVD) that can control the vortex to enable smooth operation of the power plant. In general, free surface vortex is controlled by Curtain Wall (CW) and the submerged vortex is by the anti vortex device of the curtain wall. The detailed specifications are described in the American National Standard for Pump Intake Design. In this study, the circulating water intake part of the Tripoli West 4×350 MW power plant in Libya was targeted, the actual operating conditions were applied, and the vortex reduction effect of the anti vortex device generated in the suction tank among the circulating water intake part was analyzed through a hydraulic model experiment. In addition, a floor splitter was basically applied to control the submerged vortex, and a new type of column curtain wall was additionally applied to control the vortex generated on the free surface to confirm the effect. As a result of analyzing the hydraulic characteristics by additionally applying the newly developed Column Curtain Wall (CCW) to the existing curtain wall, we have found that the vortex was controlled by forming a uniform flow. In addition, the vortex angle generated in the circulating water pump pipeline was 5° or less, which is the design standard of ANSI/HI 9.8, confirming the stability of the flow.

• Journal of Institute of Control, Robotics and Systems
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• v.2 no.1
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• pp.26-34
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• 1996

One of the challenging tasks in visual inspection using CCD camera is to identify surface defects in an image with complex textured backgeound. In microscopic view, the surface of real objects shows regular or random textured patterns. In this paper, we present a visual inspection algorithm to extract abnormal surface defects in an image with textured background. The algorithm uses the space and frequency information at the same time by introducing the Dominant Frequency Map(DFM) which can describe the frequency characteristics of every small local region of an input image. We demonstrate the feasibility and effectiveness of the method through a series of real experiments for a 14" TV CRT mold. The method successfully identifies a variety of infinitesimal defects, whose size is larger than $50\mu\textrm{m}$, of the mold. The experimental results show that the DFM based method is less sensitive to the environmental changes, such as illumination and defocusing, than conventional vision techniques.ques.