• Elastomers and Composites
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• v.40 no.3
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• pp.196-203
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• 2005

In this work, the engine oil resistant evaluation and breakdown analysis of room temperature vulcanizing silicone adhesives were performed through the surface properties, thermal stabilities, adhesive strength, and morphology measurements. As a result, the permeation of engine oil into adhesive specimens was carried out from surface to center in the specimens. And the oil content in the adhesive specimens was increased and the Si-O-Si bond of the adhesives was decomposed with increasing the aging time. The TGA results indicated that the thermal degradation was mainly occurred at under and surfaces of the specimens. The tensile strength, elongation, and adhesive strength of the adhesives were significantly decreased after the engine oil resistant tests, which could be attributed to the initial lose of adhesive properties resulting from the engine oil absorption and thermal aging. And the failure mode of the adhesive specimens was changed from cohesive failure to interfacial failure.

• The Korean Journal of Rheology
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• v.8 no.2
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• pp.129-138
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• 1996

접착강도는 접착제의 점탄성을 반영한 온도·속도 의존성을 나타낸다는 것이 잘 알 려져있다. 특히 유리전이온도(Tg)에서의 역학적 완화기구가 접착층의 변형을 수반하는 접착 층의 변형을 수반하는 접착강도에 크게 영향을 미치고 있다. 또한 접착계의 모드I의 변형에 너지 해방율(GIC)를 측정할때에도 접착제의 변형과 파괴가 발생하기 접착제의 점탄성이 그 값에 어떠한 영향을 미치는 지에 흥미가 깊다. 본 연구에서는 2종류의 에폭시 수지를 블랜 드한 접착제를 이용하여 일정한 측정조건에서 인장 접착강도와 GIC의 상관관계에 대하여서 도 토론하였다.

• Journal of the Korean Wood Science and Technology
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• v.24 no.2
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• pp.61-70
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• 1996

침엽수재(針葉樹材)(Radiata pine, Pinus radiata)MDF와 활엽수재(闊葉樹材)(Rubber wood, Hevea brasiliensis)MDF 각 1종을 대상으로 MDF를 제조하기 전 원료(原料) 섬유(纖維)의 미세(微細) 구조(構造) 및 내부결합력 시험 후 MDF의 파괴면(破壞面)에서 섬유표면(纖維表面)에 접착제(接着劑)가 도포(塗布)된 형태를 주사전자현미경(走査電子顯微鏡)으로 관찰하였다. 원료 섬유는 침(針) 활엽수재(闊葉樹材) 모두 fiber twisting 및 shrinkage fold 등이 관찰되었다. 침엽수재(針葉樹材)의 경우는 유연벽공부(有緣壁孔部)에서 유연벽공(有緣壁孔)이 없는 부분에 비하여 shrinkage fold의 발생 빈도가 낮고 표면(表面) 박리(剝離)는 가도관(假導管) 중 벽공이 없는 부분에서 관찰되었다. 활엽수재(闊葉樹材) 목섬유(木纖維)는 침엽수재(針葉樹材)와 마찬가지로 shrinkage fold가 관찰되었으나 표면(表面) 박리(剝離)는 거의 관찰되지 않았다. 활엽수(闊葉樹) 섬유(纖維)에서는 벽공의 유무에 따른 shrinkage fold의 차이(差異)가 거의 관찰되지 않았는데 이는 목섬유(木纖維)가 침엽수(針葉樹) 가도관(假導管)보다 작은 단벽공(單壁孔)을 갖기 때문으로 생각된다. 또 방사유세포(放射柔細胞)와 가도관(假導管) 및 목섬유(木纖維)의 박리(剝離) 부분(部分)에는 융기부(隆起部)가 관찰되었다. 내부결합력 시험후 나타난 파괴면을 통하여 접착제 분포를 관찰한 결과 거의 모든 섬유(纖維)들이 접착제(接着劑)로 둘러싸여 있었으며 섬유(纖維)간 접착형태(接着形態)도 매우 다양하였다. 침활엽수재(針闊葉樹材)간에 강도(强度)의 차이는 있었지만 파괴(破壞) 형태(形態)는 큰 차이를 나타내지 않았다. 즉 침활엽수(針闊葉樹) 모두 접착층(接着層)이 아닌 섬유(纖維)에서 파괴(破壞)가 발생하였으며 섬유에서 박리(剝離)된, 세포벽(細胞壁)의 일부가 다른 섬유(纖維)의 표면(表面)에 남아있는 형태와 섬유(纖維) 표면(表面)에서 떨어져 나간 형태로 관찰되었다. 세포 구성이 단순한 침엽수(針葉樹) MDF에 비하여 유세포(柔細胞)와 도관(導管) 및 목섬유(木纖維)의 파편들이 활엽수(闊葉樹) MDF에서는 다양(多樣)하게 분포하였다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.5 s.176
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• pp.1203-1214
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• 2000

In this paper, a failure model for co-cured steel-composite tubular single lap joints has been proposed incorporating the nonlinear mechanical behavior of steel adherends and different failure mode s such as steel adherend failure and composite adherend failure. The characteristics of the co-cured steel-composite tubular single lap joint were investigated with respect to the test temperature, the stacking sequence of composite adherend, the thickness ratio of steel adherend to composite adherend, and the scarf ratio of steel adherend. Thus, the optimum design method for the co-cured steel-composite tubular single lap joint was suggested.

• Composites Research
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• v.19 no.4
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• pp.15-22
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• 2006

One of the primary factors limiting the application of composite-metal adhesively bonded joints in structural design is the lack of a good evaluation tool for the interfacial strength to predict the load bearing capacity of boned joints. In this paper composite-steel adhesion strength is evaluated in terms of stress intensity factor and fracture toughness of the interface corner. The load bearing capacity of double lap joints, fabricated by co-cured bonding of composite-steel adherends has been determined using fracture mechanical analysis. Bi-material interface comer stress singularity and its order are presented. Finally stress intensities and fracture toughness of the wedge shape bi-material interface corner are determined. Double lap joint failure locus and its mixed mode crack propagation criterion on $K_1-K_{11}$ plane have been developed by tension tests with different bond lengths.

• Proceedings of the KWS Conference
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• 2001.05a
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• pp.13-19
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• 2001

• Journal of Adhesion and Interface
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• v.16 no.2
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• pp.69-75
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• 2015

Stone board for the rock bed was needed to reduce weight using thin thickness and reinforced materials. In this work, stone/wood board for rock bed was studied. Stone and wood were attached to reduce total weight of stone for rock bed. For reinforcing wood heat treatment method was used to change surface and mechanical properties. Mechanical strength of heat treated wood increased more than neat condition. The optimum heat treatment condition was set on $100^{\circ}C$ under tensile, flexural loads whereas surface energy was also obtained by contact angle measurement. Optimum adhesive condition was to get the maximum adhesion between stone and wood. Lap shear test was performed for stone/wood board with different adhesives such as amine type epoxy, polyurethane, chloro-rubber and vinyl chloride acetate type. Fracture surface of lap shear test was shown at wood fracture part on stone using amine type epoxy adhesive. It was found that for high adhesion between stone and wood the optimum adhesive was epoxy type for the rock bed.

• Journal of Korean Society of Forest Science
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• v.96 no.1
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• pp.54-57
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• 2007

Urea-formaldehyde (UF) resin was formulated similarly to plywood resin in the laboratory. The synthesized UF resin adhesive was mixed with extender, filler and acid catalyst. The mixture contained 56.1% total solids and 43.9% water. The mixes was used to bond five Com-Ply types using Korean wood species. The Com-Ply made were tested for shear strength and wood failure according to KS F 3101 ordinary plywood as well as for bending strength per KS F 3104 particleboard. The performance test results showed good strength properties for all Com-Ply types made in this study. This result represented that the UF resin adhesive mix was adequate for bonding Com-Ply with domestic wood species.

• Transactions of the Korean Society of Mechanical Engineers
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• v.4 no.3
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• pp.105-112
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• 1980

정현적 응력을 받고 있는 정탄성 결합부의 에너지 손실을 여러 가지 인자를 고려하여 구하였다. 탄성접착결합부의 해를 구하고 탄성해의 전단계수를 복소전단계수로 대치하여 점탄성 접착결 합부의 전단변형분포를 구하였다. 주어진 접착제의 최대강쇠현상은 접착제의 강성과 피접착물의 비를 증가 시킴으로서 얻을 수 있다. 구조적 결합부에서 파괴가 일어나지 않도록 피접착부와의 강성비를 결정함에 있어 주의를 요한다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.12
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• pp.2662-2669
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• 2002

Recently structural applications of adhesive bonding method have been increased extensively in automobile industry. Adhesively-bonded joints which are used in automobile field are exposed to various environmental conditions. In this study, several environmental factors were concerned to evaluate their effects on the adhesive strength such as air temperature, water temperature, exposed time in water. The specimens are exposed for 1, 10 and 100 hours at various air temperatures to evaluate the effects of the air and water temperature on the adhesive strength. It is proved that the adhesive strength decrease with rising the air and water temperature, and the adhesive strength decrease steeply at the higher temperature with increasing the exposure time in water.