• Title/Summary/Keyword: 재접착제

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An in Vitro Study of the Effects of Different Dentin Bonding Agents on the Prevention of Tooth Discoloration and the Sealing Ability of Calcium Silicate-Based Cement in Regenerative Endodontic Procedures (치수재혈관화 술식에서 다양한 상아질 접착제가 치아 변색과 칼슘 실리케이트 시멘트의 밀폐 효과에 미치는 영향에 대한 실험실적 연구)

  • Jieun Han;Gimin Kim;Jaesik Lee
    • Journal of the korean academy of Pediatric Dentistry
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    • v.50 no.3
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    • pp.277-291
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    • 2023
  • This study aimed to compare the effects of applying different types of dentin bonding agents (DBAs) on tooth and on the sealing ability of CSC in regenerative endodontic procedures (REPs). Specimens were made from 120 human first premolars and categorized into the following groups based on the presence and the type of DBA: Group I, no bonding; Group II, One-Step; Group III, Clearfil SE Bond; and Group IV, Single Bond Universal. Subsequently, the groups were categorized into Subgroup a and Subgroup b, in which Endocem MTA® Premixed Regular and Biodentine were used, respectively. The CIE L*a*b* on the photos taken prior to TAP placement (S0), 1 week after TAP placement (S1), 2 weeks after TAP placement (S2), 4 weeks after TAP placement (S3) and 2 weeks after CSC placement (S4) was used to assess discoloration. The samples were submerged in a 2% methylene blue solution and magnified by 30 times under a stereomicroscope to assess microleakage. The application of DBA during REP reduced crown discoloration, while Biodentine showed minimal discoloration with or without DBA and regardless of the DBA type. Additionally, the application of DBA did not increase microleakage.

Fabrication and Evaluation of Composite Panel with Hat-shaped Stiffeners (모자(Hat)형 보강재를 가진 복합재 패널의 제작과 평가)

  • Kim, Geon-Hui;Lim, Do-Wan;Choi, Jin-Ho;Kweon, Jin-Hwe;Lee, Tae-Joo;Song, Min-Hwan;Shin, Sang-Joon
    • Composites Research
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    • v.23 no.2
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    • pp.31-39
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    • 2010
  • In this paper, composite panels with hat-shaped stiffeners were made using the co-curing, co-bonding and secondary bonding methods. Co-curing is a manufacturing method in which the hat part and the plate are cured simultaneously in a manner that is more cost effective than other methods. Co-bonding is a method in which the stacked prepregs are cured with other cured parts, and secondary bonding is a method in which cured parts are bonded together using an adhesive. A rubber mold was manufactured for co-curing of composite panel with hat-shaped stiffeners, and finite element analyses were done to evaluate the expanding pressure of the rubber mold consistent with the curing temperature. The manufactured panels were also evaluated using a 3-D measurement tester and an ultrasonic tester. Pull-off tests were performed to evaluate their mechanical properties.

Mechanical Properties of Composite Materials Composed of Structural Steel and Structural Glued Laminated Timber (구조용 강철과 구조용 집성재 복합재료 보의 역학적 성질)

  • Jang, Sangsik;Kim, Yunhui;Jang, Youngik
    • Journal of the Korean Wood Science and Technology
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    • v.37 no.4
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    • pp.300-309
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    • 2009
  • The effective utilization of wood structure is encouraged to preserve natural resources and the global environment. Long-span and large-scale structures are preferred to promote demand for wood. This study attempts to develop new Fire-resistance Composite Material composed of Structural steel and Structural glued laminated timber for long-span and large-scale structures. Prior to take a fire-resistance test, compare properties of bending strength with Composite material composed of Structural steel and Structural glued laminated timber, structural steel and structural provides the stability of the structure, but the structural glued laminated timber has high value elasticity of bending. Using the Composite material will improve structural stability and Eco-friend construction environment.

The Bending Strength Properties and Acoustic Emissions to the Difference of Finger Widths (핑거공차에 따른 휨강도 성능과 AE 특성)

  • Ryu, Hyun-Soo;Ahn, Sang-Yawl;Lee, Gyun-Pil;Park, Han-Min;Byeon, Hee-Seop
    • Journal of the Korean Wood Science and Technology
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    • v.31 no.2
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    • pp.84-91
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    • 2003
  • In this study, the three species (Populus euramericana, Pinus densiflora and Quercus variabilis) were cut to difference (0, 0.15, 0.3, 0.45 mm) between the size of tip and that of root of the finger (DSTR) and jointed with poly vinyl acetate (PVA) and resorcinol-phenol resin (RPR). We described the relationship between the bending strength properties of finger DSTR and the acoustic emission (AE) generated during the bending test. The results were as follows: The AE generation time of finger-jointed specimens with RPR adhesive was earlier than that with PVA adhesive. The AE cumulative event count of finger-jointed specimens with RPR adhesive continuously increased with increasing load and the event count was much more than that with PVA adhesive. Also, the AE cumulative event count for resorcinol-phenol resin adhesive obtained from low load level was abundant. The AE wave in finger-jointed specimens with RPR adhesive could be detected in the below proportional limit load. Therefore, AE signals from bending test are useful for the estimation of strength in finger DSTR specimens.

Study on the Basic Survey and Materials Properties for Conservation of Plastic Artifacts: 'A Bag of Alice - a Fish without Eyes' (플라스틱 작품의 기초조사 및 보존처리 재료 연구: 이인희 '앨리스의 가방 - 눈 없는 물고기'를 중심으로)

  • Han, Ye Bin;Kim, Jung Heum;Beom, Dae Geon
    • Journal of Conservation Science
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    • v.34 no.5
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    • pp.379-385
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    • 2018
  • This study examined the condition of degraded plastic artifacts and conducted materials assessments for conservation treatment. The properties and bond characteristics of five types of adhesives(EVA, PVAc, Cyanoacrylate) were evaluated to select the adhesive most suitable for conservation treatment. The degradation of plastic artifacts caused cracks, peelings, and surface warping. According to the FT-IR analysis, the synthetic resin used in the artifact was estimated to EVA type. The properties of the adhesives were evaluated through acidity, and hardness measurements. The results showed that acidity varies with the type of adhesive, and that the hardness of PVAc was higher than those of EVA. On comparing the bond characteristics of the samples after artificial degradation, it was found that PVAc and Cyanoacrylate increased the chromaticity and hardness of the samples, while EVA was the most stable with relatively little change. Thus, EVA was confirmed to be the most suitable materials for conservation treatment of degraded plastic artifacts. In this study, as the experiment of treatment materials based on actual artifact, it is expected that it could be used a basis research for conservation treatment of plastic artifacts.

Bonding Performance of Glulam Reinforced with Glass Fiber-Reinforced Plastics (유리섬유강화플라스틱 복합집성재의 접착성능)

  • Park, Jun-Chul;Shin, Yoon-Jong;Hong, Soon-Il
    • Journal of the Korean Wood Science and Technology
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    • v.37 no.4
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    • pp.357-363
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    • 2009
  • This study was carried out to investigate whether adhesive used in manufacturing glulam can be used to bond wood and GFRP, when considering working process and economical efficiency. The six different glulams were manufactured, changing the adhesives and the mixing ratios of the adhesives, and investigated by the block shear test and the delamination of the water soaking or boiling water soaking. The three glulams were manufactured, using the resocinol resin based adhesive, the PVAc resin based adhesive and the epoxy resin adhesive, and the other three glulams, using the adhesives mixing resocinol resin and PVAc resin. The block shear strength is higher than $7.1N/mm^2$ in all types, which is standard of KS F3021. However, in the wood failure the block shear strength was the highest as 65.9% in the PVAc. The delamination of glulams glued with PVAc adhesive, which was 1.08% in water soaking and 4.16% in boiling water soaking, was lower than 5.00% which is the standard of KS F 3021, and the adhesive strength is good. In glulams glued with only resocinol resin adhesive, the wood layers were good as 1.26% in the water soaking delamination and 0.00% in the boiling water soaking delamination. The GFRP layers were not good as 21.85% in the water soaking delamination but were good as 1.45% in the boiling water soaking delamination.

Study of UV Degradation of Lacquer and Natural Adhesives Using Lacquer Mixed with Animal Glue (옻과 옻에 아교를 배합한 천연접착제의 자외선에 의한 노화 특성 연구)

  • Ahn, Sunah;Kim, Eun Kyung;Jang, Sungyoon
    • Journal of Conservation Science
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    • v.32 no.4
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    • pp.501-510
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    • 2016
  • In this study, we investigated the degradation of adhesives when exposed to ultraviolet light irradiation using samples of lacquer (L), treated lacquer (TL), lacquer mixed with glue (LG), and urushiol mixed with glue (UG). Four types of film specimens were collected under the ultraviolet exposure time, and gloss test, tensile shear strength test, scanning electron microscope analysis, and infrared spectroscopic analysis were conducted for the specimens. LG and UG showed lowering rate of gloss is somewhat later than L. Also, it was observed that with increasing exposure time to ultraviolet irradiation, the surface of L began to show spherical pits and cracks when the polysaccharide layers started to be exposed, whereas the surfaces of LG and UG remained smooth. The Infrared spectra of L and TL showed that the intensity of the overall peak decreased with increasing ultraviolet irradiation time. There was no change in the peak intensity of LG, but for UG, the peaks at $3013cm^{-1}$, $1593cm^{-1}$ and so on disappeared and the overall intensity declined. The tensile shear strength of LG and UG was maintained or increased as compared to the initial test, whereas the tensile shear strength of L decreased sharply after 600 h. LG and UG exhibited fewer changes as a result of high temperature and humidity conditions, and they retained their strength under UV exposure. These results indicate that LG and UG are more durable than L when subjected to environmental change.

A Scientific Analysis of Decorative Metal Foil Used in Pouch for the Sutra Embroidered with a Sun and Moon Design Designated as National Folklore Cultural Heritage (국가민속문화재 일월수 다라니 주머니 금속 장식지의 과학적 분석)

  • Pak, Seonghee;Park, Serin;Seo, Jeong Hun;Park, Jongseo;Lee, Ryangmi
    • Journal of Conservation Science
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    • v.38 no.2
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    • pp.124-132
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    • 2022
  • Through scientific analysis, this study identified the material characteristics of metal foil decorating the border line and knotting of the National Folklore Cultural Heritage 'Pouch for the Sutra Embroidered with a Sun and Moon Design'. Through Scanning Electron Microscope-Energy Dispersive Spectroscopy results, it was estimated that silver (Ag) and sulfur (S) were present in the metal foil, and silver leaf was also attached to the medium. S may discolor Ag from yellow to black depending on its concsentration and contact time. Yellow color could not be identified in metal foil at present. But there existed an example of the preparation of a gold-colored flat silver thread; therefore, further research is needed to estimate the original color. The lamella was reddish brown on the back. Aluminum, silicon, and iron were also detected and were the main components found in red soil. This is believed to be the red adhesive in traditional flat gold thread and is considered to be an adhesive-related component of the metal foil. From the gas chromatography mass spectrometry results, the adhesive component was confirmed to be animal glue.

Comparison of Mechanical and Interfacial Properties on Chemical Structures of Acrylic and Epoxy Adhesives (아크릴 및 에폭시 접착제의 화학적 구조에 따른 유리섬유 복합재료의 기계적 및 계면 물성 변화 평가)

  • Shin, Pyeong-Su;Kim, Jong-Hyun;Choi, Jin-Yeong;Kwon, Dong-Jun;Lee, Sang-Il;Park, Joung-Man
    • Composites Research
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    • v.29 no.2
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    • pp.79-84
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    • 2016
  • An adhesive can be used to connect two different materials in structures. In comparing with other connecting methods, such as bolt, rivet, and hot melting, the adhesive does not need to use them. It leads to reduce the weight and decrease the stress concentration along the connecting line. This work studied the comparison of mechanical and interfacial properties of commonly-used two adhesives, acrylic type and bisphenol-A epoxy type. Tensile and flexural strength of neat adhesives were also compared. Lap shear test of two adhesives was deduced from the measurement of tensile and fatigue tests. After testing, the failure patterns of adhesive surfaces were observed by a microscope. Tensile strength and mechanical fatigue resistance at using bisphenol-A epoxy adhesive were better than acrylic adhesive. Also adding CNT reinforcement in epoxy adhesive can anticipate mechanical improvement.

Study of Characteristics for Red Adhesive in Traditional Gold Thread (전통 편금사에 사용된 붉은 접착제 특성 연구)

  • Kim, Ji Eun;Yu, Ji A;Han, Ye Bin;Chung, Yong Jae
    • Journal of Conservation Science
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    • v.32 no.1
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    • pp.43-49
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    • 2016
  • Gold threads mean thread made by metal, it is composed various material to gold leaf, adhesive and media. The making technique and using materials of Gold threads are different from region, it can be used to distinguish country of origin. So this study finds characteristics and making techniques for flat gold threads of relics. Standard samples are made of animal glue, lacquer, red lacquer and etc. This materials are based on the scientific investigation of cultural gold threads properties. Then traditional techniques were estimated by comparison and analysis of actual cultural properties and standard samples. As a result of investigating cultural properties, it is similar to the standard sample which are mixed with red soil additives. After analysis of SEM-EDS, it is detected to Al, Si, Fe. So it is to the conclusion that traditional gold thread is made of adhesive mixed with red soil to improve gold color better. And this ways are similar with china that uses animal glue and red soil to adhesive and different from japan that uses lacquer to adhesive. Through this study, it will be used to data and reference for reappearance and making techniques of traditional gold threads.