• Restorative Dentistry and Endodontics
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• v.34 no.2
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• pp.113-119
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• 2009

The purpose of this study was to compare the tensile bond strength of several self-adhesive resin cements bonded to dentin surfaces with different wet conditions. Three self-adhesive resin cements: Rely-X Unicem (3M ESPE, St. Paul, MN. USA). Embrace Wetbond (Pulpdent. Oakland. MA. USA). Maxcem (Kerr. Orange. CA. USA) were used. Extracted sixty human molars were used. Each self-adhesive resin cement was adhered to the dentin specimens (two rectangular sticks from each molar) in different wet conditions. Tensile bond strength were measured using universal testing machine (EZ Test. Shimadzu corporation. Kyoto. Japan) at a crosshead speed of 1.0mm/min. After the testing. bonding failures of specimens were observed by Operative microscope (OPMI pro, Carl Zeiss. Oberkochen, Germany). T-test was used to evaluate the effect of dentin surface wetness. One-way ANOVA test was used to evaluate the tensile bond strength of self-adhesive resin cements in the same condition. Scheffe's test was used for statistical analyzing at the 95% level of confidence. The result showed that wetness of dentin surface didn't affect tensile bond strength of self-adhesive resin cements and Maxcem showed the lowest tensile bond strength.

• Journal of the Korea Institute of Building Construction
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• v.19 no.6
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• pp.485-494
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• 2019

This study is to evaluate the effect of admixtures such as blast-furnace slag and fly ash on adhesion in flexure and tension of polymer cement mortar(PCM) using SAE emulsion. The test specimens are prepared with five polymer-cement ratios and five admixture contents, and tested for flexural strength, adhesion in flexure, tensile strength and adhesion in tension. Based on the test results, no improvement of flexural strength and adhesion in flexure caused by admixtures in PCM can be indicated, but the tensile strength and adhesion in tension is improved due to mixing of the admixtures. In particular, the maximum of adhesion in tension of PCM with P/C 20% and BF content of 10% is 3.35MPa which is about 2.36 times higher than that of ordinary cement mortar, and 1.32 times that of PCM that does not contain any admixture. The average ratio of adhesion in tension to tensile strength of PCM was 48.7%. It is apparent that admixture contents of 5% or 10% could be proposed for improvement of tensile strength and adhesion in tension of PCM.

• Journal of the Korea Institute of Building Construction
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• v.19 no.1
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• pp.47-57
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• 2019

The purpose of this study is to evaluate the improvement effect of adhesion in tension and flexure of polymer cement mortars that have widely used as a repair-reinforcement material in construction field according to adding of polymer dispersions depending on different three types test methods. From the test results, the adhesion performance is improved with a raise in polymer-cement ratio irrespective of the type of polymer. The maximums of A type adhesion in tension, B type adhesion in tension and adhesion in flexure show 1.90 times, 2.17 times and 1.83 times, respectively that of plain cement mortar. The relative strength ratios, B type adhesion in tension and adhesion in flexure of polymer cement mortars to tensile and flexural strengths of plain mortar respectively are in ranges of 50.1% to 101.7% and 73.8% to 132.9% compared to 46.9% of plain mortar. It is apparent that polymer cement mortars with EVA and polymer cement ratios of 10% to 15% are recommended considering its adhesion performance and cost as a repair-reinforcement material in construction field.

• Restorative Dentistry and Endodontics
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• v.29 no.1
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• pp.1-12
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• 2004

이 연구는 발거 소구치에서 5급 와동을 형성하여 접착 시스템 및 와동 위치에 따른 상아질에 대한 접착시스템의 미세 인장결합강도의 차이를 비교, 연구하였다. 접착방법은 resin-modified glass ionomer(Gl), compomer(부식여부에 따라 DE 및 DN군으로 분류), 그리고 상아질 접착제인 Single Bond(SB) 및 Cleayfil SE Bond(SE)와 복합레진(Clearfil AP-X)을 사용한 5개의 실험군으로 분류하였다. 소구치 협측 치경부에 wedge형태의 와동을 형성하고 5종의 접착 시스템을 제조자의 지시에 따라 적용, 충전하여 시편을 제작하여 미세인장결합강도를 측정하고, One-way ANOVA / Duncan's test로 통계분석하였다. SEM 검사는 미세인장결합강도의 시편제작과 동일한 방법으로 시편을 제작한 후 관찰하였다. 실험 결과, 상아질 접착제 및 복합레진(SB, SE)의 미세인장결합강도가 GI보다 높게 나타났고(p<0.05), 치은측이 교합측보다 더 낮게 나타났으며, CI, DE, SE에서 유의성 있게 낮게 나타났다(p<0.05). Compomer에서 conditioning 여부(DN, DE)에 따른 변화는 치은측에서만 유의차 있는 것으로 나타났다. SEM 관찰에서, 교합측의 상아세관은 결합 계면과 평행하게 주행하였고, 치은측에서는 결합계면에 수직으로 주행하는 것으로 관찰되었다.

• The Korean Journal of Rheology
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• v.8 no.2
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• pp.129-138
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• 1996

접착강도는 접착제의 점탄성을 반영한 온도·속도 의존성을 나타낸다는 것이 잘 알 려져있다. 특히 유리전이온도(Tg)에서의 역학적 완화기구가 접착층의 변형을 수반하는 접착 층의 변형을 수반하는 접착강도에 크게 영향을 미치고 있다. 또한 접착계의 모드I의 변형에 너지 해방율(GIC)를 측정할때에도 접착제의 변형과 파괴가 발생하기 접착제의 점탄성이 그 값에 어떠한 영향을 미치는 지에 흥미가 깊다. 본 연구에서는 2종류의 에폭시 수지를 블랜 드한 접착제를 이용하여 일정한 측정조건에서 인장 접착강도와 GIC의 상관관계에 대하여서 도 토론하였다.

• The korean journal of orthodontics
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• v.26 no.3
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• pp.317-324
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• 1996

This study was conducted to evaluate the tensile bond strength of three commercially available glass ionomer cements as orthodontic bracket adhesives. 120 premolars extracted for orthodontic treatment were prepared for bonding and standard edgewise brackets were bonded with Shofu Glaslonomer Cement (Shofu Co., U.S.A.), GC Fuji ItGC Co., Japan), KETAC-CEM(ESPE Co., West Germany) with different P/L ratio. The tensile bond strength was tested by Instron testing device after 24hours and 3months from bonding. After debracketing, bracket bases were examined to determine the failure sites. The results of this study were as follows: 1. KETAC CEM showed the highest bond strength other than measurement after 24 hours and at its original P/L ratio, and seemed to have clinically a proper bond strength. It seemed, however, that both Shofu Giaslonomer Cement and GC Fuji I had an inappropriate bond strength. 2. The incorporation of additional powder into the mixture improved the tensile bond strength. 3. Prolonged storage time improved the tensile bond strength. 4. Of the failure, failure occured at the tooth-adhesive interface(54.2%) was the most common type. The second type of failure(36.7%) was combination type, where part of the adhesive remained on the tooth and part on the bracket. And the last type of failure(9.1%) occured at the adhesive-bracket interface.

• International Journal of Highway Engineering
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• v.4 no.3 s.13
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• pp.15-23
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• 2002

The waterproofing system's performance is known to show a determing by complex interaction of material factors, design details, and the quality of construction, and the waterproofing integrity of waterproofing membranes is determined by the bond to the deck and the amount of damage to the waterproofing membrane. In this research, the basic properties of waterproofing membranes on market and the tensile adhesive chracteristics of waterproofing systems of concrete bridge deck have also been investigated in the view of the damages frequently reported from job site. For the tensile adhesive strength of sheet waterproofing membranes, the results after asphalt concrete paving tends to increase more than before those. The results of the liquid waterproofing membranes are upside-down, and the more concrete has strength, the more strength of tensile adhesive increase. The ambient temperature of asphalt concrete when application of the waterproofing membrane has considerable influence on the performance of waterproofing system. As described above, waterproofing system can be influenced by several factors. If they are not considered under construction, the overlooking will cause the damages of pavement and waterproofing system after traffic opening.

• The korean journal of orthodontics
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• v.26 no.3
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• pp.301-307
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• 1996

The purpose of this study was to evaluate the effect of surface treatment of porcelain on tensile bond strength. To accomplish this purpose, this study was carried out with 120 samples which were divided into 12 groups with each 10 samples, and the first group was not surface treated, groups 2 through 5 underwent single surface treatment, and groups 6 through 12 underwent compound surface treatment. The results were as follows : 1. In statistic, all the single surface-treated groups showed higher tensile bond strength than the non surface-treated group and the sandblasted group showed the highest tensile bond strength as $10.34{\pm}2.50MPa$. 2. All the compound surface-treated groups showed no noticeable difference in the tensile bond strength(9-11.5MPa). 3. In statistic, no significant difference was found between the sandblasted group and the compound surface-treated groups. 4. There was no fracture of porcelain while testing in this study. Above study demonstrated that compound surface treatment or sandblasing, if used single surface treatment, should be employed to guarantee successful clinical application.

• Restorative Dentistry and Endodontics
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• v.31 no.6
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• pp.415-426
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• 2006

In this study, the changes in the degree of conversion (DC) and the microtensile bond strength (MTBS) of self-etching adhesives to dentin was investigated according to the time after curing. The MTBS of Single Bond (SB, 3M ESPE, USA), Clearfil SE Bond (SE, Kuraray, Japan), Xeno-III (XIII, Dentsply, Germany), and Adper Prompt (AP, 3M ESPE, USA) were measured at 48h, at 1 week and after thermocycling for 5,000 cycles between 5$^{\circ}$C and 55$^{\circ}$C. The DC of the adhesives were measured immediately, at 48h and at 7 days after curing using a Fourier Transform Infra-red Spectrometer. The fractured surfaces were also evaluated with scanning electron microscope. The MTBS and DC were significantly increased with time and there was an interaction between the variables of time and material (MTBS, 2-way ANOVA, p = 0.018; DC, Repeated Measures ANOVA, p < 0.001). The low DC was suggested as a cause of the low MTBS of self-etching adhesives, XIII and AP, but the increase in the MTBS of SE and AP after 48h could not be related with the changes in the DC. The microscopic maturation of the adhesive layer might be considered as the cause of increasing bond strength.

• The korean journal of orthodontics
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• v.30 no.1 s.78
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• pp.83-89
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• 2000

The purposes of this study were to evaluate clinical applicability of resin modified glass ionomer cements and to determine the effect of salivary contamination on the tensile bond strength. Fourty extracted human permanent premolars were prepared lot bonding and standard edgewise brackets were bonded with Ortho-One, Fuji Ortho LC, Vitremer and Advance. Fourty extracted human permanent premolars were contaminated with saliva, dried and bonded with same materials above. The tensile bond strength was tested by Instron testing device aster storage in normal saline at ,$37^{\circ}C$ for 24 hours from bonding. The results were as follows : 1. The tensile bond strength of Ortho-One group was $7.68\pm1.76$, Advance group was $7.87\pm2.80$, Fuji Ortho LC group was $4.99\pm2.53$, Vitremer group was $2.80\pm0.88$ MPa. The tensile bond strength in contaminated condition of Ortho-One group was $4.12\pm1.67$, Advance group was $5.37\pm0.68$, Fuji Ortho LC group was $4.41\pm1.61$, Vitremer group was $2.60\pm1.10$ Mpa. 2. Salivary contamination did not affect the tensile bond strength when compared with the uncontaminated enamel group in Fuji Ortho LC and Vitremer (p>0.05) and there was great significant difference in the tensile bond strength of Ortho-One and Advance. 3. Advance, Ortho-One and Fuji Ortho LC seemed to have clinically a proper bond strength.