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The surface morphology control of the polymeric material using a linear ion source (선형 이온 소스 적용을 통한 폴리머 소재의 표면구조 제어)

  • Sin, Min-Ho;Kim, Byeong-Jun;Park, Yeong-Bae;Kim, Do-Geun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.141.2-141.2
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    • 2016
  • 디스플레이, 센서 등 전자소자는 소형화 단계를 지나 인체 부착형 소자로의 발전을 요구하고 있다. 인체 부착을 위해서는 민감한 피부에 장시간 부착시 무해성과 탈부착의 자유로움이 요구되기에 기존의 화학물질을 활용한 접착 방식에서 개코도마뱀 또는 딱정벌레 발바닥에서 영감을 얻은 자연모사형 건식 접착 방식에 대한 연구가 활발하게 진행되고 있다. 폴리머를 이용하여 자연모사형 마이크로/나노구조 형성은 기계적으로 가공된 금형 몰딩과 후처리를 통한 매우 복잡한 공정이 요구된다. 본 연구에서는 이러한 복잡한 공정을 단순화하기 위해서 폴리머 소재에 플라즈마를 활용한 나노구조를 형성하는 방법을 소개하고자 하며, 건식 접착용 폴리머 소재(PMMA, PDMS)에 따른 표면구조 변화와 표면에너지 변화에 대한 연구를 수행하였다. 플라즈마 표면처리를 위해서 본 연구실에서 자체 개발한 선형이온소스를 활용하였으며 입사에너지, 노출시간, 사용가스에 따른 표면형상 변화를 주사전자현미경을 활용하여 관찰하였다. 또한 처리조건에 따른 표면에너지 변화를 확인하기 위해 물접촉각 변화를 측정하였다. PMMA는 입사에너지, 노출시간이 증가함에 따라 쉽게 나노기둥구조가 형성되었으나, 과도한 입사에너지 또는 노출시간에서는 표면구조가 에칭되면서 무너지는 것이 관찰되었다. 또한 PDMS는 동일한 조건에서 주름구조 형태를 보였으며 노출시간이 증가할수록 주름구조의 간격이 늘어남을 확인하였다. 본 연구 결과를 통해 나노 구조를 쉽게 제어할 수 있는 PMMA가 피부 부착형 접착 패치에 응용이 가능할 것으로 기대된다.

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Ultrasonic Inspection Technology of Defect Detection of Propellant/Liner Debond & Propellant Microcrack (초음파를 이용한 추진제/라이너 미접착 및 추진제 미세 크랙의 결함 검출 기법)

  • Na, Sung-Youb
    • Journal of the Korean Society of Propulsion Engineers
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    • v.11 no.1
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    • pp.34-42
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    • 2007
  • Ultrasonic inspection method is more profitable than X-ray radiographic inspection in cost and effect of defect detection such as debond, damage, and it doesn't need special constructions. The method can also be a possible real time inspection with safety. This report explains 1)the experiment and analysis of ultrasonic property of solid propellant, 2)the inspection methods of propellant/liner debond by inside or outside inspection, and 3)the inspection methods of propellant microcrack by damage. From the results, it is possible to detect the defect of propellant/liner debond by inside or outside inspection. Futhermore, it can be possible to detect the propellant microcrack caused by damage using the ultrasonic attenuation.

Compression and Adhesion Characteristics of Rice Dough Added with Cellulose Ethers Using Rheometer (유변물성 측정기를 이용한 셀룰로오스 에테르가 첨가된 쌀 반죽의 압축 및 접착 특성)

  • Um, In Chul;Yoo, Young Jin
    • Current Research on Agriculture and Life Sciences
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    • v.32 no.1
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    • pp.18-23
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    • 2014
  • The present study examined the effect of cellulose ether on the compression and adhesion characteristics of rice dough using a rheometer. When increasing the amount of hydroxypropyl methylcellulose (HPMC), the adhesion strength consistently increased. However, the compression strength of the rice dough was the highest with 2% HPMC. When increasing the molecular weight and decreasing the water content, the compression and adhesion strength of the rice dough were both increased. Furthermore, the substitution type and degree of cellulose ether were also found to be key factors determining the compression and adhesion strength of the rice dough.

Improvement of Adhesion of Footwear Nylon Fabric by Corona Treatment (코로나 처리를 이용한 신발용 나일론 직물의 접착력 향상)

  • Lee, Jae Ho
    • Journal of Adhesion and Interface
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    • v.7 no.3
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    • pp.26-33
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    • 2006
  • Nylon fabrics were corona treated with different current intensity (5, 10, 15, 20 A) and feeding speed (5, 10, 15 m/min). We confirmed the change of nylon fabrics surface using X-ray diffraction apparatus, scanning electron microscopy (SEM) and X-ray photoelectron spectrometer (ESCALAB). And the change of physical properties through measuring the tensile strength, tear strength, bonding and wet bonding strength. Thermosetting reactive polyurethane hot melt adhesive was used in the adhesion of nylon fabrics. Functional groups were introduced on nylon fabric surface by treating the fabrics in air atmosphere with corona discharge, and the result adhesion was improved. Bonding strength of the nylon fabric treated with corona was increased with increasing current intensity and decreasing feeding speed.

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Studies of Attachment of Fibroblasts on Microcarriers for the Production of Tissue Plasminogen Activator (TPA 생산을 위한 섬유 세포의 미립 담체와의 접착성에 관한 연구)

  • 강재구;박형환;이현용
    • KSBB Journal
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    • v.4 no.2
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    • pp.104-109
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    • 1989
  • Among commercially available five different types of micro-carriers, collagen coated Cytodex III supports the best cell growth and production of Tissue type Plasminogen Activator from fibroblasts for all three various kinds of media(FBS, horse serum containing and serum free medium). 95% of attachment yield is obtained with Cytodex III in FBS containing medium compared to about 70% in serum free medium. However, higher production of TPA can be observed in horse serum containing and serum free media as $1.2\;\mu\textrm{g}/\;ml$ and $0.7 \mu\textrm{g}/\;ml$, respectively with $5.5{\times}10^6$ cells/ ml and $0.7{\times}10^6$ cells/ ml under perfusiom chemostat operations.

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Evaluation of Laminate Property using Caulplate Application (카울플레이트 적용을 통한 라미네이트 특성 평가)

  • Park, Dong-Cheol;Kim, Yun-Hae
    • Composites Research
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    • v.29 no.5
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    • pp.231-235
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    • 2016
  • In this study, integrated co-bonded panels with the same configuration of hat stiffeners were fabricated and measured for ply waviness phenomenon. Total specimens consisted of 2 types; 1) the general co-bonded panel and 2) the co-bonded panel with caul plate made of carbon epoxy composite materials. The first general co-bonded panel specimen exhibited that laminate thickness on the stiffener location area was much thicker than the non-stiffener area and, there was ply waviness with 0.61 mm height and 3.29 mm length. In the second co-bonded panel specimen, the reduced waviness with 0.22 mm height and 1.37 length resulted in more than 50% improvements, which is due to the uniform pressure distribution of co-bonded interface by caul plate.

Preventing marine organisms adhesion by oil-infused PDMS (오일이 주입된 PDMS를 이용한 해양생물의 부착방지 방법에 대한 고찰)

  • Kim, Su-Yeong;Yun, Yeong-Cheol;Im, Chae-Gang;Jeong, Yong-Chan;Lee, Su-Yeol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2018.06a
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    • pp.45-45
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    • 2018
  • 홍합, 따개비 등의 접착성 해양생물은 선박의 하부나 발전소 해수 공급용 튜브에 부착하여 운영 효율을 저하 시키고, 냉각기기 고장을 유발하는 파울링(Fouling) 문제를 야기시킨다. 일반적으로 이러한 문제에 대응하기 위해서 초접착성 해양생물이 주로 부착하는 부위에 $Cu_2O$, ZnO 등을 포함한 유기화합물로 표면처리를 하여 부착방지를 하고 있지만, 이 소재들을 장시간 사용 시 해양 오염 및 부식을 가속화하는 문제를 초례하기 때문에 최근에는 사용을 금지하고 있다. 이러한 유해성 소재 문제를 해결하고자 친환경적이고 부작용이 없는 초접착성 해양생물 부착방지 소재를 개발하고자 하였다. 본 연구에서는 낮은 표면장력을 갖는 PDMS(Polydimethylsiloxane) 소재를 기반으로 소수성 oil을 침투시킨 I-PDMS(Oil-Polydimethylsiloxane) 표면처리법을 고안하였고, 이 방법을 활용하여 초접착성 해양생물에 대한 부착방지 성능을 향상시키고자 하였다. 기존의 개발품들 보다 성능이 향상된 I-PDMS 제조하고자, Nano-indentation을 이용한 기계적 특성 평가, X컷 및 cross-cut을 이용한 부착력 평가, 실제 바다환경에서 해양생물의 부착력 시험, 바다 환경을 모사한 수조에서의 I-PDMS와 비교군 기판에서의 홍합 거동, 홍합과 기판의 접착강도 시험, 해양 미생물 평가를 실시하였으며, 이를 통해서 I-PDMS 성능 및 내구성을 입증하고자 하였다.

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Measurement of Surface Energy and Intrinsic Work of Adhesion Using Johnson-Kendall-Roberts (JKR) Technique (Johnson-Kendall-Roberts (JKR) 기법을 이용한 표면 에너지 및 고유접착에너지 측정)

  • Lee, Dae Ho;Lee, Dong Yun;Cho, Kilwon
    • Journal of Adhesion and Interface
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    • v.5 no.3
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    • pp.18-22
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    • 2004
  • By using JKR technique, the surface energy of a solid material and the intrinsic work of adhesion between two materials were determined. JKR technique is based on the contact mechanics, and is now being accepted as a new method which can overcome the demerits of the existing test methods such as contact angle measurement and other adhesion test. In this study, the surface energy of polydimethylsiloxane (PDMS) is measured by JKR method and the experimental results and the applicability of JKR apparatus were discussed.

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Study on Adhesion and Mechanical Properties of Adhesive Resin Using Microcapsule with Isocyanate Compound (이소시아네이트를 포함하는 Microcapsule을 사용한 접착수지의 특성에 관한 연구)

  • Kim, Dong Ho;Kim, Gu Ni
    • Journal of Adhesion and Interface
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    • v.15 no.3
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    • pp.109-115
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    • 2014
  • In this study, we synthesized and identified microcapsule containing isocyanate, and investigated the mechanical and adhesion properties of polyurethane resin by adding microcapsule. We found out that the core material of microcapsule and the component weight fraction of microcapsule from the FT-IR and TGA analysis. From the results of adhesion and mechanical property tests, we confirmed that in case of using microcapsule for adhesive resin composition, adhesion strength, tensile strength and abrasion were improved by cross-linking reaction between urethane and IPDI in microcapsule.

A Study on Adhesion Characteristics for Rubber Parts of Footwear Containing Plasma Treatment (플라즈마 처리에 의한 신발용 고무부품의 접착특성 연구)

  • Jeong, Booyoung;Cheon, Jungmi;Lee, Sangjin;Moon, Jinbok;Chun, Jaehwan
    • Journal of Adhesion and Interface
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    • v.14 no.3
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    • pp.111-116
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    • 2013
  • In this study, we studied surface and adhesion properties with plasma treatment for substitution of buffing and solvent-cleaning in footwear adhesion process. The distance between nozzle and rubber parts was decreased with decreasing the contact angle. And when a speed of plasma treatment increased, the contact angle increased. The result of surface roughness, Ra and Rz increased in 20% and 16% after the plasma treatment. The distance of between nozzle and rubber parts was decreased with decreasing the peel strength. And the speed of plasma treatment was increased with decreasing the peel strength.