• Applied Chemistry for Engineering
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• v.17 no.3
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• pp.274-279
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• 2006

To synthesize ZnO colloidal solution by a sol-gel process, zinc acetate ($C_{4}H_{6}O_{4}Zn{\cdot}2H_{2}O{\cdot}0.2\;mol$) and lithium hydroxide ($LiOH{\cdot}H_{2}O{\cdot}0.14\;mol$) in the ethanol were added to the solution containing a dispersing agent, hydroxypropyl cellulose (HPC). The nanosize and physical shape of the synthesized ZnO particles were determined by HPC acting as the dispersing agent. Nanosized ZnO particles were also obtained by a precipitation method based on zinc-2-ethylhexagonate. The precipitates were characterized by DLS, XRD, FE-SEM, and UV-vis. As the results, the ZnO colloids tend to self-assemble into a well-ordered hexagonal close-packed structure. The ZnO nanoparticles have an average diameter of nearly 40 nm with a narrow size distribution.

• Tribology and Lubricants
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• v.2 no.1
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• pp.39-45
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• 1986

Wear simulation test have been conducted in mild, severe and transient wear regions by a four-ball wear tester. Wear particles are separatively deposited by the RPD technique, and quantitatively analysed in terms of wear particles size distribution. Characteristics of the wear particle size distribution are compare to the results of wear tests through both weibull parameters and center moment method of the weibull distribution function.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2006.10a
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• pp.423-424
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• 2006

• Proceedings of the Korean Institute of Industrial Safety Conference
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• 1999.06a
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• pp.83-86
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• 1999

산업이 고도로 발달함에 따라 인류는 여러 가지 재해에 직면하게 되며, 재해의 규모나 종류도 다양하게 변화하고 있다. 그 중에서 가장 대표적인 화재나 폭발에 의한 재해는 규모가 클 뿐 아니라 모든 산업현장이나 공정에서 폭 넓게 발생하고 있다. 고체 형태의 가연성 물질의 경우에 입자의 크기, 입도 분포, 분해온도, 입자의 형태, 화학 조성, 가연성액체나 기체와의 혼합 등 여러 가지 복잡한 변수에 의해 연소 위험성이 변화한다. (중략)

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2011.05a
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• pp.149-150
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• 2011

미세화된 반도체 배선에 무전해 은도금을 적용하고자 새로운 Pd 활성화 공정을 제안하였다. 시편 표면에 작은 크기의 Pd 입자를 균일하게 분포시키기 위하여 Pd 활성화 도중 초음파을 가하였다. 추가적인 무전해 은 도금을 실시하여, 초음파에 의한 Pd 입자 분산이 은도금 피막 형성에 미치는 영향에 대하여 고찰하였다.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2000.11a
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• pp.28-28
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• 2000

HTPB/AP/AI 추진제는 none-reinforcing filler가 다량 함유되어 있어 기계적 특성은 바인더와 고체 충진제의 계면 접착력에 따라 크게 영향을 받으며 이를 향상시키기 위해 결합제의 연구가 다수 진행되었고 추진제의 인장 변형율을 증가시키기 위해 HTPB의 관능기수에 따른 가교밀도, 경화제와 경화촉매, 가소제등 최적의 바인더조성을 위해 가능한 원료 및 함량 연구에 많은 노력을 기울여 왔다. 또한 추진제의 주원료로서 AP는 추진제의 성능 및 내탄도 관점에서 입자크기에 따른 연소특성 및 고성능을 위한 충전 분율에 대해 주로 연구되었으며 특히 Oberth와 Farris는 고체추진제 분야에서 많은 업적을 이루었다.(중략)

• Particle and aerosol research
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• v.12 no.3
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• pp.95-102
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• 2016

Controlling exposures to occupational hazards is important for protecting workers. Certified facepiece respirators are recommended when engineering controls do not adequately prevent exposures to airborne nanomaterials. The objective of this study is to carry out the experimental performance test to investigate the fractional efficiencies of the filter media for two grades of facepiece respirators. Experimental performance evaluations were carried out for the test NaCl particles and silver nanoparticles. For media of respirator filter, the penetration of NaCl particles was less than 5% and the most penetrating particle size occurred at about 40 nm. For silver nanoparticles, the most penetrating particle size was about 20nm with higher efficiency than those of NaCl particles. Charge characteristics of airborne nanoparticles is important because the media of respirator filter is made by the electret filter media.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.02a
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• pp.261-261
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• 2010

본 연구에서는 PBMS (Particle Beam Mass Spectrometer)와 ISPM (In-Situ Particle Monitor)을 연계하여 BPSG (Borophosphosilicate Glass) 및 PSG (Phosphosilicate Glass) 박막 증착을 위한 CVD (chemical vapor deposition) 공정 중 발생하는 오염입자 발생특성에 대해 비교 평가하였다. 소스는 TEB (Triethylborate), TEPO (Triethylphosphate) 및 TEOS (Tetraethoxysilane)를 사용하였고, 운반가스 및 반응가스로 He과 $O_2$ 및 $O_3$를 사용하였다. 증착온도와 압력은 각각 $450^{\circ}C$, 200 Torr 이었다. 반응기의 배기라인에 PBMS와 ISPM을 설치하고 500 nm 이하의 입자에 대해 공정단계별 시간에 따른 모니터링 결과 전 공정에 걸쳐 동일한 패턴의 입자발생분포를 보였으며, 특히 PBMS의 경우 ISPM의 입자측정한계인 260 nm 이하의 입자크기도 측정할 수 있었다. 입자발생이 안정적으로 일어나는 증착공정 중 PBMS를 통하여 입자크기를 측정한 결과 BPSG의 경우 약 110 nm, PSG의 경우 약 80 nm의 분포를 나타내었다. 이를 통해 TEB 소스가 배제된 PSG의 경우 BPSG의 경우보다 입자의 성장이 지체됨을 확인하였다. 측정에 대한 신뢰성을 확보하기 위해 PBMS 내의 TEM (Transmission Electron Microscopy) grid를 이용하여 입자를 샘플링 하였고, TEM 분석을 실시한 결과 PBMS 측정결과와 잘 일치하였다. 또한 EDS (Energy Dispersive Spectroscopy) 분석을 통하여 입자성분에 대해 검증하였다.

• Journal of Bio-Environment Control
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• v.12 no.1
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• pp.12-16
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• 2003

The effect of humidifying methods on the mean size of droplets ejected from humidifier and distributions of relative humidity in a graft-taking enhancement system (GTES) was investigated. The mean sizes of droplets ejected from an ultrasonic humidifier and a steam humidifier with electrodes were 7.58$\pm$0.14 and 9.01$\pm$0.06 $\mu$m, respectively. Assuming that the particles ejected from humidifiers were mutually combined with distance, the mean diameter of droplets became larger as the distance apart from the outlet of humidifiers increased. When the relative humidity in GRS was controlled at 90％ using the ultrasonic humidifiers, the average relative humidity at the height of 0.4, 1.1 and 1.8 m were 92.1$\pm$5.3, 90.9$\pm$5.6, and 89.7$\pm$6.8%, respectively. However, the average relative humidity using the steam humidifier with electrodes showed 93.4 $\pm$5.4, 90.7$\pm$5.9, and 89.3$\pm$7.0%, respectively. Therefore, it was concluded that humidification by ultrasonic humidifier would be appropriate for the uniform distribution of relative humidity in GTES.

• Journal of the Korean Applied Science and Technology
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• v.32 no.1
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• pp.165-169
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• 2015

N-propyl-N,N-dimethylethanolamine was directly ultrasonicated in acidic water for 6 minute to give clear stock solutions. The catalytic hydrolysis of N-propyl-N,N-dimethylethanolamine was studied at $30{\sim}55^{\circ}C$ in the presence of uni-lamellar vesicle and mixture of uni- and multi-lamellar aggregates. The difference of rate between uni- and mixture was observed, where uni-lamellar reaction was more catalytic effect. The phase transition temperature of vesicle was $37{\sim}44^{\circ}C$. The particle size of multi-lamellar than that of uni-lamellar of biological membrane was measured more largely.