• Journal of the Korea Concrete Institute
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• v.29 no.4
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• pp.407-413
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• 2017

The fundamental property of magnesia phosphate cement (MPC) for concrete repair material was investigated in this research. For mechanical properties, setting time, compressive strength and tensile/flexural bond strength were measured, and hydration products were detected by X-ray diffraction. The specimens were manufactured with dead burnt magnesia and potassium dihydrogen phosphate was admixed to activate the hydration of magnesia and a borax was used as a retarder. To observe the pore structure and ionic permeability of MPC mortar, mercury intrusion porosimetry was performed together with rapid chloride penetration test (RCPT). As a result, time to set of Fresh MPC mortar was in range of 16 to 21 min depend on the M/P ratio. Borax helped delaying setting time of MPC to 68 min. The compressive strength of MPC with M/P of 4 was sharply developed to 30 MPa within 12 hours. The compressive strength of MPC mortar was in range of 11.0 to 30.0 MPa depend on the M/P ratio at 12 hours of curing. Both tensile and flexural bond strength of MPC to old substrate (i.e. MPC; New substrate to OPC; Old substrate) were even higher than ordinary Portland cement mortar (i.e. [OPC; New substrate] to [OPC; Old substrate]) does, accounting 19 and 17 MPa, respectively. The total pore volume of MPC mortar was lower than that of OPC mortar. MPC mortar had the entrained air void rather than capillary pore. The RCPT showed that total charge passed of OPC mortar had more than that of MPC mortar, which can be explained by the pore volume and pore distribution.

• Journal of the Architectural Institute of Korea Structure & Construction
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• v.35 no.9
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• pp.143-150
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• 2019

The purpose of this study was to propose how to determine the setting time related to the determination of the surface finish working time of the concrete using a Durometer, which is used as a rubber hardness meter. Two different types of Durometer were used to measure the setting time of the concrete. High flowing concrete with 40% of water to binder ratio was fabricated maintaining $600{\pm}100mm$ of slump flow. The test results indicated that the application of the Durometer resulted in a high correlation with the penetration resistance tester in both mortar and concrete. When measuring the setting time of the concrete, with properly used with Durometer, evaluation of the setting time of the concrete can be available. Therefore, it is thought that the measurement of the final set of the durometer C type can be useful to decide the limit time of the finishing operation and the time of the rejuvenation of the curing process by measuring the finishing set at 40 HD in the case of the initial set and 10 HD in the case of D type.

• Journal of the Korea Concrete Institute
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• v.14 no.6
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• pp.973-981
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• 2002

Recently, the use of high strength concrete (HSC) has increased dramatically md however, few studies have been conducted on the early-age properties of HSC such as setting. The penetration resistance test (specified by KS F 2436) that is the standard test method for determining initial and final setting times of concrete, may not be appropriate for HSC because of the high viscosity of the mortar mixture. To address this issue, an ultrasonic pulse velocity (UPV) monitoring system was used to investigate the setting behavior of mortar and concrete. The experimental study was carried out to measure the UPV's of mortars and concretes having various water/binder ratios (W/B) and various fly ash replacement levels, during the first 24 hours of testing. Test results showed that the UPV in concrete was developed faster than that of mortar with the same W/B, and that of ordinary concrete was greater than that of fly ash concrete. Typical values of UPV were suggested that correspond to the initial and final setting times, based on following criteria: (1) the penetration resistance method; (2) the instant when the UPV begins to develop; and (3) the instant when the UPV development rate is maximum. The method and UPV monitoring device used in this study is promising for the setting assessment of concrete, particularly for HSC.

• Journal of the Korean Recycled Construction Resources Institute
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• v.11 no.3
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• pp.218-225
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• 2023

In this study, we examine the feasibility of using chlorine in clinker as an early-strength cement by the effect of accelerating the cement hydration reaction of chlorine. Clinker with a chlorine content of 200-1,000 ppm was prepared using actual cement kilns, and 46 cement samples were prepared by adding gypsum and admixtures(GGBFs and limestone). We measured consistency, setting, 1-28 days compressive strength and analyzed them statistically. Test results indicated that an increase of the chlorine content resulted in shortening of initial and final setting time and the improvement of 1 day compressive strength. But the 28 days compressive strength was decreased. Specifically, when the chlorine content was increased from 230 to 965 ppm, the 1 day compressive strength increased up to 4.6 MPa, improvement effect was superior to that of increasing Blaine in the range of 3,400-3,970 cm²/g.

• Journal of the Korean Recycled Construction Resources Institute
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• v.8 no.1
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• pp.33-38
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• 2020

The aim of the research is to evaluate the feasibility of durometer for assessing setting time of the concrete by comparing it with the currently used proctor penetration test method to improve the surface finishing timing determining method generally determined based on the experience of the worker. As a research result, the correlation between suggesting method using durometer with currently used proctor penetration test method was high enough. Hence, on the surface of the concrete, the initial setting time and the final setting time could be designated as 41 HD with C-type, and 11 HD with D-type, respectively. Therefore, the durometer can be used as a portable setting time evaluation device with the easiness of handling and measuring for determining concrete surface finishing timing quantitatively.

• Journal of the Korea Concrete Institute
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• v.14 no.3
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• pp.349-356
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• 2002

This research deals with the properties of fresh and hardened high-performance concrete(HPC) incorporating high-reactivity metakaolin(HRM). The properties of fresh and hardened state concrete were investigated included air content, slump flow, setting time, heat of hydration, compressive strength, resistance to chloride-ion penetration, abrasion and repeated freezing and thawing. The properties of the HRM concrete were also compared with those of the portland cement concrete and silica fume(SF) concrete. The laboratory test results indicate that HRM material can be used as a supplementary cementitious material to produce high-performance concrete.

• Journal of the Korean Ceramic Society
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• v.39 no.1
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• pp.57-67
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• 2002

The effect of $\beta$-TCP and PHA as additives on initial setting time, compressive strength and surface micro-structure after in vitro test of bone cement in TTCP and DCPA system was investigated. The median particle sizes of TTCP, $\beta$-TCP, DCPA and PHA for bone cement were about 3, 5, 0.9 and 4${\mu}{\textrm}{m}$, respectively. Initial setting time and compressive strength of bone cement with various composition was measured by Vicat test and Universal Testing Machine, and surface morphology and crystalline phases of bone cements were observed and analyzed by SEM and x-ray diffractometer. Initial setting time was not affected by composition but by powder/liquid ratio, and cement with PHA required double amount of solution for paste as much as one without PHA, especially. It was thought that $\beta$-TCP and PHA in bone cements was not related to setting reaction. Thus, the addition of $\beta$-TCP and PHA in bone cements decreased compressive strength and inhabited HAP from being produced on surface in vitro test. In conclusion, it was not expected that $\beta$-TCP and PHA in TTCP-DCPD bone cements enhanced the strength and bioacitivity.

• Proceedings of the Korea Concrete Institute Conference
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• 2010.05a
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• pp.387-388
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• 2010

In this study, early-age properties of mortar containing calcium chloride as an accelerator was investigated. The time of setting of the mortar by ultrasonic tester and penetrometer was assessed to prove its acceleration effect on hydration and the compressive strength was also measured to examine the effect of calcium chloride on the early-age strength.

• Journal of the Korea Concrete Institute
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• v.24 no.1
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• pp.87-95
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• 2012

This study investigated the compressive strength, flexural strength, setting time, and rebound when blast furnace slag and anhydrite, which are widely used mineral admixtures for concrete, are applied to shotcrete. When Ordinary Portland Cement (OPC) was replaced at a rate of 10% with blast furnace slag and anhydrite, the initial and final setting time requirements were all satisfied. However, when OPC was replaced at a rate of 20%, final setting was delayed, revealing that this mixture was not suitable for shotcrete. Compressive strength test results showed that the mixture with 10% OPC replacement rate met the target strength at 1 day and 28 days for permanent tunnel support usage. Particularly, the mixture designed with OPC replacement by blast furnace slag and anhydrite at rates of 5% showed the highest compressive strength. Rebound measurements revealed that this mixture exhibited excellent performance with 23% reduction in the rebound compared to the shotcrete that was produced with only OPC binder.

• Proceedings of the Korea Concrete Institute Conference
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• 2008.11a
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• pp.513-516
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• 2008

Recently, a demand for reduction of construction cost by reducing construction period is increasing because of the slump of the construction business, the increasing price of raw-materials and the enforcement of after-sale system. As a method of reducing construction period, many construction companies usually apply a method of reducing curing period. But if they use an existing early strength cement or admixture, they spend a heavy cost on materials and there are many problems, such as a heat of hydration and a loss of workability. The purpose of this research is a reduction of construction cost by reducing construction period as a earlier removal time of form. To check up application of concrete using high early strength binder and admixture, comparative tests were carried out with concrete using an existing early strength cement or admixture such as tests of diurnal variation, setting time and compressive strength.