• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2003.04a
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• pp.35-35
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• 2003

)를 금속와이어에 인가하면 저항발열에 의해 와이어가 미세한 입자나 금속증기상태로 폭발하는 현상을 이용한 것으로 기상합성법에 속한다고 할 수 있다. 선폭법은 다른 제조법에 비해 공정이 간단하여 생산비용이 저렴하며, 원재료의 조성을 갖는 분말의 합성과 금속간화합물, 융점차이가 나는 재료의 합금화 등이 가능하다. 인가에너지의 크기와 폭발 시 분위기를 제어함으로써 분말의 평균크기와 분포 제어 또한 가능하다. 본 연구는 러시아의 우수한 기초기술을 바탕으로 Pb-Sn계 합금은 전기폭발법으로 극미세분말을 제조하였으며, 분말의 형상, 상 화학조성의 변화를 조사하였다. 본 실험에 사용된 Sn-Pb계(All-Union State Standard 1499-70, 0.53mm)합금와이어는 자동시스템(1-0.6Hz)에 의해 챔버안으로 공급되었다. 이 때 임계폭발 와이어 길이는 50-80nm으로 실험을 행하였다. 챔버 압력은 1.4~2.0atm으로 유지하였다. 제조된 분말의 특성은 XRD, XRPES, SEM등을 이용하여 분말의 형상과 상, 화학조성, 표면분석을 행하였으며 DSC, TGA, BET분석을 통하여 온도변화에 따른 금속분말의 열량변화, 질량변화, 비표면적을 측정하였다. 제조된 Sn-Pb계 분말은 모두 평균 입도 117nm~220nm의 구형형상이었다. 이때 합금분말의 조성은 51.17~63.21 at%Sn, 35.47~46.37 at%Pb로 나타났다. 와이어에 인가되는 비에너지(W/Wc)가 감소된에 EK라 표면층의 Pb함량이 증가함을 보였다. 이는 와이어 내부 저항의 감소로 인한 공정시간의 지연과 Sn, Pb의 확산계수 차이에 의한 것으로 사료된다. 열분석 결과, Sn~Pb계 화합물의 융점은 167~$169^{\circ}C$로 관찰되었으며, $10^{\circ}C$/min로 $920^{\circ}C$까지 승은 하였을 때 17.1~18 wt%의 질량증가를 보였다.TEX>계 나노복합분말이 얻어짐을 알 수 있었다. 이 때 X션 회절피크의 line broadening으로부터 복합분말의 Fe 명균 결정립 크기는 24nm로 초미세 결정럽의 분말합금이었다. 포화자화값은 볼밀처리에 따라 점점 증가하여 MA 30시간에는 20.3emu/g로 포화됨을 알 수 있었다. 또한 보자력 Hc는 MA초기단계에 350e로 매우 낮으나 30시간 후에는 Hc값이 2600e로 매우 큰 값을 나타내었다. 이것은 환원반응결과 초기에 생성된 Fe의 결정립이 비교적 크고 결정결함이 적으나 볼밀처리를 30시간까지 행하면 Fe 결정렵의 미세화 빛 strain 증가로 magnetic hardening이 일어나기 때문인 것으로 사료된다.길이가 50, 30cm인 압출재를 제조하였다. 열간압출한 후의 미세조직을 광학현미경으로 압출방향에 평행한 방향과 수직방향으로 관찰하였고, 열간 압출재 이방성을 검토하기 위하여 X선 회절분석을 실실하여 결정방위를 확인하였다. 전기 비저항 및 Seebeck 계수 측정을 위하여 각각 2$\times$2$\times$10$mm^3$ 그리고 5$\times$5$\times$10TEX>$mm^3$ 크기의 시편을 준비하였다.준비하였다.전류를 구성하는 주요 입자의 에너지 영역(75~l13keV)에서 가장 높은(0.80) 상관계수를 기록했다. 넷째, 회복기 중에 일어나는 입자들의 유입은 자기폭풍의 지속시간을 연장시키는 경향을 보이며 큰 자기폭풍일수록 현저했다. 주상에서 관측된 이러한 특성은 서브스톰 확장기 활동이 자기폭풍의 발달과 밀접한 관계가 있음을 시사한다.se that were all low in two aspects, named "the Nonsignificant group". And the issues were high risk perception in general setting and lo

• The Journal of Engineering Geology
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• v.13 no.4
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• pp.457-474
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• 2003

This study aims to elucidate characteristics of groundwater level fluctuation at riverbank filtration sites in Daesan-myeon, Changwon City. Groundwater level fluctuation, river water level change and stream-aquifer interaction are very important to estimate optimal discharge rate of the pumping well. Water level contours from February 2003 to October 2003 show normal decreasing trend toward the Nakdong river with the hydraulic gradient of 0.008. However, flow reversion occurs when groundwater is discharged at the pumping wells or rise of the Nakdong river by rainfall. The fluctuation of the Nakdong river ranges 0 - 10 m msl. Autocorrelation analysis was conducted to the groundwater levels measured on the six monitoring wells (DS1, DS2, DS3, DS4, DS6 and DS7). The analyzed waterlevel data can be grouped into three: group 1 (DS1 and DS3) represents strong linearity and long memory effect, group 2 (DS1 and DS6) intermediate linearity and memory, and group 3 (DS4 and DS7) weak linearity and memory. Waterlevels of group 1 wells are relatively closely related to the change of river-water level. Those of group 2 wells are largely affected by the pumping and the river-water level, and those of group 3 wells are strongly linked to pumping.

• Journal of the Korean Society for Marine Environment & Energy
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• v.19 no.1
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• pp.62-73
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• 2016

The variation of groundwater by wave, tide and precipitation conditions is closely related to the vegetation environment at the natural vegetation and sandy based beach, and it has a significant impact on the vegetation development and ground stabilization. In this study, the water temperature, electrical conductivity, and pressure were monitored at five observational stations normal to the Jinu-do(Island) shoreline of Nakdong river estuary from March 2012 to September 2014 (approximately 799 days) with the aim of measuring the variation in groundwater-table characteristics. The purpose of the study was to identify factors (tide, wave etc.) affecting groundwater-table variation using time series and correlation analysis, and to record spatial variations in the groundwater level and electrical conductivity as a result of storm events. The observational station in the intertidal zone was strongly affected by wave period and tide level. During the storm period, the groundwater-table and electrical conductivity were stabilized at the edge of sand dunes, vegetation, and areas of transition between freshwater and seawater.

• Journal of the Korean Applied Science and Technology
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• v.33 no.2
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• pp.385-390
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• 2016

In our study, ceramics coatings by additives of nano alumina and magnesia have cured on 304 stainless steel at $170^{\circ}C$ 2h. We designed and experimented the coated specimens that were characterized by laser induced fluorescence spectroscopy using the charge coupled device and scanning electronic microscopy(SEM). The result was revealed the ceramic coatings added fillers has more excellent on adhesive property and scratch resistance, and less weight loss in acid solution than ceramic coatings non-added fillers. Therefore, this study has designed and manufactured the electromagnetic spectrometry with CCD and then analyzed the coatings on 304 stainless steel using the High Resolution Charge Coupled Device in improving the corrosion resistance of 304 stainless steel. Nowadays, coatings of stainless steel have increased by industrial demand in hygienes, aviation, instrumentations and robotics as the industry special application develops.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.21 no.6
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• pp.246-252
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• 2011

The semiconducting $MnSi_{1.73}$ compound has been recognized as a thermoelectric material with excellent oxidation resistance and stable characteristics at elevated temperature. In the present work, we applied mechanical alloying (MA) technique to produce $MnSi_{1.73}$ compound using a mixture of elemental manganese and silicon powders. The mechanical alloying was carried out using a Fritsch P-5 planetary mill under Ar gas atmosphere. The MA powders were characterized by the X-ray diffraction with Cu-$K{\alpha}$ radiation, thermal analysis and scanning electron microscopy. Due to the observed larger loss of Si relative to Mn during mechanical alloying of $MnSi_{1.73}$, the starting composition of a mixture Mn-Si was modified to $MnSi_{1.83}$ and then $MnSi_{1.88}$. The single $MnSi_{1.73}$ phase has been obtained by mechanical alloying of $MnSi_{1.88}$ mixture powders for 200 hours. It is also found that the grain size of $MnSi_{1.73}$ compound powders analyzed by Hall plot method is reduced to 40 nm after 200 hours of milling.

• Journal of the Korean Vacuum Society
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• v.6 no.4
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• pp.298-307
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• 1997

TDS(Thermal Desorption Spectroscopy)system, for diagnosis of CRT manufacturing process, was designed and constructed. Outgassings and thermal desorptions from the part or materials of CRT can be measured and analysed with this system at various temperatures. The system is consisted of 3 parts, vacuum chamber and pumping system with variable conductance, sample heating stages & their controller, and outgassing measurement devices, like as ion gauge or quadrupole mass spectrometer. The ultimate pressure of the system was under $1{\times}10^{-7}$ Pa. With the variable conductance system, the effective pumping speed of the chamber could be controlled from sub l/s to 100 l/s. The effective pumping speed values were determined by dynamic flow measurement principle. The temperatures and ramp rate of sample were controlled by tungsten heater and PID controller up to 600℃ within ±1℃ difference to setting value. Ion gauge & QMS were calibrated for quantitative measurements. Some examples of TDS measurement data and application on the CRT process analysis were shown.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.33 no.4
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• pp.1707-1718
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• 2013

Historical cost data estimating system has been introduced since 2004 in the construction industry. Based on contract prices of past projects, this estimating system estimates construction cost according to work types. The Korea Institute of Construction Technology (KICT) announces the historical cost data twice a year annually. The unit price of a small construction project is higher than large construction project due to the increase on production cost per work unit, equipment and labor cost, etc. However, the historical cost data estimating system is applied to project estimation uniformly regardless the construction project's size. This study compared and analyzed the historical cost data of large and small construction project to indicate the problem of historical cost date estimating system. The study derived that the unit price of a small construction project is 21.8% higher than that of large construction project.

• Fire Science and Engineering
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• v.26 no.2
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• pp.105-111
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• 2012

In this research, aluminum composite panels of the general materials and fire retardant materials as building claddings make researches about fire performance comparison analysis. Test methods of the small and medium cone calorimeter experiments and SBI (Single Burning Item) experiments was applied to the determination. As a result, in the experiments peak heat release rate cone calorimeter the general aluminum composite panel $1,293kW/m^2$ ($75kW/m^2$), flame-retardant aluminum composite panel $70kW/m^2$ ($75kW/m^2$) was measured. In the SBI experiments fire growth rate the general fire aluminum composite panel is approximately 743 W/s and the flame-retardant aluminum composite panel is approximately 97 W/s of the value were measured. Thus, a standards enactment are urgently required in this case it is used as building claddings of the aluminum composite panel by fire risk assessment.

• Journal of the Korean GEO-environmental Society
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• v.10 no.7
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• pp.93-101
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• 2009

Standing column well (SCW) heat pump system produces geothermal energy by the heat exchange of the groundwater. If SCW system changed the temperature of soil and groundwater, it could also change species or population of microorganisms. Therefore it is needed to research about the effect of temperature change on microorganisms to use eco-friendly geothermal energy. We produced the simulative heat pump system (SHPS) and observed the change of the soil temperature in SHPS. Characteristic analysis of microorganisms isolated from soil was performed and groundwater temperature variation was evaluated. Also the bleeding effect in SHPS was investigated and the results are included. As the results, the population of microorganisms was increased about 90%, as the groundwater temperature increased 2-3 celsius degree. However the species of microorganism was little influenced by the temperature change of the soil.

• Polymer(Korea)
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• v.29 no.4
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• pp.392-398
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• 2005

Self-assembled multilayer thin films of poly(ethylene-alt-maleic anhydride) (PEMAh) and poly(4-vinyl pyridine) (P4VP) were fabricated by layer-by-layer (LbL) sequential adsorption. Fourier transform infrared (FT-IR) spectroscopic analysis of the self-assembled PEMAh/P4VP multilayer films confirms that the driving forces for the multilayer buildup are the intermolecular hydrogen bonding and electrostatic interactions. The linear increase of absorption peak of P4VP at 256 nm with increasing number of PEMAh/P4VP bilayers indicates that the multilayer buildup is an uniform assembling process. We also investigate the effects of polyelectrolyte concenhation variation of the dipping solution and pH variation of the PEMAh solution on the multilayer film formation. Thickness. adsorbed polyelectrolyte mass and surface roughness of the multilayer films were measured by UV-visible spectroscopy, quartz crystal microbalance (QCM), and atomic force microscopy (AFM), respectively.