• Korean Journal of Materials Research
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• v.8 no.5
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• pp.399-407
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• 1998

본 연구에서는 LCD패키지용 이방성 전도 필름의 전기적, 기계적 특성 및 신뢰성에 미치는 접속 변수의 영향을 연구하였다. 이방성 전도 필름을 통한 전기적 전도 현상을 각각의 도전 입자와 기판 사이의 기계적 접촉에 의해 접촉 방향으로만 전류가 흐르게 되는 것이 주되는 전도 기구이다. 따라서 접속 압력에 따라 각각의 도전 입자의 변형으로 기판 사이의 접촉 면적이 변하는데 이방성 전도필름의 접촉 저항은 이런 접촉 변화에 의해 결정된다. 접속 압력에 따라 초기에 접촉 저항은 감소하다가 점차 접촉 저항기가 안정화되는 거동을 보였다. 그러나 높은 접속 압력에서는 오히려 저항치가 약간 증가함을 보였다. 이방성 전도 필름 접속의 접착력을 평가하기 위해 필 테스트(peel test)를 시행하였는데, 접속 압력과 접속 온도를 증가 시킬수록 이방성 전도 필름 접속의 접착력을 평가하기 위해 고온 시효 시험, 온도 사이클링 시험, 고온 고습 시험의 신뢰성 시험을 시행하였으며, 이중 고온 고습 시험이 ACF접속의 전기적, 기계적 특성에 가장 악영향을 주었다. 또 큰 압력으로 접속된 것보다 작은 압력으로 접속되었을 때, 그리고 도전입자로는 금속 코팅 된 폴리머 입자가 사용될 때 신뢰성이 상대적으로 좋은 것을 발견했다.

• Clean Technology
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• v.18 no.3
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• pp.295-300
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• 2012

Synthesis of well-defined particle with tunable size, shape, and functionalities is strongly emphasized for various applications such as chemistry, biology, material science, chemical engineering, medicine, and biotechnology. This study presents micromolding method for the fabrication of anisotropic particles with elegant control of curvature of covex roof. For the demostration of rapid fabrication of the particles, we have applied polydimethylsiloxane (PDMS) micromold as structure guiding template and wetting fluid to control curvature of roof of the particles. Based on this approach, we can control the radius of curvature from $20{\mu}m$ to $70{\mu}m$ with different aspect ratio of mold. In addition, wetting fluids with different wetting properties can also modulate the height and radius of curvature of the particles. We envision that this methodology is promising tool for precise control of particle shape in 3-dimensional space and new synthetic route for anisotropic particles with cost effective, simple, easy, and fast procedure.

• Membrane Journal
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• v.29 no.1
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• pp.61-65
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• 2019

Anisotropic particles have been issued in various fields due to their unique physical properties. Herein, a novel dynamic phase separation method (DPS) is introduced to fabricate anisotropic acorn-like nanoparticles. DPS consists of two dynamic conditions; solvent evaporation and nonsolvent induced precipitation. The bottom layer is controlled by feeding the water as a non-solvent diluent, and the phase separation of the upper layer relies on the diffusion and evaporation of a volatile good solvent. At this condition, the acorn-like particles were fabricated. Under a closed box filled with water (spontaneous phase separation), monodisperse polystyrene (PS) particles were synthesized. At the coexistence between DPS and spontaneous phase separation, the sizes of cap and particle were changed. Also, the volume of PS solutions influences on the particle shape. Since the unique structures could be utilized into various applications, if advanced techniques such as membrane-based controlled water feeding is developed, monodisperse acorn-like particles could be tuned.

• Clean Technology
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• v.24 no.2
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• pp.105-111
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• 2018

This study presents a novel and eco-friendly process that can precisely control the location of the patches on the patch particles. The method of manufacturing these anisotropic hexagram patch particles consists of sequential combinations of two separate methods such as a sequential micromolding technique for fabricating patch particles and a selective localization method for controlling the location of patches on the patch particles. The micromolding technique was carried out using physicochemically stable material as a micromold. In order to fabricate the highly stable patch anisotropic hexagram particles, the perfluoropolyether (PFPE) micromold was used to the process of the micromolding technique because they could prevent the problem of diffusion of hydrophobic monomers while conventional poly(dimethylsiloxane) (PDMS) micromold is limited to prevent the problem of diffusion of hydrophobic monomers. Based on combination methods of the micromolding technique and the selective localization method, the reproducibility and stability have been improved to fabricate 12 different types of anisotropic hexagram patch particles. This fabrication method shows the unique advantages in eco-friend condition, easy and fast fabrication due to less number of process, the feasibility of a mass production. We believe that these anisotropic hexagram patch particles can be widely utilized to the field of the directional self-assembly.

• Journal of the Korean Magnetics Society
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• v.13 no.1
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• pp.29-35
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• 2003

Anisotropic Sr-ferrites were prepared by the spark plasma sintering process (SPS). The Ferrite particles were oriented and densified during sintering process, and the anisotropic ferrites were manufactured at low sintering temperature and a remarkable short time processing by SPS method. It was showed that the anisotropy of ferrite particles at the specimen outer side was more higher than that at the specimen center, and it seems possible that the orientation of ferrite particles was related to DC current. Magnetic and physical properties of sintered Sr-ferrites are Br = 3.15 kG, iHc : 2.67 kOe, and density : 5.033 g/cm$^3$ when the samples were sintered for 8 minutes at 106$0^{\circ}C$.

• Journal of the Korean Geotechnical Society
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• v.22 no.11
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• pp.47-54
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• 2006

Shear wave velocity of uncemented soil can be expressed as the function of effective stresses when capillary phenomena are negligible. However, the terms of effective stresses are divided into the direction of wave propagation and polarization because stress states are generally anisotropy. The shear wave velocities are affected by ${\alpha}$ parameters and ${\beta}$ exponents that are experimentally determined. The ${\beta}$ exponents are controlled by contact effects of particulate materials (sizes, shapes, and structures of particles) and the ${\alpha}$ parameters are changed by contact behaviors among particles, material properties of particles, and type of packing (i.e., void ratio and coordination number). In this study, consolidation tests are performed by using clay, mica and sand specimens. Shear wave velocities are measured during consolidation tests to investigate the stress-induced and inherent anisotropies by using bender elements. Results show the shear wave velocity depends on the stress-induced anisotropy for round particles. Furthermore, the shear wave velocity is dependent on particle alignment under the constant evvective stress. This study suggests that the shear wave velocity and the shear modulus should be carefully estimated and used for the design and construction of geotechnical structures.

• Journal of the Korean Geotechnical Society
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• v.34 no.8
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• pp.5-14
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• 2018

The grain size of clastic sedimentary rocks classifies the rock types and also causes of anisotropy of the rock. The anisotropy is one of the most important factors that dominates the strength and weathering behavior of rocks. The anisotropy of clastic sedimentary and igneous rocks in the Gyeongsang Basin including Yeongju, Daegu, and Busan were analyzed by magnetic susceptibility expressed by the degree of anisotropy and shape parameter. As the results of the study, the sandstone deposited under lacustrine environment unaffected by the external force shows 1.03 degree of anisotropy. The degrees of anisotropy of the rocks affected by faults and fault rocks show 1.06 and 1.14, respectively. The magnetic susceptibility of rocks is to decrease with the distance from the fault. A fresh mudstone and shale formed by fines show a similar magnitude of the degree of anisotropy to fault rock and correspond to oblate shape parameter due to their sedimentary structure. Due to these reasons, we need attention in design, construction, and maintenance of a structure constructed in mudstone and shale.

• Journal of the Korean GEO-environmental Society
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• v.12 no.12
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• pp.5-12
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• 2011

Macro- and micro-behaviors of soluble granular media during dissolution process is investigated by numerical analysis. Soluble media are represented by assemblies of non-soluble particles and soluble particles with the different soluble particles contents. Dissolutions of particles are implemented by reducing sizes of soluble particles. The numerical simulations results exhibit that the vertical displacements increase to certain times and become constant while the porosities still increase until no soluble particles are present. However, the porosities and vertical displacements increase with the increase of soluble particles content. The microscopic views show that the fabrics of media change during dissolution process until the certain times, the higher soluble particles contents, and the larger change in fabric.

• Journal of the Korean Magnetics Society
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• v.4 no.1
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• pp.25-31
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• 1994

The magnetic properties of aluminum anodized film in which Co-Fe alloy electrodeposited are investigated with regard to the alloy composition of magnetic films. The electrodeposited Co-Fe particles are confirmed to be single phase Co-Fe alloys by X-ray diffractions. At 34 at% Co, the sample with small pore diameter(particle diameter $150\;{\AA}$) has a large magnetic energy product($B_{max}$) of about 1.44 MGOe due to the large saturation magnetization, the high coercive force and good squareness of the M-H curve. However, for the samples with particle diameter larger than $450\;{\AA}$, the bottom of each particle forms abnormal particle claaed branch-shaped unlike the sample of the particle diameter $150\;{\AA}$. In this case, the magnetic anisotropy energy was about zero at the compositions of 45 and 75 at% Co. Moreover, at the compositions from 50 to 70 at% Co, the anisotropy became negative value. This means that an easy axis of magnetization of the film is in plane in plane in spite of the perpendicular shape anisotropy of the particle. It was found that the bottom extremity of the particle contains FeC from the X-ray diffraction. Thus the effect of the bottom extremity, that is, an unusal magnetic property was removed by electrodepositing Cu at the bottom extremity of the particle. Itis clear that the magnetic properties of the ilms are influenced by he branch-shaped bottom extremity filled with FeC.

• Polymer Science and Technology
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• v.25 no.1
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• pp.11-14
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• 2014