• Title/Summary/Keyword: 자기포화도

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Characteristics of Constructed SPR (Surface Plasmon Resonance) Sensor System for the Detection of Salmonella and hIgG Antigen-Antibody Reaction. (살모넬라와 면역글로블린(hIgG)의 항원-항체반응 감지를 위한 표면 플라즈몬 공명형 센서시스템의 특성)

  • Um, N.S.;Koh, K.N.;Hahm, S.H.;Kim, J.H.;Lee, S.H.;Kang, S.W.
    • Journal of Sensor Science and Technology
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    • v.7 no.4
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    • pp.263-270
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    • 1998
  • Surface Plasmon Resonance (SPR) sensor system, has rapid response and high sensitivity, can be applicable for detecting reaction times of many biospecific interactions. A SPR sensor system was constructed to detect the antigen-antibody reactions of salmonella and hIgG (human immunoglobulin G). Sensor chips made of gold thin film were used for detecting biological bindings of antigen and antibody reactions. The antigen and antibody reactions for salmonella and hIgG were carried out with various time intervals to observed characteristics of these reactions using SPR sensor system. The resonance angle shift changes were clearly observed at the time of salmonella or hIgG antibody injection into sample cell since each antibody was self-assembled on gold chip surface of the sensor. It was found that the antibodies of salmonella and hIgG reacted with its sensor chip surface in 10 minutes and 60 minutes respectively. And the antigens of both salmonella and hIgG were bound to its antibody within 1 minute.

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Properties of Blocking Filter as a function fo Magnetic Core shapes for Power Line Communication (자심재료의 형상에 따른 전력선 통신용 블로킹 필터의 특성)

  • Kim, Hyun-Sik;Lee, Hae-Yon;Ji, Min-Kwon;Oh, Young-Woo;Byun, Woo-Bong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.230-230
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    • 2007
  • 전력선 통신(Power Line Communication)은 최근 전력선을 이용한 통신기술의 발달과 더불어 세계적으로 관심도가 높아지고 연구 개발 및 자본 투자가 활발히 진행되고 있으며, 안정적인 네트워크를 구성하기 위해서는 고주파 전력선 통신 신호를 차단하는 블로킹 필터가 반드시 적용되어야 한다. 전력선 통신용 블로킹 필터는 광대역의 주파수 특성과 높은 신호감쇄 특성 및 대전류 특성이 요구되며, 이러한 특성을 구현하기 위해서는 블로킹 필터의 핵심부품인 자심재료의 고투자율 및 대전류화가 이루어져야 한다. 따라서 본 연구에서는 우수한 전 자기적 특성이 균일하게 유지되고, 전력선에 흐르는 대전류에 의한 자심재료의 포화가 발생하지 않도륵 새로운 자심 재료를 설계하여, 전력선 통신을 적용한 홈 네트워크 구축의 핵심 부품인 광대역 블로킹 필터를 개발하고자 하였다. 2350과 0.3 T의 투자율과 포화자속 밀도를 갖는 EI 형상의 자심재료를 해석모델로 설정하고 다중 에어 갭의 위치에 따른 전류와 자속밀도 변화를 유한요소 해석법으로 분석한 결과 자심재료의 대전류 특성에 지배적인 영향을 미치는 에어 캡의 삽입 위치를 알 수 있었고, 새로운 해석 모델인 I 형상의 로드(ROD) 코어에 대해 수치해석을 수행하여, 100A의 통전 전류에서도 자기적으로 포화되지 않고 인덕턴스의 정밀 제어가 가능하고, 특성의 신뢰성과 대전류에 대한 안정성을 증가시킬 수 있는 인덕터를 설계하였다. 또한 수동소자를 이용한 LC 공진회로를 기본 구성으로 하고, 주파수 대역, 신호 감쇄율과 대전류 특성, 상용화를 고려하여 블로킹 필터 회로를 설계하였으며, 유한요소해석법을 적용한 전자장 모의해석을 통하여 최소의 크기를 갖는 I 형상의 자심재료에 $6{\Phi}$의 에나멜 동선을 6.5턴, 6턴 권선하여 2.5, $2.15\;{\mu}H$의 인덕턴스를 갖는 직렬 인덕터를 구현하였고 블로킹 필터를 구성하였다. 주파수에 따른 신호감쇄 특성을 5 Hz~1 MHz의 주파수 범위에서 측정한 결과 약 490 kHz~450 kHz의 주파수 대역에서 -70dB의 신호감쇄 특성을 나타냈다. 본 연구를 통해 개발된 100A급 광대역 블로킹 필터가 적용되어 상용화 될 수 있을 것으로 판단되며, 또한 모뎀 통신 주파수 대역에서 -70dB 이상의 높은 감쇄 특성을 갖기 때문에 신호차단 특성이 보다 우수할 것으로 사료된다.

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Preparation and characterization of magnetic nanoparticles with two kinds of core/shell structures (핵/껍질 구조를 가진 두 종류의 자기 나노입자의 제조와 특성비교)

  • 고영재;손인호;김영국;동성용;이근진;박규섭
    • Journal of the Korean Vacuum Society
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    • v.10 no.1
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    • pp.87-92
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    • 2001
  • Magnetic Fe-Co(C) nanocapsules and Fe-Co nanoparticles were prepared by arc-discharge in two kinds of atmospheres, i.e. methane and a mixture of ($H_2$+Ar), respectively. Characterization and magnetic properties of this two kinds of ultrafine particles were investigated systematically by means of X-ray diffraction, Mssbauer spectroscopy, X-ray photoelectron spectroscopy, transmission electron microscopy, energy disperse spectroscopy analysis, chemical analysis, oxygen determination and magnetization measurement. Effects of carbon element, decomposed from a methane atmosphere in carbon arc process, on phase structures, magnetic states and surface characterization were studied in comparison to that of Ar element. Two ultrafine particles showed a little difference in the weight ratio of (Fe/co) and the size for Fe-Co nanoparticles was about two times bigger than Fe-Co(C) nanocapsules. The saturation magnetization of Fe-Co (C) nanocapsules was about 8% higher than that of Fe-Co nanoparticles while their phase constitutions were similar. Although no carbon could be detected by XRD measurement because of extremely thin shells on the surfaces of the cores, it is still believed that they are carbon and oxygen layers.

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B-H Loop Measurement of a High Tensile Steel Plate (사각판재형 강재의 자기특성측정)

  • Kim, Young-Hak;Kim, Ki-Chan;Shin, Kwang-Ho;Kim, Hwi-Seok;Yoon, Kwan-Seob;Yang, Chang-Seob
    • Journal of the Korean Magnetics Society
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    • v.20 no.3
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    • pp.94-99
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    • 2010
  • Minor B-H loop measurement for a rectangular high tensile steel was obtained by using Labview. A ferrite cores of high permeance with primary and secondary windings on the steel plate were used to form a closed loop of magnetic flux. To compensate errors due to an extremely small gap between a pair of ferrite core, and between the ferrite core and the rectangular high tensile steel, quadratic function of least square method was used. Also a 3D FEM magnetic analysis tool was used to measure H and B of the steel. B-H loop of the high tensile steel plate can be measured up to 520 A/m of a magnetic field and 0.15 T of a magnetic flux density.

Carrier-enhanced Ferromagnetism in Cr-doped ZnO (Cr이 치환된 ZnO에서 나르개에 의한 강자성의 향상)

  • Sim, Jae-Ho;Kim, Hyo-Jin;Kim, Do-Jin;Ihm, Young-Eon;Yoon, Soon-Kil;Kim, Hyun-Jung;Choo, Woong-Kil
    • Journal of the Korean Magnetics Society
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    • v.15 no.3
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    • pp.181-185
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    • 2005
  • We have investigated the effects of Al codoping on the structural, electrical transport, and magnetic properties of oxide diluted magnetic semiconductor $Zn_{1-x}Cr_xO$ thin films prepared by reactive sputtering. Nondoped $Zn_{0.99}Cr_{0.01}O$ thin films show semiconducting transport behavior and weak ferromagnetic characteristic. The Al doping increases the carrier concentration and results in an decrease of resistivity and metal-insulator transition behavior. With increasing carrier concentration, the magnetic properties drastically change, exhibiting a remarkable increase of the saturation magnetization. These results show carrier-enhanced ferromagnetic order in Cr-doped ZnO.

Magnetic Properties of (Fe, Co)-Al-B-Nb Nanocrystalline Alloys on Composition and Annealing Temperature ((Fe, Co)-Al-B-Nb 초미세결정립합금의 조성 및 열처리온도에 대한 자기적 특성변화)

  • 강대병;김택기;조용수
    • Journal of the Korean Magnetics Society
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    • v.5 no.1
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    • pp.1-7
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    • 1995
  • ${(Fe_{0.85}Co_{0.15})}_{75}Al_{7}B_{18-x}Nb_{x}(x=2,\;4\;and\;6\;at%)\;and\;{(Fe_{0.85}Co_{0.15})}_{75}Al_{y}B_{21-y}Nb_{4}(y=3,\;5,\;7,\;9\;at%)$ alloys were prepared by a single-roll quenching method. Microstructure and magnetic properties of the alloys such as saturation magnetization, initial permeability, coercive force and power loss have been investigated as functions of composition and armea1ing temperature. Nanocrystallines are obtained by armealing of as-prepared amorphous alloys in all compositions except the alloy of 9 at% AI. Saturation magnetization increases after armea1ing and, decreases with Nb content. However, AI and B affects the saturation magnetization insignificantly. Initial perrreability of nanocrystallized alloy at 50 kHz is improved roore than twice compared to that of the as-prepared alloy. Coercive force and core loss reach less than half after armea1ing.

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Effects of Metal Ion Mole Ratio and Calcination Temperatures on Magnetic Properties and Microstructure of Ba2Co2Fe12O22 Powders Synthesized by Solid State Reaction (고상반응법으로 제조된 Ba2Co2Fe12O22분말의 자기적 성질과 미세구조에 미치는 금속이온몰비와 열처리 온도의 영향)

  • Cho, Kwang-Muk;Nam, In-Tak
    • Journal of the Korean Magnetics Society
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    • v.19 no.6
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    • pp.216-221
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    • 2009
  • Y-type barium ferrite $Ba_2Co_2Fe_{12}O_{22}$ was synthesized by a solid state reaction method. Effects of metal ion mole ratio and calcination temperatures on magnetic properties and microstructures of the synthesized powders were investigated. Phase analysis and microstructure observation were performed with a XRD (X-ray diffractometer) and a FESEM (field effect scanning electron microscope), respectively. Magnetic properties of the powders were measured with a VSM (vibrating sample magnetometer). Single phase Y-type was synthesized when metal ion mole fraction $Fe^{3+}:\;Ba^{2+}:\;Co^{2+}$ was 6 : 1 : 1 and calcination temperature was $1050\;{^{\circ}C}$. High saturation magnetization value of 39.1 emu/g was obtained when metal ion mole fraction $Fe^{3+}:\;Ba^{2+}:\;Co^{2+}$ was 8 : 1 : 1 and calcination temperature was $1200\;{^{\circ}C}$.

Magnetic Properties of FeZrBAg Soft Magnetic Thin Films with High Permeability and High Magnetization (고투자율, 고포화자화 FeZrBAg 연자성 박막의 자기적 특성)

  • 민복기;김현식;송재성
    • Journal of the Korean Magnetics Society
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    • v.9 no.6
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    • pp.285-290
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    • 1999
  • The magnetic properties of sputtered amorphous $Fe_{86.7}Zr_{3.3}B_4Ag_6$ thin films, which contains an additional insoluble element Ag, have been investigated as a function of uniaxal field annealing temperature. The amorphous $Fe_{86.7}Zr_{3.3}B_4Ag_6$ thin films produced by relatively low temperature annealing at 40$0^{\circ}C$ for 1 hour was found to have very high permeability of 7800 at 50 MHz, 0.2 mOe, high magnetization of 1.7 T, low coercivity of 1.0 Oe and very low core loss of 1.4 W/cc at 1 MHz, 0.1 T, respectively. It is notable that the permeability and core loss values for various kinds of the soft magnetic thin films reported up to now. The reason for the appearance for the good soft magnetic properties is presumably due to the homogeneous formation of very fine bcc $\alpha$-Fe clusters with the size in the amorphous $Fe_{86.7}Zr_{3.3}B_4Ag_6$ thin films matrix, which can be deduced from the XRD results.

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The Magnetic Properties of Polycrystalline Yttrium Iron Garnet by Ferromagnetic Resonance (강자성공명 현상을 이용한 YIG의 자기적 특성 연구)

  • 김기현;이대하;김영호
    • Journal of the Korean Magnetics Society
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    • v.9 no.1
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    • pp.7-16
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    • 1999
  • Stoichiometric and nonstoichiometric $Y_{3-x}Fe_{5+x}O_{12})$ polycrystalline samples (x=0.00, 0.05, 0.10, 0.30, -0.05, -0.10, -0.30) were prepared by solid state reaction method. The magnetic properties of the sample were investigated by FMR (ferromagnetic resonance) technique at microwave frequency 5.11 GHz (G-band) and 23.39 GHz (K-band) respectively. The spectroscopic splitting factor g were estimated to be 2.04~2.35 from the derivative absorption lines. As the samples became yttrium $(Y^{3+})$ excess and iron $(Fe^{3+})$ excess, Magnetizations were decreased. But resonance linewidth were increased. To investigate the anisotropy, the angular dependence of resonance magnetic fields were measured. Angular dependence of effective magnetizations were measured by FMR from 77 K to 300 K at K-band microwave frequency (23.39 GHz) and the saturation magnetizations were measured by VSM. The Bloch coefficients B and C were determined by fitting. $M_{eff}(0)$ was obtained by the extrapolation from 80 K. From this result, the spin wave stiffness constant D $(about\; 162~206 \;eV{\AA}^2)$and average square range of exchange interaction $$$(about \;5.84~12.13\;{\AA}^2)$ were determined.

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First-Principles Study on the Magnetism and Electronic Structure of Fe Nanostripes (나노 구조 철띠의 자성과 전자구조에 대한 제일원리 연구)

  • Byun, Y.;Lee, J.I.
    • Journal of the Korean Magnetics Society
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    • v.16 no.5
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    • pp.229-233
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    • 2006
  • We investigated the magnetic properties of Fe nanostripes by using the all electron full-potenial linearized augmented plane-wave (FLAPW) energy band method within the generalized gradient approximation (GGA). The magnetic moments of the Fe atoms in the edge Fe chains of the stripes composed of three, five, and seven chains have saturated values of 2.97 or 2.98 ${\mu}_B$, and the values of the center chains are 2.82 ${\mu}_B$ which is similar to that of 2D square lattice. The charge and spin density contour plots showed that the flat distribution in the edge region of the stripes, and it is due to the spilled out p-electrons from the atoms in the edge line. The calculated density of states for the edge atoms in the stripes with seven Fe chains showed that the narrowed width compared to that of center atoms due to the band narrowing effect at the edge.