• Title/Summary/Keyword: 중심합성계획법

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Optimization of Process Time by Peeling of ABS Plating using Design of Experiment (실험계획법(DOE)을 이용한 ABS 도금의 Peeling 향상을 위한 공정 시간 최적설계)

  • Jeon, Seong-Uk;U, Chang-Ho
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2013.05a
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    • pp.130-131
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    • 2013
  • 최근 연구에서는 상용 통계분석 프로그램인 Minitab을 사용하여 실험 요소 설계 및 최적 공정조건을 구하는데 많이 이용하고 있다. 본 연구에서는 도금 제품의 Peeling 최적화를 위해 도금 전처리 공정인 에칭 및 화학 니켈 공정 시간을 인자로 설정하였다. 또한 2인자 2수준(2 factor 2 Level)의 직교 배열표를 구성하고 도금 제품의 밀착성을 만족하는 범위 내에서 설계변수에 의한 반응표면법(Response surface analysis)을 사용하여 최적 조건을 설정하였다. 실험 결과, 에칭 및 화학니켈 공정 시간의 주효과도에서 에칭 공정시간이 낮을수록, 화학니켈 공정시간이 높을수록 Peeling 값이 향상된다는 결과를 얻었다. 그리고 최적 조건을 도출하기 위한 방법으로 반응표면 설계법 중의 중심합성법을 사용하여 에칭(10min 15sec)및, 화학니켈(10min 15sec)의 최적 공정 시간을 도출하였다.

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Optimization Study of Trace Analysis of Potential Diesel Oxygenate Using the Design Of Experiment (DOE) in Solid-Phase Microextraction with GC/FID (고체상미량분석법(SPME-GC/FID)에서 실험계획법을 이용한 디젤첨가제 미량분석의 최적화 연구)

  • Park, Jae-Sang;Chang, Soon-Woong
    • Journal of Soil and Groundwater Environment
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    • v.12 no.5
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    • pp.73-85
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    • 2007
  • In this study, the experiment of solid-phase microextraction (SPME) technique using GC/FID was conducted as a possible alternative to liquid-liquid extraction for the analysis of EGBE, DGBE, DBM and TGME in water, and also, an optimization condition of trace analysis for disel oxygenates including EGBE by the design of experiment (DOE) was described. Experiments used a fractional factorial design method followed by central composite design allowing optimization of a number of factors as well as statistical analysis of the results. The response surface analysis showed that the extraction efficiency could be represented by a second-order polynomial equation in which the salts concentration, extraction temperature, extraction time and sonication time are the major influences. Using DOE method, a new datadependent method was developed to improve the quantity of confidently analyzed disel oxygenates in water samples.

Optimization of coagulant dosage using response surface methodology with central composite design (반응표면분석법-중심합성계획을 이용한 최적 응집제 주입량 산정 연구)

  • Kim, Yeseul;Oh, Jeill
    • Journal of Korean Society of Water and Wastewater
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    • v.29 no.2
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    • pp.193-202
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    • 2015
  • The determining the appropriate dosage of coagulant is very important, because dosage of coagulant in the coagulation process for wastewater affects removing the amount of pollutants, cost, and producing sludge amount. Accordingly, in this study, in order to determine the optimal PAC dosage in the coagulation process, CCD (Central composite design) was used to proceed experimental design, and the quadratic regression models were constructed between independent variables (pH, influent turbidity, PAC dosage) and each response variable (Total coliform, E.coli, PSD (Particle size distribution) (< $10{\mu}m$), TP, $PO_4$-P, and $COD_{cr}$) by the RSM (Response surface methodology). Also, Considering the various response variables, the optimum PAC dosage and range were derived. As a result, in order to maximize the removal rate of total coliform and E.coli, the values of independent variables are the pH 6-7, the influent turbidity 100-200 NTU, and the PAC dosage 0.07-0.09 ml/L. For maximizing the removal rate of TP, $PO_4$-P, $COD_{cr}$, and PSD(< $10{\mu}m$), it is required for the pH 9, the influent turbidity 200-250 NTU, and the PAC dosage 0.05-0.065 ml/L. In the case of multiple independent variables, when the desirable removal rate for total coliform, E.coli, TP, and $PO_4$-P is 90-100 % and that for $COD_{cr}$ and PSD(< $10{\mu}m$) is 50-100 %, the required PAC dosage is 0.05-0.07 ml/L in the pH 9 and influent turbidity 200-250 NTU. Thus, if the influent turbidity is high, adjusting pH is more effective way in terms of cost since a small amount of PAC dosage is required.

Reverse Engineering of Aged Planner Miller Main Spindle Using Central Composite Design (중심합성계획법을 이용한 노후 플래너 밀러 주축 스핀들의 역설계에 관한 연구)

  • Kim, Hong-Rok;Chung, Won-Jee;Seol, Sang-Seok;Hong, Dae-Sun;Gong, Seok-Whan;Lee, Hyun-Jun;Lee, Seong-Won
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.21 no.3
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    • pp.36-42
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    • 2022
  • Whereas the necessity for recycling and reuse is being emphasized owing to the depletion of resources and waste disposal problems caused by the continuous development of the industry, the importance of remanufacturing has been highlighted recently. Re-manufacturing involves a series of processes in which failed disposal or aging goods are recovered to a state similar to that of a new product. In this regard, machine tools, which are large structures, can achieve the effect of remanufacturing. Among the various elements constituting the machine tool, the main spindle portion that affects the processing precision is critical. Therefore, this study is conducted to derive improvement measures for the main axis of an old Miller planner via reverse engineering and central composite design, which is one of the core processes of remanufacturing.

야채를 이용한 soup mix의 제조조건이 야채죽의 물리적 특성 및 관능적 특성에 미치는 영향

  • 이용욱;금준석;이종욱;은종방
    • Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
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    • 2003.04a
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    • pp.123-123
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    • 2003
  • 야채 soup mix의 제조조건이 야채죽의 물리적 및 관능적 특성에 대한 영향을 조사하였다. Soup mix의 제조조건인 주입액의 양 (쌀 무게에 대한 물의 체적 비), 버섯, 당근 그리고 대파의 첨가량(쌀 무게에 대한 잣의 무게 비)에 따른 물리적 특성과 관능적 특성의 변화를 모니터링 하고자 반응 표면분석법 (response surface methodology, RSM)을 사용하였으며, 이때 실험계획은 중심합성계획법을 적용하였다. 요인변수(Xn)를 중심합성계획에 따라 17실험구로 구분하여 조리실험을 실시하였고, 이들 요인변수에 의해 영향을 받는 반응변수(Yn)는 야채죽의 물리적 특성으로 하여 회귀분석에 사용하였다. 회귀분석에 의한 모델식의 예측에는 SAS (statistical analysis system) program을 사용하였으며, 야채죽의 조리조건이 물리적 및 관능적 특성에 미치는 영향은 SAS program을 이용한 3차원 반응표면분석법으로 해석하였다. 야채의 배합비를 달리한 야채죽의 물리적 특성인 색도 L, a 및 b값에 대한 F-value는 자각 1.50, 11.75 및 5.58이고,유의수준이 각각 0.3044, 0.0019와 0.0169로서 a값과 b값의 유의성이 1% 수준에서 인정되어 이들 제조조건이 a값과 b값에 큰 영향을 미치는 것으로 나타났다. 점도와 퍼짐성에 대한 유의수준은 각각 0.6920과 0.7528이고, 반응표면회귀식의 $R^2$은 각각 0.4766과 0.4436으로 유의성이 인정되지 않았다. 고형분에 대한 유의수준은 0.2026이고 회귀식의 $R^2$는 0.7107으로서 버섯, 당근 및 대파 첨가량이 고형분의 변화에 영향을 미치지 않은 것을 알 수 있었다. 관능적 특성인 색상에 대하여 soup mix의 제조조건이 야채죽에 미치는 영향은 F-value는 6.23이고, 유의수준이 0.0124으로서 1%수준에서 유의성이 인정되었으며, 회귀식의 $R^2$은 0.8890이다. 향에 대한 유의확률은 0.4555이고 0.05이상이므로 유의성이 인정되지 않아 설정된 범위내에서 야채죽의 향에 대하여 크게 영향을 미치지 않는 것으로 나타났다. 점성에 대한 반응표면회귀식의 $R^2$은 0.8134로서 그 유의성이 5%수준에서 인정되었다. 맛과 전반적 기호도에 대하여 야채의 배합비에 따른 반응표면회귀식의 $R^2$은 각각 0.7374와 0.8651이며, 유의화률은 0.1578과 0.0228으로 나타나 전반적인 기호도에 대한 영향은 10% 유의수준에서 영향을 주었다. 결론적으로, 물리적 특성인 색도, 점성, 퍼짐성과 고형분의 함량은 관능적 특성인 색과 비교적 높은 정(正)의 상관을 나타내었으며, 관능적 특성인 향과의 상관은 유의성이 인정되지 않았다. 야채죽 제조를 위한 soup mix의 제조조건에 있어서 야채의 배합비는 색과 점성에 영향을 미치는 가장 주요한 조건이라고 생각된다.

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Optimum Design of Dynamic Vibration Absorber for Reducing Bending Vibrations of Two-Piece Vehicle Drive Line (2축 분할식 차량 구동라인의 굽힘진동 저감을 위한 동흡진기 최적설계)

  • Lee, Sang-Beom;Yoo, Young-Sun
    • The Journal of the Acoustical Society of Korea
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    • v.29 no.2
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    • pp.118-124
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    • 2010
  • In this paper, design parameters of dynamic vibration absorber, which is used to reduce bending vibrations of a vehicle drive line, is optimized. For obtaining the correct dynamic response characteristics, a flexible-body drive line is made by applying the flexibility data extracted from vibration analysis of propeller shafts to the drive line dynamic model. Inner tube mass, rubber stiffness and rubber damping coefficient of the dynamic vibration absorber are taken as design parameters for optimization. To minimize the vertical acceleration of the drive line, a second-order regression equation of the objective function is generated by performing the central composite experimental design with 3 factors, 2 levels and 15 test runs. And the design parameters of the dynamic vibration absorber are determined by using optimization program. The vehicle model with optimized dynamic vibration absorber reduces the vertical acceleration peak of the drive line by 17.1 % in compared with the initial model.

Optimization of Organosolv Pretreatment of Waste Wood for Lignin Extraction (폐목재로부터 리그닌 추출을 위한 Organosolv 전처리공정의 최적화)

  • Lee, Hyunsu;Kim, Young Mo
    • Journal of Korean Society of Environmental Engineers
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    • v.39 no.10
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    • pp.568-574
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    • 2017
  • The purpose of this study was to optimize experimental conditions (time ($X_1$) (ranging of 26.36 - 93.64 min), concentration of sulfuric acid ($X_2$) (ranging of 0-2.5%) and temperature ($X_3$) (ranging of $136.4-203.6^{\circ}C$) for an organosolv pretreatment process to extract lignin from waste wood. The resulting quadratic model equation using RSM (response surface methodology) represented y (lignin yield) = $-79.89+0.91X_1+9.8X_2-2.54{\times}10^{-3}X_1{^2}-2.11X_2{^2}$. The $R^2$ (coefficient of determination) value of 0.8531 for a model indicates this model has statistically significant predictors at the 10% levels. The predictive results optimized by quadratic model produced a lignin yield of 12.46 g/100 g of dry wood under conditions of $178.2^{\circ}C$ and 2.32% $H_2SO_4$. The lignin yield was more affected by the acid catalyst concentrations than the reaction temperature, but the reaction time was not an influential factor for improving lignin extraction from waste wood in this organosolv pretreatment. According to ANOVA (analysis of variance), the significance probability (p-value) of model was smaller than 0.001 and simulation of obtained model equations showed a good reproducibility based on actual organosolv tests under optimal conditions.

Structural Optimization for Small Scale Vertical-Axis Wind Turbine Blade using Response Surface Method (반응표면법을 이용한 소형 수직축 풍력터빈 블레이드의 구조 최적화)

  • Choi, Chan-Woong;Jin, Ji-Won;Kang, Ki-Weon
    • The KSFM Journal of Fluid Machinery
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    • v.16 no.4
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    • pp.22-27
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    • 2013
  • The purpose of this paper is to perform the structural design of the small scale vertical-axis wind turbine (VAWT) blade using a response surface method(RSM). First, the four design factors that have a strong influence on the structural response of blade were selected. Analysis conditions were calculated by using the central composite design(CCD), which is a typical design of experiment for the response surface method(RSM). Also, the significance of the central composite design(CCD) was verified using analysis of variance(ANOVA). The finite element analysis was performed for the selected analytical conditions for the application of response surface method(RSM). Finally, a optimization problem was solved with a objective function of blade weight and a constraint of allowable stress to achieve a optimal structural design of blade.

Optimal Design of the Monolithic Flexure Mount for Optical Mirror Using Response Surface Method (반응표면법을 이용한 광학미러용 일체형 유연힌지 마운트 최적설계)

  • Kyoungho Lee;Byounguk Nam;Sungsik Nam
    • Journal of the Korea Institute of Military Science and Technology
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    • v.26 no.3
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    • pp.205-213
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    • 2023
  • An optimal design of a simple beam-shaped flexure hinge mount supporting an optical mirror is presented. An optical mirror assembly is an opto-mechanically coupled system as the optical and mechanical behaviors interact. This side-supporting mount is flexible in the radial direction and rigid for the remaining degrees of freedom to support the mirror without transferring thermal load. Through thermo-elastic, optical and eigenvalue analysis, opto-mechanical performance was predicted to establish the objective functions for optimization. The key design parameters for this flexure are the thickness and length. To find the optimal values of design parameters, response surface analysis was performed using the design of experiment based on nested FCD. Optimal design candidates were derived from the response surface analysis, and the optimal design shape was confirmed through Opto-mechanical performance validation analysis.

Optimization of Extraction Conditions of Antioxidant Activity and Bioactive Compounds from Rice Bran by Response Surface Methodology (반응표면분석법을 이용한 미강으로부터 항산화 활성 및 생리활성물질의 초음파 추출조건 최적화)

  • Gam, Da Hye;Jo, Jae Min;Jung, Hyun Jin;Kim, Jin Woo
    • Applied Chemistry for Engineering
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    • v.29 no.6
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    • pp.726-733
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    • 2018
  • The rice's waste byproduct is known as a rice bran and produced annually about 400,000 to 600,000 tons. Most of the rice bran are used as a livestock feed or waste disposal, and needed to be used to produce high-added substances, such as bioactive materials. In this study, extraction conditions of the ultrasound-assisted extraction (UAE) of the rice bran were optimized using a statistically-based optimization. The influence of extraction variables including the extraction time ($X_1$), extraction temperature ($X_2$) and ethanol concentration ($X_3$) were investigated using the response surface methodology in order to determine optimum extraction conditions which maximize total phenolic compounds (TPC), total flavonoid compounds (TFC) and electron donating abilities (EDA). The optimal UAE from rice bran was achieved under the extraction temperature of $94.9^{\circ}C$, extraction time of 41.6 minute and ethanol concentration of 74.0% (v/v) with maximum yields of TPC 2.78 mg GAE/g DM, TFC 1.63 mg QE/g DM and EDA 42.86%. The UAE process shows its potential to the extraction of bioactive and antioxidant compounds from rice bran in a short extraction time and low temperature. Also, it is proposed that rice bran could be considered as food additives and cosmeceutical products.