• Title/Summary/Keyword: 체화인지

Search Result 424, Processing Time 0.03 seconds

Reverse-Phase High Performance Liquid Chromatographic Determination of Amino Acids after Precolumn Derivatization with 1-Dimethyl-aminonaphthalene-5-sulfonyl chloride (Dansyl 유도체화와 역상 고성능액체크로마토그래피에 의한 아미노산의 정량)

  • 나혜경;전덕영;홍윤호
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.22 no.6
    • /
    • pp.815-822
    • /
    • 1993
  • This experiment was carried out to determine the separation condition of 1-dimethylaminonaphthalene-5-sulfony(Dansyl) derivatives of amino acids by reverse-phase high performance liquid chromatography with Nova-Pak C18 column. Determined solvent system was solvent A(200mA phosphate buffer pH 6.8 15%, acetonitrile 11%, water 74%) and solvent B(acetonitrile 65%, methanol 28%, water 7%). Linear gradient of solvent B was applied from 12% to 80% for 50min. Complete separation of 20 amino acids including asparagine and glutamine which constitute protein was achieved within 50min. As the detection limit was the range of picomole, the resolution power was excellent. Reproducibility of the retention time was less than mean $\pm$0.05min. According to the above optimum chromatographic conditions, the amino acid composition of some food and human blood was examined. The most affluent amino acid was alanine in human blood, aspartic acid and glutamic acid in soy sauce, alanine and threonine in soy milk and proline in milk and yoghurt.

  • PDF

A Study on the Modal Shift Effects by Car-ferry Networks in Korea (한반도 카페리 네트웍화에 의한 물류수단이전과 그 효과에 관한 연구)

  • Kim, Myung-Jae;Jang, Woon-Jae
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
    • /
    • 2013.06a
    • /
    • pp.209-213
    • /
    • 2013
  • The expense Our country's land logistics system is becoming backlog day by day. The greenhouse gas which it discharges specially from the vehicle causes a ecocide and traffic expense to make. The traffic energy curtailment which the government enforces during that time and environment-friendly green goods policy lost the effect. Therefore, This research propose the car-ferri network which is the most effective logistics system substitutes the land logistics system. This research will contribute improving the north and south logistics network of Pusan and Seoul region and will be able to reduce a various goods expense.

  • PDF

The Effect of Mn Content Solution-treatment Temperatures on Insoluble Phases in Al-Li-Cu-Mg-Mn-Zr Alloys (Al-Li-Cu-Mg-Zr 합금의 미고용상에 미치는 용체화 처리 및 Mn 함량의 영향)

  • Shin, Hyun-Sik;Ming, He;Cho, Kwon-Koo;Chung, Young-Hoon;Shin, Myung-Chul
    • Analytical Science and Technology
    • /
    • v.7 no.4
    • /
    • pp.517-526
    • /
    • 1994
  • Large insoluble phases and dispersoids in Al-Li-Cu-Mg-Mn-Zr alloys containing Mn were analyzed with EPMA(Electron Probe Microanalyzer) and SAEM(Scanning Auger Electron Microscope). Morphology, distribution and volume fraction of the large insoluble phase were also analyzed quantitatively by optical microscopy. Mechanical properties were tested at room temperature and at $200^{\circ}C$. With increasing Mn contents, the volume fraction of the large insoluble phases increased steeply, thus decreasing ductility. Mn was found to be very effective for obtaing uniformly distributed fine-grain structures. The alloy containing 0.44 wt% Mn showed the highest tensile strength among Mn-bearing alloys tested.

  • PDF

Determination of Elastic Modulus of Equal-Channel-Angular-Pressed Aluminum 5052 Alloy by Acoustic Material Signature (음향재료신호를 이용한 강소성변형된 알루미늄 5052 합금의 탄성계수 측정)

  • Kim, Chung-Seok;Park, Ik-Keun;Jhang, Kyoung-Young;Miyasaka, Chiaki
    • Journal of the Korean Society for Nondestructive Testing
    • /
    • v.30 no.2
    • /
    • pp.146-154
    • /
    • 2010
  • The effects of severe plastic deformation, equal channel angular pressing, and annealing of Al 5052 alloy on elastic modulus have been studied. The AI 5052 alloy was plastically deformed by ECAP method after solution treatment, and then finally annealing heat treated. Elastic modulus was measured by conventional tensile and nano-indentation test, and also measured on the surface of the specimen using acoustic material signature of the acoustic microscope. The variation in the elastic modulus influenced by plastic deformation and heat treatment, inaccessible by the conventional techniques, was successfully measured by acoustic material signature and obtained the elastic modulus depending on crystal orientation at each grain.

The Effect of Solid Solution Heat-Treatment Temperature on the Tensile Property in Intermediate Thermo-Mechanical Treated Al-Li Alloys (중간가공열처리한 AI-Li계 합금의 인장성질에 미치는 용체화처리온도의 영향)

  • Yoo, C.Y.;Lee, K.B.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.4 no.1
    • /
    • pp.37-41
    • /
    • 1991
  • In this study, the effect of solution treatment temperature on the tensile property in intermediate thermo-mechanical treated Al-Li alloys are investigated. After the intermediate thermo-mechanical treated Al-Li, Al-Li-Mg and Al-Li-Mg-Zr alloys were solution treated at various temperatures (500, 520 and $540^{\circ}C$), these were aged at $190^{\circ}C$, $240^{\circ}C$ and tested tensile properties. The results obtained from the experiment are as follows ; 1) The optimum solution heat-treatment temperature is $540^{\circ}C$ for a Al-Li alloy, and the recrystallized grain size is about $70{\mu}m$. 2) The optimum solution heat-treatment temperature is $500^{\circ}C$ for a Al-Li-Mg alloy, and the recrystallized grain size is the most coarse in all alloys. 3) The tensile property is independent of the solution treatment temperature in a Al-Li-Mg-Zr alloy, and the recrystallized grain size is the finest owing to addition of Zr.

  • PDF

Effect of Hot Forging Ratio and Solution Treatment Temperature on the Mechanical Properties of Incoloy 825 Alloy (Incoloy 825 합금의 기계적 성질에 미치는 열간 단조비와 용체화 온도의 영향)

  • Kim, D.H.;Park, Y.T.;Son, Y.M.;Kang, C.Y.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.31 no.5
    • /
    • pp.213-219
    • /
    • 2018
  • This study was carried out to investigate the effect of hot forging ratio and solution treatment temperature on the mechanical properties of incoloy 825 alloy. With an increasing of the hot forging ratio, grain size and range of grain size was decreased. With an increasing of the solution treatment temperature after 90% forging, grain size and range of grain size was increased. Cr carbides and Ti nitrides was precipitated at below $900^{\circ}C$ and volume fraction of precipitate was increased with an decreasing of the solution treatment temperature. With an increasing of the hot forging ratio, hardness, tensile strength and elongation, toughness was increased. With an increasing of the solution treatment temperature after 90% forging, hardness and strength was increased, elongation and toughness was decreased by grain refinement. With an increasing of the forging ratio, effect of solution treatment temperature on the hardness, strength and elongation was small, but on the toughness was large.

Determination of ${\alpha}-Keto$ Acids in Serum and Urine Using 1,2-Diamino-4,5-methylendioxybenzene as a Fluorescent Derivatizating Agent by High Performance Liquid Chromatography (HPLC법에 의한 1,2-디아미노-4,5-메틸렌디옥시벤젠을 형광유도체화제로 한 혈청 및 뇨 중의 ${\alpha}$-케토산의 분석)

  • Ok, Chi-Wan;Kim, Dae-Ki;Park, Song-Ja;Park, Jong-Sei
    • YAKHAK HOEJI
    • /
    • v.36 no.4
    • /
    • pp.370-378
    • /
    • 1992
  • A simple and sensitive high performance liquid chromatographic method to quantitate ${\alpha}-keto$ acids in serum and urine was investigated. ${\alpha}-Keto$ acids react with 1,2-diamino-4,5-methylenedioxybenzene (DMB) in the presence of 2-mercapto-ethanol and sodium hydrogen sulfite to form highly fluorescent derivatives, substituted 6,7-methylenedioxyquinoxalinol. The derivatization procedure was performed in water bath at $100^{\circ}C$, and completed within 50 min. By the use of a reversed-phase column and multi-step gradient with two solvents, a mixture containing twelve of these derivatives were efficiently resolved within 35 minutes. The optimal wavelengh of the fluorescence detector are ${\lambda}_{ex}=364\;nm$ and ${\lambda}_{em}=445\;nm$. The quantitation of the individual ${\alpha}-Keto$ acids was reproducible with relative standard deviation of $3.0{\sim}7.9%$ and had a detection limits of $10{\sim}60$ fmol, except for p-hydroxyphenylpyruvic acid (960 fmol).

  • PDF

An Analysis for basic Concepts of The Integrated Management of Records and Archives in China (중국의 '문건·당안 일체화' 개념 분석)

  • Seo, Seok-jae
    • The Korean Journal of Archival Studies
    • /
    • no.10
    • /
    • pp.198-226
    • /
    • 2004
  • This paper analyses the theories and practices of the integrated management of records and archives in china which means that records and archives management departments should be interrelated each other with organic association and their records and archives be managed in an integrated manner. In 1930s chinese nationalist regime had conducted a campaign for reforming documents and archives management system to increase administrative efficiency called "The Connection of Documents and Archives Management Act(文書檔案連鎖法)". Although this campaign has not been continued to the present, It has been proved to be a quite successful attempt at that time in china and also regarded as an origin of the integrated management of records and archives in china. The practical types of the integrated management of records and archives as follows: first is to establish institutional documents/archives department in charge of managing records and archives in an integrative manner; second, to reform filing system, that is, to file on a case basis or abolish filing system and arrange records on an item level instead; third, to install software application for the integrated management of records and archives in order to make arranging operations convenient by increasing data processing efficiency. The chinese case shows us that the integrated management of records and archives could not be realized until records and archives departments make united efforts to build up a new national records and archives management system based on advanced and scientific principles.

Haptic Perception in Fashion Film - Drawing on the theory of Laura Marks - (패션필름에 나타난 햅틱(Haptic)지각 -로라 막스(Laura Marks)의 이론을 바탕으로-)

  • Chung, Soo-Jin;Yim, Eun-Hyuk
    • The Korean Fashion and Textile Research Journal
    • /
    • v.21 no.4
    • /
    • pp.379-389
    • /
    • 2019
  • Fashion brands have traditionally conveyed emotions through brand image and images such as fashion photos; however, fashion films play an important role in conveying emotion to consumers due to changes that have resulted from the development of digital technology. This study investigates haptic perceptions in fashion films based on Laura Marks' theory. The study concurrently conducted literature and case studies. Haptic and is a condition of touching an object without actually touching it. Marks describes haptic theory as an embodied perception of physical effects that occur as images affect the body. Haptic perceptions that cause a sense of touching when looking at a fashion film can be understood as a formality embodied in the body of the object and spectator created by the object and spectator's clothing experience. Our bodies and apparel can be seen as being perceived and imprinted in our bodies by constantly experiencing and maintaining relationships in an inseparable relationship. Thus, when we look at fashion films, the haptic image invites feeling embodied in our body and provide a haptic perception. As a result, factors for the haptic perception in fashion film are ambiguity of images, fetish image, and non-narrative. Fashion companies are expected to make active use of haptic elements as an era of artificial intelligence arrives and the size of the e-commerce market grows.

Cultural Capital in Online-RPG - Focusing on experience of 'World of Warcraft' play - (온라인 RPG에서의 문화자본 - '월드 오브 워크래프트' 플레이 경험을 중심으로 -)

  • Choi, Han-jeong;Ryu, Seoung-ho
    • Journal of Korea Game Society
    • /
    • v.19 no.2
    • /
    • pp.95-110
    • /
    • 2019
  • This paper aims to study on attribute of interaction between user from cultural capital perspective of Bourdieu who expanded the concept of capital and presented class production and reproduction through 'World of Warcraft' play and analysis. The results of this study is that First, game ability showed properties of cultural capital that embodied, objectified, institutionalized. Second, the types of interaction by difference of cultural capital appeared that lurking, reciprocity, exclusion. This study identified game ability have attributes of cultural capital and that Due to the nature of the interaction for 'Disticion', individual actions are related to the process of accumulating power and contribute to class reproduction.