• Composites Research
• /
• v.30 no.1
• /
• pp.71-76
• /
• 2017

The purpose of this study was to predict the long-term performance using the interlaminar shear strength of carbon fiber/epoxy composites exposed to environmental factors. Interlaminar shear specimens, manufactured by the filament winding method, were exposed to the conditions of drying at $50^{\circ}C$, $70^{\circ}C$, and $100^{\circ}C$ and of immersion at $25^{\circ}C$, $50^{\circ}C$, and $70^{\circ}C$ for up to 3000 hours, respectively. According to the results, the interlaminar shear strength did not vary significantly with the exposure time for the drying at $50^{\circ}C$ and $70^{\circ}C$, but it increased somewhat for the drying at $100^{\circ}C$ due to the post curing as the exposure time increased. The interlaminar shear strength of the specimens exposed to the immersion at $25^{\circ}C$ did not change significantly at the beginning of exposure, but it decreased with the exposure time and the degree of decrease increased as the environmental temperature increased. The linear regression equations for the environmental temperatures were obtained from the interlaminar shear strength of the specimens exposed to the immersion for up to 3000 hours. Using these linear regression equations, the interlaminar shear strength was estimated to be within 5.5% of the measured value at $25^{\circ}C$ and $50^{\circ}C$, and 2.3% of the measured value at $70^{\circ}C$. Therefore, the proposed performance prediction procedures can predict well the long-term interlaminar shear strength of carbon fiber/epoxy composites exposed to environmental factors.

• Journal of the Korean Ceramic Society
• /
• v.37 no.10
• /
• pp.955-961
• /
• 2000

사티탄산칼륨을 리튬이온 전지의 양극재료로써 사용하고자 할 때 사티탄산칼륨의 합성 열처리 온도가 리튬이온 치환량에 미치는 영향에 대해 조사하였다. 사티탄산칼륨은 $K_2$O와 TiO$_2$의 몰 비를 1 : 3.91로 칭량하여 95$0^{\circ}C$, 100$0^{\circ}C$, 105$0^{\circ}C$에서 각각 합성하였다. 그 후, 사티탄산칼륨의 (Ti$_4$O$_{9}$ )$^{2-}$ 층간에 존재하는 $K^{+}$ 이온을 H$^{+}$ 이온으로 치환하고 이것을 다시 Li$^{+}$ 이온으로 치환하였다. 사티탄산칼륨의 합성 열처리 온도가 증가할수록 사티탄산칼륨의 (Ti$_4$O$_{9}$ )$^{2-}$ 층간의 거리가 감소했고 사티탄산칼륨의 길이가 증가했다. 95$0^{\circ}C$에서 열처리된 사티탄산칼륨의 리튬이온 치환량이 가장 많았다. 이는 상대적으로 낮은 합성 열처리 온도에서 사티탄산칼륨의 (Ti$_4$O$_{9}$ )$^{2-}$ 층간의 거리가 넓어져 리튬이온의 층간 이동이 쉬어졌고, 고온에서 열처리되어 길이가 긴 사티탄산칼륨에 비해 저온에서 열처리된 사티탄산칼륨은 길이가 짧아져 리튬이온이 (Ti$_4$O$_{9}$ )$^{2-}$ 층간으로 이동해 가는 거리가 짧아졌으며 아울러 짧은 사티탄산칼륨의 개수가 동일한 무게 당긴 사티탄산칼륨의 개수보다 많으므로 리튬이온의 치환량이 많아진다고 사료된다.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.39 no.5
• /
• pp.491-497
• /
• 2015

This paper reports an experimental study for evaluating the effect of temperature on the mode I, mode II and mixed-mode interlaminar fracture toughness of adhesive joints with a curved cross-section of filament-wound dome-separated composite pressure vessel. Mode I and mixed-mode interlaminar fracture toughness were evaluated using DCB specimens, while mode II interlaminar fracture toughness was determined using ENF specimens. $[{\pm}10^{\circ}]_6$, $[{\pm}27^{\circ}]_6$ and ($[{\pm}10^{\circ}]_3/FM73/[{\pm}27^{\circ}]_3$) winding specimens with the curved cross-section were considered. In-situ temperature environments were simulated with a range of $-30^{\circ}C-60^{\circ}C$ using an environmental chamber and furnace. Experimental results on the effect of temperature indicate that interlaminar fracture toughness tends to be high at low temperature and is degraded with increase in temperature. For specimen types, it was found that interlaminar fracture toughness of $[{\pm}10^{\circ}]_3/FM73/[{\pm}27^{\circ}]_3$ winding specimens considered as adhesive joints of dome and helical part was higher than other specimens.

• Journal of the Korean Magnetics Society
• /
• v.26 no.5
• /
• pp.149-153
• /
• 2016

In Fe/Gd multilayers, patterning effect on the interlayer coupling was studied by comparing patterned and unpatterned samples that were cut from a multilayer film. A comparative study of the two samples via temperature dependent Gd-specific magnetization vector using X-ray magnetic circular dichroism (XMCD) shows that the temperature dependence of the Gd magnetization vector can be modified in the patterned sample due to a competition between the patterning and antiferromagnetic interlayer coupling effects.

• Journal of Welding and Joining
• /
• v.15 no.3
• /
• pp.56-64
• /
• 1997

Macrostructural characteristic of the transverse cracks and fatigue behavior were studied for EH 32 TMCP 50mm thick plate welded with FACW under the variation in preheat and interpass temperatures. Transverse cracks were detected in specimen welded with preheat and interpass temperature below $30^{\circ}C$, but cracks were not detected in the specimens welded with preheat and interpass temperatures at the range of $100~120^{\circ}C$.C. The location of crack formation was found to strongly depend upon the thickness of weld layers as regard to the plate thickness.

• Proceedings of the KWS Conference
• /
• 1996.05a
• /
• pp.176-178
• /
• 1996

• Polymer(Korea)
• /
• v.24 no.6
• /
• pp.794-801
• /
• 2000

The effect of chain length and packing density of intercalated surfactants, annealing temperature, and annealing time on static melt intercalation of thermoplastic polymers was examined using x-ray and FTIR spectroscopy. Although melt intercalation of polymers was not successful when alkyl chains in organosilicates form a lateral monolayer structure, the type and structure of surfactants could not much affect final interlayer distances of most polymer/silicate hybrids. As annealing time increases, interlayer distance in organosilicates increases while the dispersity of the spacing between silicate layers decreases. However, the dispersity of interlayer spacing as well as interlayer distance in organosilicates increase with annealing temperature.

• Korean Chemical Engineering Research
• /
• v.46 no.1
• /
• pp.56-62
• /
• 2008

Characteristics of heat transfer were investigated in a three-phase swirling fluidized bed whose diameter was 0.102 m and 2.5 m in height. Effects of gas and liquid velocities, particle size and liquid swirling ratio ($R_S$) on the immersed heater-to-bed overall heat transfer coefficient were examined. The heat transfer characteristics between the immersed heater and the bed was well analyzed by means of phase space portraits and Kolmogorov entropy(K) of the time series of temperature difference fluctuations. The phase space portraits of temperature difference fluctuations became stable and periodic and the value of Kolmogorov entropy tended to decrease with increasing the value of liquid swirling ratio from 0.1 to 0.4. The value of Kolmogorov entropy exhibited its minimum with increasing liquid swirling ratio. The value of overall heat transfer coefficient (h) showed its maximum with the variation of liquid velocity, bed porosity or liquid swirling ratio, but it increased with increasing gas velocity and particle size. The value of K exhibited its maximum at the liquid velocity at which the h value attained its maximum. The overall heat transfer coefficient and Kolmogorov entropy were well correlated in terms of dimensionless groups and operating variables.

• Journal of the KSME
• /
• v.32 no.3
• /
• pp.247-254
• /
• 1992

이 글에서는 고충아파트에서 층간 열공급의 불균일성이 발생하는 원인을 설명하였고 이 불균일 성을 해소시키는 새로운 열공급 설비 기술을 설명하였으며 그 내용들에 대한 결론은 다음과 같다. (1) 온수 난방 고층아파트의 층간 열공급의 불균일성은 온수공급관과 회수관의 정수압력의 차 이에 의한 유동저항에 의해서 발생한다. (2) 다구역배관망 시스템은 온수공급관과 회수관의 정수압력의 차이에 의해 발생하는 열공급 불균일성의 해소에 거의 기여하지 못한다. (3) 연속난방방식에서 서모스타트의 설치는 각세대의 열공급을 균일하게 할 수 있고 에너지 절 약면에서 가장 유리한 방식이나 고장의 위험성이 가장 크며, 운전의 미숙에 의한 열공급 제어의 불균일성을 초래하기 쉬우며 외기온도가 매우 낮으면 층간 열공급제어가 되지 않을 수 있어서 자동유량조절밸브를 병용하거나 온수공급압력을 충분히 크게 할 필요가 있다. (4) 자동유량조절밸브에 부착하면 단구역 배관망 시스템에서도 층간의 유량공급의 불균일성을 없앨 수 있으나 순환 펌프유량이 부족하면 밸브의 자동유량조절 기능이 상실된다. (5) 수동유량조절밸브는 TAB에 의해서 충간의 유량을 균일하게 조절할 수 있으나 펌프 성능변화 관부식 등이 발생하면 TAB를 다시 할 필요가 발생할 수 있다. 그러나 밸브의 고장이 적고 유 동저항을 적게 발생시키며 한 개의 밸브로 조절할 수 있는 유량의 범위가 큰 점에서는 가장 유 리하다.

• Proceedings of the Korean Radioactive Waste Society Conference
• /
• 2016.10a
• /
• pp.247-248
• /
• 2016