• Title/Summary/Keyword: 연신특성

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Investigation on Resistance to Hydrogen Embrittlement of High Nitrogen Austenitic Steels for Hydrogen Pipe by the Disc Pressure Test and the Tensile Test on Hydrogen Pre-charged Specimens (디스크 시험 및 수소처리 인장시험에 의한 수소배관용 고질소 스테인리스강의 내수소취성 평가 연구)

  • Dong-won, Shin;Min-kyung, Lee;Jeong Hwan, Kim;Ho-seong, Seo;Jae-hun, Lee
    • Journal of the Korean Institute of Gas
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    • v.26 no.6
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    • pp.16-23
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    • 2022
  • In this study, characteristics of effect on hydrogen gas was investigated to hydrogen embrittlement by disk and tensile tests. The developed and commercial alloy was fabricated to a plate material made from an alloy ingot. The prepared materials were processed in the form of a disk to measure rupture pressure by hydrogen and helium gas at a rate of 0.1 to 1,000 bar/min. In the hydrogen pre-charged tensile test, a specimen was hydrogenated using an anode charging method, and the yield strength, ultimate tensile strength, elongation, and reduction in area rate were carried by a strain rate test. Also, the microstructure was observed to the fracture surface of the tensile test specimen. As a result, the developed materials satisfied endurable hydrogen embrittlement, and the fractured surface showed a brittleness fracture surface with a depth of several ㎛, but dimple due to ductile fracture could be observed.

Properties of Smart Vapor Self-Releasing Composite Films to Microwave Packaging (증기 자가방출 스마트 전자레인지 포장재 적용을 위한 복합필름 특성연구)

  • Wooseok, Song;Hojun, Shin;Jongchul, Seo
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.28 no.3
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    • pp.157-163
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    • 2022
  • The demands for Home Meal Replacement (HMR) products are continuously increasing owing to the convenience of instant food and online food delivery. Ready-to-heat (RTH) products have received massive attention in the HMR industry because these products can be easily warmed using a microwave oven. However, the conventional microwave packaging should be opened before microwave heating to prevent bursting or food loss owing to the steam-pressure build-up inside the package. Open packaging might lead to non-uniform food heating and cross-contamination. Therefore, packaging materials that are able to release steam without opening are of interest to the HMR industry. In this study, polylactic acid(PLA)/polyethylene glycol(PEG)/nanoclay composite films were manufactured using an extrusion method as packaging materials with a smart steam-releasing function. The introduction of PEG to the PLA imparted a steam self-releasing feature to the composite films owing to the morphology change of composite films during microwave heating. Further, PEG increased the ductility of PLA, which in turn prevented bursting caused due to the steam-pressure build-up. The uniform dispersion of nanoclay obtained by a twin-screw extrusion led to stronger mechanical properties. Therefore, the smart composite films developed here can be applied as microwave packaging materials with a self-releasing function.

Study on the optimization of additive manufacturing process parameters to fabricate high density STS316L alloy and its tensile properties (고밀도 STS316L 합금 적층 성형체의 제조공정 최적화 및 인장 특성 연구)

  • Yeonghwan Song
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.33 no.6
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    • pp.288-293
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    • 2023
  • To optimize the process parameters of laser powder bed fusion process to fabricate the high density STS316L alloy, the effect of laser power, scanning speed and hatching distance on the relative density was studied. Tensile properties of additively manufactured STS316L alloy using optimized parameters was also evaluated according to the build direction. As a result of additive manufacturing process under the energy density of 55.6 J/mm3, 83.3 J/mm3 and 111.1 J/mm3, high density STS316L specimens was suitably fabricated when the energy density, power and scan speed were 83.3 J/mm3, 225 W and 1000 mm/s, respectively. The yield strength, ultimate tensile strength, and elongation of STS316L specimens in direction perpendicular to the build direction, show the most competitive values. Anisotropic shape of the pores and the lack of fusion defects probably caused strain localization which result in deterioration of tensile properties.

Mechanical Properties of Joints according to Welding Methods and Sensitivity Analysis of FSW's Welding Variables for A6005 Extruded Alloy of Rolling Stock (철도차량용 A6005 압출재의 용접방법에 따른 접합부 기계적 특성 및FSW 용접 변수의 민감도 분석)

  • Kim, Weon-Kyong;Won, Si-Tae;Goo, Byeong-Choon
    • Journal of the Korean Society for Railway
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    • v.13 no.2
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    • pp.131-138
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    • 2010
  • Recently, extruded aluminium-alloy panels have been used in the car bodies in order to meet the needs for the speed-up and light-weight of the railway vehicles. Most of the car bodies were jointed by arc weldings, like GMAW (GasMetal Arc Welding) and GTAW (Gas Tungsten Arc Welding), but these weldings became fairly worse the mechanical properties of the junction than the base metal. Nowadays, FSW (Friction Stir Welding), which is superior to the arc weldings, has been applied in the railway vehicles. In this study, the mechanical properties of the joints in both FSW and GMAW for A6005 extruded aluminium-alloy sheets have discussed. In addition, the relationships between the welding conditions and the mechanical properties for the joint of FSW have analyzed through the sensitivity analysis. It can be concluded that the mechanical properties for the joint of FSW are better than those of GMAW and the welding speed is the most sensible welding condition in the process of FSW.

A Statistical Analysis on the Mechanical Properties of Structural Welding Steels (용접구조용강재의 기계적 성질에 관한 통계적 분석)

  • Chang, Dong-Il;Kyung, Kab-Soo;Hong, Sung-Wook;Nam, Wang-Hyone
    • Journal of Korean Society of Steel Construction
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    • v.12 no.3 s.46
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    • pp.281-290
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    • 2000
  • In this study, we have quantitatively estimated the mechanical properties of structural welding steels widely used in steel structures after correcting the millsheets of the steels using statistical technique. From this result, in present, the mechanical properties of the steels produced in domestics have satisfied the prescribed values in Korean Standards. The mechanical properties of the steels were dependent upon the plate thickness & class of the steels. Also, there have been linear relations between the plate thickness & class of the steels and the mechanical properties of the steels. And the results of this study have shown the similar tendencies with the existing results. Because the upper limit value of yield strength is not prescribed at Korean Standards in present, it is necessary to prescribe the upper limit value of yielding ratio(or yield strength) in order to assure the deformation performance of the steels.

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Study on the Improving Penetration Performance of Tungsten Heavy Alloy Penetrator by Heat Treatment (열처리 공정을 통한 텅스텐 중합금 관통자의 관통능력 향상에 관한 연구)

  • Kim, Myunghyun;Noh, Jooyoung;Lee, Youngwoo;An, Daehee
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.2
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    • pp.322-327
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    • 2020
  • An Armor Piercing Fin Stabilized Discarding Sabot (APFSDS), which penetrates and sabotages the target by physical energy, consists of a general penetrator using Depleted Uranium (DU) or Tungsten Heavy Alloy (THA) but THA is preferable because of manufacturing and environmental issues. On a THA penetrator, the penetration performance is determined mainly by self-sharpening depending on the hardness and toughness of materials. In particular, the tensile strength and impact strength work as key factors. The correlation coefficient for the penetration performance of the tensile strength was 0.721 and the impact strength was -0.599. The improved penetration performance by additional heat treatment was proven experimentally. Therefore, maintaining elongation over 9 % and tensile strength over 123 kg/㎟ is desirable, and the impact strength should be less than 6.8 kg·m/㎠ for good penetration performance.

Electrochemical and Mechanical Characteristics of Covalently Cross-Linked SPEEK Polymer Electrolyte Membrane for Water Electrolysis (수전해용 공유가교 SPEEK 고분자 전해질 막의 전기 화학적 및 기계적 특성)

  • Kim, Kyung-Eon;Jang, In-Young;Kweon, Oh-Hwan;Hwang, Yong-Koo;Moon, Sang-Bong;Kang, An-Soo
    • Transactions of the Korean hydrogen and new energy society
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    • v.18 no.4
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    • pp.391-398
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    • 2007
  • The covalently cross-linked sulfonated polyetheretherketone (CL-SPEEK) membrane was prepared by four-step synthesis of sulfonation-sulfochlorination, partial reduction, lithiation, and cross-linking, and its electrochemical and mechanical properties were investigated for water electrolysis application. The prepared ion exchange membranes showed good electrochemical and mechanical properties; proton conductivity of 0.116 S/cm at $80^{\circ}C$, water uptake of 44.6%, ion exchange capacity of 1.75 meq/g-dry-memb., tensile strength of 64.25 MPa and elongation of 61.11%. The membrane electrode assembly (MEA) with homemade membranes were prepared by non-equilibrium impregnation-reduction (I-R) method. Especially, the electrochemical surface area (ESA) and roughness factor of CL-SPEEK electrolyte by cyclic voltammetry method were 23.46 $m^2/g$ and 307.3 $cm^2-Pt/cm^2$, respectively. The prepared MEA was used in the unit cell of water electrolysis and the cell voltage was 1.81 V at 1 A/$cm^2$ and $80^{\circ}C$, with platinum loadings of 1.31 mg/$cm^2$.

The Preparation and Physicochemical Characteristics of Covalently Cross-Linked SPEEK/HPA Composite Membranes for Water Electrolysis (수전해용 공유가교 SPEEK/HPA 복합막의 제조 및 물리화학적 특성)

  • Hwang, Yong-Koo;Lee, Kwang-Mun;Woo, Je-Young;Chung, Jang-Hoon;Moon, Sang-Bong;Kang, An-Soo
    • Transactions of the Korean hydrogen and new energy society
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    • v.20 no.2
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    • pp.95-103
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    • 2009
  • In order to improve the electrochemical, mechanical and electrocatalytic characteristics, engineering plastic of polyether ether ketone (PEEK) as polymer matrix was sulfonated (SPEEK) and the organic-inorganic blend composite membranes has been prepared by loading heteropoly acids (HPAs), including tungstophosphoric acid (TPA), molybdophosphoric acid (MoPA), and tungstosilicic acid (TSiA). And then these were covalently cross-linked (CL-SPEEK/HPA) as the electrolyte and MEA of polymer electrolyte membrane electrolysis (PEME). As a result, the optimum reaction conditions of CL-SPEEK/HPA was established and the electrochemical characteristics such as ion conductivity ($\sigma$) were in the order of magnitude: CL-SPEEK /TPA30 (${\sigma}=0.128\;S/cm^{-1}$) < /MoPA40 (${\sigma}=0.14\;S/cm^{-1})$ < /TSiA30 (${\sigma}=0.22\;S/cm^{-1}$) at $80^{\circ}C$, and mechanical characteristics such as tensile strength: CL-SPEEK /TSiA30 $\fallingdotseq$ /MoPA40 < /TPA30. Consequently, in regards of above characterisitics and oxidation durability, the CL-SPEEK/TPA30 exhibited a better performance in PEME than the others, but CL-SPEEK/MoPA40 showed the best electrocatalytic activity of cell voltage 1.71 V among the composite membranes. The dual effect of higher proton conductivity and electrocatalytic activity with the addition of HPAs, causes a synergy effect.

Annealing Effect in the Cold-Plastic Deformation of Amorphous PET Material (무정형 PET 재료의 플라스틱 냉간 변형에서의 열처리 효과)

  • Lee, Jong-Young;Park, Seong-Soo
    • Polymer(Korea)
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    • v.25 no.1
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    • pp.56-62
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    • 2001
  • When polyethylene terephthalate(PET) film specimen were stepwise elongated under tension with various speeds of about 0.5~500 mm/min, the necking area, consisted of transparent and opaque bands, was formed during plastic deformation. Stress oscillation was apparently obtained in the stress-strain curve of above specimen. However, stress oscillation was not obtained in the stress-strain curve of annealing specimen. Microstructure was examined dynamically using an optical microscopy and thermal analysis was carried out in a differential scanning calorimeter at a heating rate of 10${\circ}$/min. Also, orientation and crystallization were examined using monochromatic-pinhole technique and elastic modulus was measured by a dynamic mechanical analyzer in the temperature range of -150~70 ${\circ}$ with the frequency of 1 Hz. Transparent PET products were fabricated by use of the PET pellets annealed at 83${\circ}$ for 30 min in an electric furnace.

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Carbon Nanotubes Reinforced Poly(ethylene terephthalate) Nanocomposites (탄소나노튜브로 강화시킨 Poly(ethylene terephthalate) 나노복합재료)

  • Choi, Soohee;Jeong, Youngjin
    • Polymer(Korea)
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    • v.38 no.2
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    • pp.240-249
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    • 2014
  • Multi-walled carbon nanotube (MWNT) reinforced poly(ethylene terephthalate) (PET) composites are studied. To increase the interfacial interactions between PET and MWNTs, the MWNTs are functionalized with bishydroxy-ethylene-terephthalate (BHET). The functionalized MWNTs are melt blended into PET matrix using a twin screw extruder. The amount of MWNTs loaded in PET matrix ranges from 0.5 to 2.0 wt%. After compounding and spinning, the filaments are post-drawn and annealed. To verify the chemical modifications of carbon nanotubes, Raman, $^1H$ NMR, XPS, TGA and FE-SEM are used. The nanocomposites are also analyzed with DSC, TGA, and UTM. These tests show that crystallization temperature and thermal degradation temperature increase due to the functionalized MWNTs. Also, tensile test shows that yield strength and toughness increase more than 30% with addition of only 1 wt% of MWNTs. These results show that the introduction of BHET onto the MWNTs is a very effective way in manufacturing MWNT/PET composite.