• 제목/요약/키워드: 열화학

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Ultrasonic linear and nonlinear properties of fatigued aluminium 6061-T6 with voids (기공을 포함한 피로손상 알루미늄 6061-T6의 초음파 특성평가)

  • Kang, To;Song, Sung-Jin;Na, Jeong K.;Park, Jin-Ho
    • Journal of the Korean Institute of Gas
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    • v.19 no.5
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    • pp.41-46
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    • 2015
  • It is known that in aluminum 6061-T6, which is composed of $Mg_2Si$ and ${\beta}-Al_5FeSi$, void nucleation grows around ${\beta}-Al_5FeSi$ of Al606-T6. In this work, growth of voids was checked by scanning a 6061-T6 specimen with SEM observation. The effects of dislocation damping, coherency strain and voids on ultrasonic attenuation and nonlinearity parameters were experimentally measured. It was observed that a nonlinearity parameter increases until 75 percent of fatigue life and decreases after that. From the results, the authors inferred that dislocation damping and coherency damping increase nonlinearity parameters and void nucleation decreases them as ultrasonic scattering increases with void. The application of nonlinearity parameters in estimating degradation of materials with complex microstructures through fatigue process, therefore, should be carefully considered.

Sensitive Characteristics of Hot Carriers by Bias Stress in Hydrogenated n-chnnel Poly-silicon TFT (수소 처리시킨 N-채널 다결정 실리콘 TFT에서 스트레스인가에 의한 핫캐리어의 감지 특성)

  • Lee, Jong-Kuk;Lee, Yong-Jae
    • Journal of Sensor Science and Technology
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    • v.12 no.5
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    • pp.218-224
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    • 2003
  • The devices of n-channel poly silicon thin film transistors(TFTs) hydrogenated by plasma, $H_2$ and $H_2$/plasma processes are fabricated. The carriers sensitivity characteristics are analyzed with voltage bias stress at the gate oxide. The parametric sensitivity characteristics caused by electrical stress conditions in hydrogenated devices are investigated by measuring the drain current, threshold voltage($V_{th}$), subthreshold slope(S) and maximum transconductance($G_m$) values. As a analyzed results, the degradation characteristics in hydrogenated n-channel polysilicon thin film transistors are mainly caused by the enhancement of dangling bonds at the poly-Si/$SiO_2$ interface and the poly-Si grain boundary due to dissolution of Si-H bonds. The generation of traps in gate oxide are mainly dued to hot electrons injection into the gate oxide from the channel region.

Combustion Characteristics Analysis of a Non-class 1E Cable for Nuclear Power Plants according to Aging Period (경년열화 기간에 따른 원자력발전소용 비안전등급 케이블의 연소특성 분석)

  • Kim, Min Ho;Lee, Seok Hui;Lee, Min Chul;Lee, Sang Kyu;Lee, Ju Eun
    • Journal of the Korean Society of Safety
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    • v.35 no.5
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    • pp.22-29
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    • 2020
  • In this study, combustion and smoke release characteristics of a non-class 1E cable for nuclear power plants were investigated according to aging period. The aging was reproduced through an accelerated aging method for interval of 10 years :10, 20, 30 and 40 year, which was applied the Arrhenius equation. The cable was subjected to accelerated aging. In order to understand combustion and smoke release characteristics, the cone calorimeter test was performed according to the standard code of KS F ISO 5660-1. Heat release rate, mass loss rate, average rate of heat emission and smoke production rate were examined through cone calorimeter test. Fire performance index, fire growth index and smoke factor were derived from test results for the comparison of quantitative fire risk. When comparing the fire performance index and the fire growth index, the early fire risk tends to decrease as aging progresses, which might be attributed from the fact that the volatile substances of cables were evaporated. However, when comparing the heat release rate, average rate of heat emission and mass loss rate, which represent the mid and late periods of the fire risk, the values of accelerated aging cables were much higher than those of non-aged cable, which signifies the unstable formation of the char layer resulted in the change in the performance of flame retardants. In addition, the results from the smoke characteristics show that the accelerated aging cables were lager than the non-aged cables in terms of overall fire risk. These results can be used as baseline data when assessing fire risk of cables and establishing fire safety code for nuclear power plants.

Development of Automatic Crack Detection System for Concrete Structure Using Image Processing Method (이미지 분석기법을 이용한 콘크리트 구조물의 균열 검출 시스템 개발)

  • Lee, Ho Beom;Kim, Jong Woo;Jang, Il Young
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.1
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    • pp.64-77
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    • 2012
  • In this study, the crack detecting system with digital image processing techniques based on the mathematical morphology method was developed to detect cracks in concrete structures. In the developed system, the image combining technique of reconstructing multiple images as an entire single image considering efficient management of analysis results was applied as an additional module. The developed system was verified through a field test with the cracked concrete culvert and the crack width of 0.2 mm was able to be detected in the 40m span. In the image analysis, the difference between calculated crack width and actual crack width were less than 0.08mm. For image combination in the stitching test of pattern images, the stitched image was identical with the original picture of entire subject in the visual perception level.

Simulation of Heat and Smoke Behavior for Wood and Subway Fires by Fire Dynamics Simulator(FDS) (FDS에 의한 목재 및 지하철 화재의 열 및 연기 거동 시뮬레이션)

  • Sonh, Yun-Suk;Dan, Seung-Kyu;Lee, Bong-Woo;Kwon, Seong-Pil;Shin, Dong-Il;Kim, Tae-Ok
    • Journal of the Korean Institute of Gas
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    • v.14 no.6
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    • pp.31-37
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    • 2010
  • In this study, to propose the analysis method of heat and smoke behavior of fire using the CFD-based fire simulator FDS, comparison of the simulation results against the experimental results and the sensitivity of the results to the grid sizes have been investigated. For the wood fire, thermal images captured from the experiments were compared against the FDS simulations, and the maximum temperatures agreed in~4.3 % error, showing the applicability of FDS in the interpretation of the fire phenomena. In the aspect of the sensitivity to the grid size for the subway fire, FDS results of smoke temperature, CO concentration and visibility converged and showed no distinct changes for the grid size < $28(L){\times}28(W){\times}14(H)$, guaranteeing that the FDS fire model set in this research could interpret the fire phenomena successfully.

Assessment of Yield Characteristics of Gas Pipeline Materials by Observing Surface-Local Deformation (미소 표면변형 관찰을 통한 가스배관 부재의 항복특성 평가)

  • Lee, Yun-Hee;Baek, Un-Bong;Cheong, In-Hyeon;Nahm, Seung-Hoon;Lee, Sang-Houck
    • Journal of the Korean Institute of Gas
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    • v.12 no.2
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    • pp.92-98
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    • 2008
  • A combination of the instrumented indentation and 3D morphology measurement has been tried in order to perform a real-time property measurement of degraded materials in gas pipelines; three-dimensional indent morphologies were recorded using a reflective laser scanner after a series of insturmented indentations on three metallic specimens. Dimensions of the permanent deformation zone and contact boundary were analyzed from the cross-sectional profile over an remnant indent and used for estimating yield strength and hardness, respectively. Estimated yield strength was comparable with that from uniaxial tensile test and actual hardness implying material pile-up effects was lower than the calculated value from indentation curve by $20{\sim}30%$. It means that this 3D image analysis can explain the material pile-up effects on the contact properties. Additionally, a combined system of indentation and laser sensor was newly designed by modifying a shape of the indentation loading fixture.

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The Development of Life Evaluation Program for LNG Storage Tank considering Fatigue and Durability (피로 및 내구성을 고려한 LNG 저장탱크의 수명평가 프로그램 개발)

  • Kim, Jung-Hoon;Kim, Young-Gu;Jo, Young-Do
    • Journal of the Korean Institute of Gas
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    • v.21 no.3
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    • pp.39-45
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    • 2017
  • The LNG storage tank as core facility of LNG industry is mainly composed of the inner tank of nikel 9% steel and the outer tank of prestressed concrete. To respond proactively increased risk of structure performance deterioration due to fatigue of the inner tank and durability reduction of the outer tank, life evaluation program for LNG storage tank is needed. In this study, life evaluation program for LNG storage tank was developed to assess fatigue of the inner tank and durability(carbonation and chloride attack) of the outer tank. By defining the main three scenarios in the inner tank, the fatigue life analysis is conducted from structural analysis and Miner's damage rule. Carbonation progress of the outer tank is predicted according to thickness of cover concrete by using carbon dioxide contents and data of penetration depth. To consider a variety of input conditions and a reliability in results of chloride attack, the evaluation of choride attack for the outer tank is constructed through Life-365 program of open source.

The Development of Compressive Strength Estimation Equation for LNG Storage Tank using Rebound Hardness Method (반발경도법을 이용한 LNG 저장탱크 콘크리트의 압축강도 추정식 개발)

  • Kim, Jung-Hoon;Kim, Young-Gu;Jo, Young-Do
    • Journal of the Korean Institute of Gas
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    • v.21 no.3
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    • pp.26-32
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    • 2017
  • Outer tank concretes of LNG storage tank are composed of prestressed concrete structures that act as a protective wall. The danger such as the collapse of structures will exist if concrete structures is not secured due to the deterioration. Concrete compressive strength directly related to the safety of structures can be predicted by using estimation equation of compressive strength through rebound hardness test and ultrasonic wave velocity method. But, there is no the estimation equation of LNG storage tank for a relation between NDT data and real strength. In this study, to obtain more accurate real strengths for LNG storage tank, core specimens were sampled from walls of pilot LNG storage tank. The rebound hardness test of general NDT for concrete structures was carried out at each 3 positions for the four areas. The compressive strength estimation equation of LNG storage tank was developed by using the data for rebound hardness test of pilot LNG storage tank and compressive strength test of sampled concrete cores.

Development of Dynamic Interface for Improvement of Diagnostic Algorithms in "G15 Condition Monitoring and Diagnosis System" (GIS 예방진단시스템의 진단알고리즘 향상을 위한 다이나믹 인터페이스 개발)

  • Min, Byoung-Woon;Lee, Byoung-Ho;Choi, Hang-Sub;Cho, Chul-Hee;Cho, Pil-Sung;Lee, Dong-Chul
    • Proceedings of the KIEE Conference
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    • 2006.07e
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    • pp.57-58
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    • 2006
  • 과거 2003년 북미 대 정전 이후 전력기기의 사고 발생 후 얼마나 빨리 사고를 제거하고 피해가 적도록 신속하게 복구하는 개념에서 사고이전에 사고를 미연에 방지하는 예방개념으로 관심이 높아지고 있다. 전력기기를 사고로부터 보호하는 보호기기도 중요하지만 사고이전의 상태를 감시하여 미연에 사고를 방지할 수 있도록 하는 예방진단시스템의 중요성도 높아지고 있다. 이렇듯 관심이 높아짐에 따라 각종 진단알고리즘의 개발이 신속히 이루어지고 있다. 보호기기처럼 어떤 설정된 정정 값 이상의 값이 입력되면 보호동작을 수행하는 단순 동작과는 달리 예방진단 시스템은 입력되는 신호의 패턴을 인식하여 열화/노화 등의 진행상황 및 정비조치에 대한 정보를 만들므로 인공지능적인 요소가 많이 적용되고 있다. 따라서 각종 Fuzzy, Neural Network, Expert 등 각종 판단 알고리즘과 패턴을 인식하는 확률통계, 프랙탈 기하학 등이 적용되고 있다. 모두가 틀리다는 것은 아니지만 보다 정확한 예방진단을 위해 각종 알고리즘이 추가 및 수정이 자주이루어지고 있는 실정이다. 그러나 새로운 알고리즘을 적용하기 위해서 기 개발되어 운영 중이거나 설치된 예방진단시스템을 멈추고 전반적으로 수정을 수행하는 것은 감시진단시스템의 본래 모습을 무시하는 행동이라고 할 수 있다. 본 연구에서는 이런 문제를 해결하기 위하여 온라인 상태에서 장비를 감시하는 예방진단 시스템의 알고리즘 변형 시 시스템의 운영이 문제되지 않도록하는 다이나믹 인터페이스를 개발하였다.

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단일벽 탄소나노튜브의 직경과 촉매 나노입자 크기의 상호 연관성

  • Kim, Jin-Ju;Jeong, Gu-Hwan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.75-75
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    • 2010
  • 단일벽 탄소나노튜브(SWNT)는 뛰어난 물리적 성질과 화학적 안정성을 가지고 있어서 다양한 분야의 응용이 기대되어 폭넓은 연구가 진행 되고 있다. 특히 SWNT의 전기적 및 기계적 특성들은 SWNT의 직경 및 뒤틀림도(chirality)에 의해 크게 좌우되기 때문에, 합성하는 단계에서 직경 또는 chirality를 제어에 관한 많은 이론적 연구가 진행되어 왔으며, 최근에는 초기 SWNT의 핵생성 단계에서의 촉매의 거동 및 상호 연관성 등에 관한 실험적인 연구결과들이 속속 보고되고 있는 실정이다. 하지만, 아직도 이에 관한 더욱 다양하고 활발한 연구 접근 및 결과들이 필요한 시점이다. 상기 배경을 바탕으로 본 연구에서는 균일한 직경을 갖는 SWNT의 합성을 위한 기초연구로서 SWNT의 직경과 촉매나노입자의 크기의 상호 연관성에 대해 체계적으로 조사하였다. 우선 SWNT합성을 위한 촉매나노입자를 얻기 위해 페리틴(ferritin)용액의 농도 및 스핀코팅 조건을 변화시킴으로써 기판 위에 분산농도를 제어한 후, 대기 열처리를 통하여 촉매나노입자의 농도를 제어하였다. 나노입자의 평균직경은 4 nm 정도로 비교적 균일하였으며, 고농도의 촉매입자는 SWNT의 다발화(bundling)를 유발하였다. 따라서, SWNT와 나노입자 직경의 상호연관성을 조사하기 위해서는 단분산(monodispersed) 된 나노입자를 이용하였으며, 아르곤 분위기에서 추가적으로 고온($900^{\circ}C$) 열처리를 실시함으로써 나노입자의 크기감소를 도모하였다. 실험결과, 열처리 시간의 증가에 따라 입자크기가 감소함을 확인하였으며, 이는 나노입자의 증발에 의한 것으로 예상된다. 다음으로는 열처리를 통하여 직경이 제어된 나노입자를 이용하여 SWNT를 합성한 후 SWNT와 촉매크기 사이의 크기 관계를 조사하였다. SWNT의 합성은 메탄을 원료가스로 열화학증기증착법을 이용하였고, 합성기판으로는 산화실리콘웨이퍼와 퀄츠기판을 이용하였다. 성장한 SWNT의 직경은 AFM을 이용하여 측정하였으며, 퀄츠기판에 수평배향 성장시킨 SWNT를 3차원 구조의 기판으로 전사(transfer)하여, 라만분석이 용이하도록 하였다.

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