• Proceedings of the KSME Conference
• /
• 2004.04a
• /
• pp.36-41
• /
• 2004

A method to measure the interfacial toughness of film/substrate by nanoindenter is proposed. As the thickness of the film decreases, the measurement of the interfacial toughness requires the more sophisticated equipment such as nanoindenter. In this study, the nanoindenter is applied to the substrate near the interface of film/substrate in the direction perpendicular to the normal of the interface, causing the cohesive fracture of the substrate, followed by the interfacial cracking. The specimen of Cu($0.56 {\mu}m$)/Si(530 ${\mu}$) are made by sputtering the copper onto the silicon wafer. By scratching the copper surface, we can make the easy interfacial cracking during the nanoindentation. It is found that the averaged values of the interfacial toughness of the Cu/Si is $0.664{\pm}0.3\;J/m^2$ . The phase angle of the specimen in this study is ${\psi}{\simeq}-36.8^{\circ}$, computed by the method of Suo and Hutchinson.[1]

• Journal of Ocean Engineering and Technology
• /
• v.9 no.2
• /
• pp.89-97
• /
• 1995

The investigate the effect of fiber orientation on the interlaminar fracture toughness of carbon fiber reinforced plastics three prepregs which are domestic products are used in this paper. Those are used for the unidirectional composites, but only one is used for the cross-ply laminate composites which is molded $[0/90]_{6s},\;[0/45]_{6s},\;and\;[0/45/90]_{4s}$. The specimens used for the mode I and mode II Tests are DCB and ENF samples are examined by scanning electron microscope(SEM). The value of $G_{IC}$ is almost same when modified three calculating methods are applied. The highest value of $G_{IC}$at crack initiation is obtained at the $[0/90]_{6s}$ interlaminar and the lowest one is at the $[0/45/90]_{4s}$ interlaminar. The highest value of $G_{IIC}$ at crack initiation, however, is obtained at the $[0/90]_{6s}$ interlaminar and the lowest one is at the $[0/45]_{6s}$. The photographs of SEM show a difference behaviour between mode I and mode II fracture surface.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.26 no.6
• /
• pp.1187-1193
• /
• 2002

Anodic bonding process has been quantitatively evaluated based on the Taguchi analysis of the interfacial fracture toughness, measured at the interface of anodically bonded silicon-glass bimorphs. A new test specimen with a pre-inserted blade has been devised for interfacial fracture toughness measurement. A set of 81 different anodic bonding conditions has been generated based on the three different conditions for four different process parameters of bonding load, bonding temperature, anodic voltage and voltage supply time. Taguchi method has been used to reduce the number of experiments required for the bonding strength evaluation, thus obtaining nine independent cases out of the 81 possible combinations. The interfacial fracture toughness has been measured for the nine cases in the range of 0.03∼6.12 J/㎡. Among the four process parameters, the bonding temperature causes the most dominant influence to the bonding strength with the influence factor of 67.7%. The influence factors of other process parameters, such as anodic voltage and voltage supply time, bonding load, are evaluated as 18%, 12% and 2.3%, respectively. The maximum bonding strength of 7.23 J/㎡ has been achieved at the bonding temperature of 460$\^{C}$ with the bonding load of 45gf/㎠, the applied voltage of 600v and the voltage supply time of 25minites.

• Journal of the Korean Society for Precision Engineering
• /
• v.14 no.12
• /
• pp.160-165
• /
• 1997

The instrumented Charpy impact test is generally used to evaluate the dynamic fracture toughnesses for varying engineering materials. However, the test is known to be difficult to evaluate the dynamic fracturetoughnesses for very brittle materials because of the small crack initiation load which may be engulfed by the inertia load of the instrumented tup. To evaluate the dynamic fracture toughnesses of very brittle materials, such as chalk or plaster,it is thus, necessary to develop a load sensitive instrumented tup. In this study, a polymer tup, which has very small Young's modulus comparing to one of the conventional steel tup, is used for the instrumented Charpy impact test, and a proper testing method to evaluate the dynamic fracture behavior of very brittle materials is developed. The results show that the developed method can measure rapidly changing loads from the moment of contact between the tup and the specimen to dynamic crack initiation of the very brittle materials.

• Journal of the Computational Structural Engineering Institute of Korea
• /
• v.12 no.3
• /
• pp.271-279
• /
• 1999

본 연구에서는 국내에서 가장 취약할 것으로 예상되는 원자력 발전소에 가압열충격 사고를 유발할 수 있는 주증기관 파단사고를 가정하여 열수력 해석과 파괴역학 해석을 수행하였다. 원전수명관리연구의 일환으로 계통열수력 해석 및 혼합열유동 해석에 의하여 구한 냉각제의 온도와 압력의 이력 및 용기의 재질성분으로부터 용기의 응력확대계수와 파괴인성치를 계산하고 이들을 비교하여 균열의 진전여부를 판단하여 형상계수가 1/6인 표면균열이 견딜 수 있는 최대 기준무연성천이온도를 결정하였다.

• Journal of the Korean Society for Precision Engineering
• /
• v.22 no.3 s.168
• /
• pp.130-136
• /
• 2005

The nondestructive evaluation system consisted of a ball indentation tester and a ultrasonic tester was developed to evaluate material properties. The relations between the parameters from test results using the system and the results of tensile and fracture toughness tests were investigated. The fracture toughness and tensile properties could be determined using the system. Some metallic materials were experimented to predict the fracture toughness and tensile properties and verify the relations between them. The predicted fracture toughness and tensile properties show a good agreement with the results obtained by conventional tests. It is found that the material properties and the material degradation can be evaluated using the nondestructive evaluation system.

• Korean Journal of Materials Research
• /
• v.7 no.11
• /
• pp.974-980
• /
• 1997

SiC$_{p}$/AI 합금 복합재료에 있어서 동적 및 정적파괴인성시험을 실시하고 파괴거동에 미치는 부하조건의 영향을 검토하였다. 동적파괴인성시험은 CAI시스템을 이용하여 1.5m/sec의 부하속도로 실시하였고, 정적파괴인성시험은 만능시험기를 이용하여 0.3 mm/min의 부하속도로 실시하였다. 또한 파괴과정을 명확히 해석하기 위하여 동적부하조건에 대해서는 stop block법을, 정적부하조건에 대해서는 복수시험편법을 이용하였다. 균열의 발생 및 성장은 부하조건에 의해 크게 영향을 받으며, 변위량에 대한 균열의 발생은 정적부하조건에서 더 빨리 일어나고, 균열의 성장은 동적부하조건에서 더 급격하다. 또한 부하조건은 파괴의 형태에도 크게 영향을 미치며, 동적부하조건하에서는 정적부하조건하에 비하여 균열이 입자부분(입자의 파단 또는 박리)을통과해 가는 경향이 크고 비교적 많은 편향을 반복해서 진행해 가지 때문에 파괴인성치도 크다.다.

• Proceedings of the Safety Management and Science Conference
• /
• 2001.05a
• /
• pp.311-317
• /
• 2001

The notched Charpy and Izod impact tests are the most prevalent techniques used to characterize the effects of high impulse loads on ploymeric materials. An analysis method for rubber toughened PVC is suggested to evaluate critical strain energy release rates(Gc) from the Charpy impact energy measurements. An Instrumented Charpy Impact tester was used to extract ancillary information concerning fracture properties in addition to total fracture properties and maximum critical loads. The stress intensity factor Kd was computed for varying amounts of rubber contents from the obtained maximum critical loads and also toughening effects were investigated as well.

• Journal of the KSME
• /
• v.35 no.6
• /
• pp.481-494
• /
• 1995

원자로 압력용기 및 주 배관등 원자력발전소 주요부품 구조재료에서의 파괴저항성 및 건전성 문제를 일부 시험결과 및 평가결과와 함께 살펴보았다. 원자력환경하에서는 중성자 조사에 의한 조사취화 및 고온에서의 장기간 유지에 따른 열취ㅘ로 재료 고유의 파괴저항치가 가동에 따라 매우 감소하고, 이에 따라 부품의 건전성 및 수명이 매우 위협받고 있음을 확인하였다. 현재 가동중인 원자로 10기, 건설중인 8기, 합계 18기로 세계 9위의 원자력발전국이 되며, 대북 경수로 지원과 세계시장 진출을 계획하고 있는 우리나라에서는, 보다 안전한 원자력발전소가 건설되기 위해서, 재료의 균질성 및 파괴인성 개선연구, 조사특성 연구 등을 통해 파괴저항성이 우수한 국산소재를 제작\ulcorner공급하도록 하여야 한다. 또한, 수명기간 동안 고도의 건전성을 유지하면서 운전하고, 나아가 수명연장 운전을 위해서는, 용기 등 주요 부품의 상태(파괴인성치, 결함, 작용 응력)를 정확히 진단, 예측, 평가하여야 하고, 이들이 건전성에 미치는 영향평가와 건전성평가기술 확립을 통한 수명예측기술을 확보하여야 한다(이들은 대부분 파괴역학 시험 침 해석기술에 바 탕을 두고 있다). 국내 산\ulcorner학\ulcorner연 관련자들의 특별한 관심을 촉구하는 바이다.

• Journal of Ocean Engineering and Technology
• /
• v.16 no.4
• /
• pp.42-47
• /
• 2002

This paper describes the effect of loading rate, specimen geometries and material properties for Mode II interlaminar fracture toughness of hybrid composite by using end notched flexure(ENF) specimen. In the range of loading rate 0.5~2mm/min, there is found to be no significant effect of loading rate with the value of critical energy release rate( $G_{IIc}$). there is no dependence of the interlaminar fracture energy upon the specimen width over the specimen widths examined. The value of $G_{IIc}$ for variation of initial crack length are nearly similiar values when material properties are CF/CF and GF/GF, however, the value of $G_{IIc}$ are highest with the increasing intial crack length at CF/GF. The values of $G_{IIc}$ for variation material properties are higher with the increasing moulding pressure when moulding pressures are 307, 431, 585㎪. The SEM photographs show good fiber distribution and interfacial bonding of hybrid composites when the moulding is the CF/GF.e CF/GF.