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원통형 Saddle Field Ion Source의 특성에 관한 연구

  • Choe, Seong-Chang
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.234-234
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    • 2012
  • Saddle field ion source는 구조가 간단하고 영구자석을 사용하지 않아 소형화에 유리하고 구조가 간단한 DC 파워서플라이를 이용하기 때문에 장치 가격이 저렴하여 다양한 분야에서 응용되고 있으며 특히 이온빔 밀링 분야에 많이 사용된다. 초기 saddle field ion source 는 대칭형의 구형이었으나 지속적인 연구 개발로 와이어형, 원판형, 원통형 등 다양한 형태의 saddle field ion source가 개발되었다. 본 연구에서는 비교적 제작이 용이하고, 구조적으로 외부간섭에 대하여 덜 민감한 원통형 saddle field ion source를 제작하였다. 초기 saddle field ion source는 이온원 내부에 saddle field를 형성하기 위하여 대칭 구조를 가지 형태로 제작되었으나, 비대칭 구조에서도 saddle field가 형성될 수 있고 비대칭 구조를 채택할 경우 한쪽으로 더 많은 이온빔을 인출할 수 있기 때문에 실제 응용면에서는 비대칭 구조가 더 유리하다. 따라서 본 연구에서는 원통형 비대칭 saddle field ion source를 제작하였으며, 제작된 이온소스는 높이가 62 mm 지름이 55 mm의 소형 이온소스였다. 제작된 원통형 saddle field ion source는 진공도와 가속전압에 따라 방전 모드 변화하였다. Saddle field ion source는 전극과 extractor의 구조에 따라 조금씩 다르지만 대체로 5x10-5 Torr ~ 5x10-4 Torr 영역에서 안정적으로 작동하였다. 이온소스 내부의 압력이 높을 경우 수십 mA 의 방전 전류가 흐르는 고전류 방전 모드로 작동하였으며 압력이 낮을 경우에는 동일한 전압에서 수 mA 의 방전 전류만 흐르는 저전류 방전 모드로 작동하였다. 압력이 더 높아질 경우 아크 방전이 발생하여 이온소스의 작동이 불안정하여 연속적인 작동이 어려웠다. 고전류 방전 모드에서는 이온빔 전류가 Child-Langmuir 방정식에 따라 Vi3/2에 비례하여 증가하는 경향을 보여주었으며 저전류 방전 모드에서는 Vi에 선형적으로 증가하였다. 가속 전압이 동일한 경우 고전류 방전 모드가 저전류 방전 모드에 비하여 더 많은 이온빔 인출이 가능하지만, 고전류 방전 모드의 경우 이온의 방출 각도가 매우 넓은 반면 저전류 방전 모드에서는 이온빔의 퍼짐이 현저히 줄어듦을 관찰할 수 있었다. 원통형 saddle field ion source는 내부 구조가 간단하기 때문에 내부 전극의 구조 변화에 따라 방전 특성 및 이온빔 인출 특성이 심하게 변동하였다. Saddle field ion source에서는 Anode에 인가되는 방전 전압이 가속 전압과 같은 역할을 하는데 가속 전압은 2~10 kV 사이에서 인가가 가능하였다. 일반적으로 동일한 방전 모드에서 진공도가 높아질수록 방전 전류의 양과 인출되는 이온의 양이 증가하는 것이 관찰되었다. 제작된 이온소스는 최적 조건에서 5 mm 인출구를 통하여 0.7 mA의 이온빔 인출이 가능하였으며, 9 mm 인출구를 사용한 경우 1 mA까지 이온빔 인출이 가능하였다.

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Synthesis and Structural Analysis of Binary Alloy ($MoRu_3$, $MoRh_3$) (이성분계 금속합금($MoRu_3$, $MoRh_3$)의 합성 및 구조분석)

  • Park, Yong Joon;Lee, Jong-Gyu;Kim, Jong Goo;Kim, Jung Suk;Jee, Kwang-Yong
    • Analytical Science and Technology
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    • v.11 no.3
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    • pp.189-193
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    • 1998
  • Binary alloys, $MoRu_3$ and $MoRh_3$, have been prepared using arc melting furnace. Mo and the noble metals Ru and Rh are the constituents of metallic insoluble residues, which were found in the early days of the post-irradiation studies on uranium oxide fuels. Detailed structural informations about these alloys have not been reported on JCPDS files of ICDD (International Centre for Diffraction Data). The results of X-ray diffraction study showed that the alloy was crystallized in hexagonal close-packing, well known as ${\varepsilon}$-phase. The X-ray diffraction patterns of these alloys matched well to that of $WRh_3$ with $P6_3/mmc$ of space group. The lattice parameters, a and c, were calculated using the least squares extrapolation. It was found from X-ray photoelectron spectroscopic measurements that Mo on the surface of the alloy was oxidized to Mo(6+), which could be removed by sputtering with Ar ions for approximately 15 minutes. The changes in binding energy of Mo, Ru, and Rh on the surface of the alloy were not observed. Magnetic susceptibility measurements resulted in the typical Pauli-paramagnetic behavior in the temperature range of 2 to 300 K.

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The effect of heat input and PWHT on the mechanical properties and microstructure of HSB600 steel weldments with GMAW (HSB600강 가스메탈아크용접부에서 입열량과 용접후 열처리가 기계적 특성과 미세조직에 미치는 영향)

  • Ju, Dong-Hwi;Jang, Bok-Su;Lim, Young-Min;Koh, Jin-Hyun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.5
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    • pp.1939-1946
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    • 2012
  • High performance steel for bridges requires higher performance in tensile and yield strength, toughness, weldability, etc. The purpose of this study is to investigate the weldability of HSB 600 steel. The effects of heat input (1.4~3.2kJ/mm) and postweld heat treatment (PWHT, $600^{\circ}C$, 40hr.) on the TMCP HSB600 steel weldments made by GMAW process were investigated. The tensile strength and hardness of as-welded specimens decreased with increasing heat input. Charpy V-notch impact energy did not show any significant difference by postweld heat treatment. The fine-grained acicular ferrite was mainly formed in the 2.1kJ/mm of heat input while polygonal and side plate ferrites were dominated in the high inputs. Meanwhile, tensile strength and hardness of PWHT weldments decreased due to the coarsening and globularization of ferrite microstructure and reduction of residual stresses with increasing heat inputs. However, there was no significant difference in the impact energy absorption.

Analysis of Orbit Determination of the KARISMA Using Radar Tracking Data of a LEO Satellite (저궤도위성의 레이더 관측데이터를 이용한 KARISMA의 궤도결정 결과 분석)

  • Cho, Dong-Hyun;Kim, Hae-Dong
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.43 no.11
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    • pp.1016-1027
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    • 2015
  • In this paper, a orbit determination process was carried out based on KARISMA(KARI Collision Risk Management System) developed by KARI(Korea Aerospace Research Institute) to verify the orbit determination performance of this system, in which radar tracking data of a space debris was used. The real radar tracking data were obtained from TIRA(Tracking & Imaging Radar) system operated by GSOC(German Space Operation Center) for the KITSAT-3 finished satellite. And orbit determination error was approximately 60m compared to that of the GSOC's orbit determination result from the same radar tracking data. However, those results were influenced due to the insufficient information on the radar tracking data, such as error correction. To verify and confirm it, the error analysis was demonstrated and first observation data arc which has huge observation error was rejected. In this result, the orbit determination error was reduced such as approximately 25m. Therefore, if there are some observation data information such as error correction data, it is expected to improve the orbit determination accuracy.

The Effects of Partial Substitution of Mo and Heat Treatment on the Electrode Characteristics of ZrV0.1Mn0.7Ni1.2 Hydrogen Storage alloy (Ni-MH 2차 전지용 ZrV0.1Mn0.7Ni1.2 수소저장합금의 전극특성에 미치는 Mo의 부분치환과 열처리의 영향)

  • Han, Dongsoo;Oh, Myunghark;Jeong, Chigyu;Chung, Wonsub;Kim, Ingon
    • Transactions of the Korean hydrogen and new energy society
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    • v.9 no.1
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    • pp.16-24
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    • 1998
  • Recently Zr-based $AB_2$ type hydrogen absorbing alloy has received much attention as a negative electrode material for the Ni-MH batteries because of its high capacity. In this study $ZrV_{0.1}Mn_{0.7}Ni_{1.2}$ alloy was chosen and the effects of heat treatment and a partial substitution of the Mo in Mn site on the various electrode properties were investigated. The alloys was prepared by arc melting (as-cast sample). Some of them were heat treated at $1,100^{\circ}C$ for 4 hours. After this they were differentiated by the different cooling rates of slow cooling and quenching. Various electrode characteristics such as activation process, high rate dischargeability and self discharge characteristic were investigated with the three types of electrodes. It was found that heat treated alloys resulted in an increase in plateau flatness of P-C isotherms however both discharge capacity and high rate capability were decreased. And the partial substitution of Mo for Mn in $ZrV_{0.1}Mn_{0.7}Ni_{1.2}$ alloy improved the self-discharge characteristic without the loss of discharge capacity (300mAh/g).

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THE COMPARISON OF POLYMERIZATION OF COMPOSITE RESIN INFLUENCED BY CURING DEPTH AND SHADE (광중합 복합레진의 색상과 깊이에 따른 중합도의 비교)

  • Choi, Kung-Ho;Lee, Ju-Hyun;Park, Ho-Won
    • Journal of the korean academy of Pediatric Dentistry
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    • v.31 no.2
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    • pp.280-289
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    • 2004
  • Adequate polymerization is a crucial factor in obtaining optimal physical properties and clinical performance of resin composite restorative materials. The purpose of this study was to determine the effectiveness of shade and depth on dental composite resin polymerized with plasma arc curing unit employing FTIR and microhardness. From this experiment, the following results were obtained : 1. The light transmission and microhardness by mode 6 in plasma arc curing were similar to by 20 secs in halogen light curing. 2. The experimental groups of A1, A2, A3, A3.5 were not signifcant difference to light transmission and microhardness on surface and 2mm depth, but were significant difference on 3mm and 4mm depth. Especially light transmission and microhardness were small in darker shade and deeper thickness. 3. Compared with depth cure, uncured monomer amount increased at more than 2mm depth. 4. The light transmission by FTIR and polymerization by microhardness were significant corelation.

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$M\"{o}ssbauer$ studies of $NdFe_{10.7}TiM{0.3}(M\;=\;B,\;Ti)$ ($NdFe_{10.7}TiM{0.3}(M\;=\;B,\;Ti)$$M\"{o}ssbauer$ 연구)

  • 김철성;이용종;김윤배;김창석
    • Journal of the Korean Magnetics Society
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    • v.5 no.1
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    • pp.64-70
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    • 1995
  • The authors have studied crystallographic and magrletic properties of $NdFe_{10.7}TiM_{0.3}(M=B,\;Ti)$ by X-ray diffraction, VSM magnetometer, and Mossbauer spectrometer. The Alloys were prepared by arc-melting under argon atmosphere. The $NdFe_{10.7}TiM_{0.3}$ has pure single phase, whereas the $NdFe_{10.7}Ti_{1.3}$ contains some $\alpha-Fe$, from powder X-ray diffractometry. The $NdFe_{10.7}TiM_{0.3}$ has the $ThMn_{12}$-type tetragonal structure with $a_{0}=8.587\;{\AA}\;and\;c_{0}=4.788\;{\AA}$. The Curie temperature ($T_c$) is $570{\pm}3\;K$ from $M\"{o}ssbauer$ spectroscopy performed at various temperatures ranging from 13 to 770 K. Each spectrum of below $T_c$ was fitted with five subspectra of Fe sites in the structure ($8i_{1},\;8i_{2},\;8j_{1},\;8j_{2}\;and\;8f$). The area fraction of the subspectra at room temperature are 16.4, 8.2, 14.8, 21.3 and 39.3 %, respectively. Magenetic hyperfine fields for the Fe sites decrease in the order, $H_{hf}(8i)>H_{hf}(8j)>H_{hf}(8f)$.

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Crystallographic and Magnetic Properties of $NdFe_{10.7}Ti_{1.3}$ ($NdFe_{10.7}Ti_{1.3}$의 결정학적 및 자기적 성질 연구)

  • 이승화;이용종;안성용;김철성;김윤배;김창석
    • Journal of the Korean Magnetics Society
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    • v.6 no.6
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    • pp.361-366
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    • 1996
  • $NdFe_{10.7}Ti_{1.3}$ has been studied with X-ray diffraction, Mossbauer spectroscopy and vibrating sample magnet-ometer(VSM). The alloys were prepared by arc-melting under an argon atmosphere. The $NdFe_{10.7}Ti_{1.3}$ contains some $\alpha-Fe$, from X-ray and Mossbauer measurements. The $NdFe_{10.7}Ti_{1.3}$ has the $ThMn_{12}$-type tetragonal struc-ture with $a_{0}=8.607{\AA}\;and\;c_{0}=4.790{\AA}$. The Curie temperature ($T_c$) of the $NdFe_{10.7}Ti_{1.3}$ is 590 K from $M\"{o}ssbauer$ spectroscopy performed at various temperatures ranging from 13 to 800 K. Each spectrum below $T_c$ was fitted with six subspectra of Fe sites in the structure$(8i_{1},\;8i_{2},\;8j_{2},\;8j_{1},\;8f\;and\;{\alpha}-Fe)$. The area fractions of the subspectra at room temperature are 13.8%, 15.4%, 17%, 16.4%, 34.1% and 3.3%, respectively. Magenetic hyperfine fields for the Fe sites decrease in the order, $H_{hf}(8i)>H_{hf}(8j)>H_{hf}(8f)$. The abrupt changes in the magnetic hyperfine field, isomer shift and magnetic moment observed at about 180 K in $NdFe_{10.7}Ti_{1.3}$ are attributed to spin reorientation.

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Effect of Nb, V and Cr on the High Temperature Oxidation of Ti-(42, 44)% Al Alloys (Ti-(42, 44)%Al 합금의 고온내산화성에 미치는 Nb, V 및 Cr의 영향)

  • Lee, Yeong-Chan;Kim, Mi-Hyeon;Kim, Seong-Hun;Lee, Won-Uk;Baek, Jong-Hyeon;Lee, Dong-Bok
    • Korean Journal of Materials Research
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    • v.9 no.10
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    • pp.1025-1031
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    • 1999
  • Alloys of TiAl with six different compositions. i. e., Ti-(42, 44)Al-2Nb-4V. Ti-(42, 44)Al-4Nb-2V and Ti -(42, 44)Al-4Nb-2Cr, were manufactured by arc-melting. and their oxidation behavior was studied. Both isothermal and cyclic oxidation tests were performed at 700, 800 and $900^{\circ}C$ in air for 50hr. The oxidation resistance increased in the order of Ti-(42, 44)Al-2Nb-4V, Ti-(42, 44)Al-4Nb-ZV and Ti-(42, 44)Al-4Nb-2Cr. It was found that V was a deleterious element, while Cr was a beneficial element in terms of oxidation resistance. During oxidation, a simultaneous interdiffusion was observed. All the constituent elements in the base alloys diffused outward. whereas oxygen from the atmosphere diffused inward, to form triple oxide layers composed of an outermost $\textrm{TiO}_2$ layer. upper ($\textrm{TiO}_2+\textrm{Al}_2\textrm{O}_3$) mixed layer, and lower $\textrm{TiO}_2$-rich layer.

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Evaluation of Scatter Reduction Effect of the Aft-Multiple-Slit (AMS) System Using MC Simulation (MC 시뮬레이션을 이용한 Aft-Multiple-Silt 시스템의 산란선 제거 효과 평가)

  • Chang, Jin-A;Suh, Tae-Suk;Jang, Doh-Yun;Jang, Hong-Seok;Kim, Si-Yong
    • Radiation Oncology Journal
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    • v.28 no.4
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    • pp.224-230
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    • 2010
  • Purpose: We designed the aft-multiple-slit (AMS) system to reduce scatter in cone-beam computed tomography (CBCT). As a preliminary study, we performed a Monte Carlo N-Particle Transport Code (MCNP) simulation to verify the effectiveness of this system. Materials and Methods: The MCNPX code was used to build the AMS geometry. An AMS is an equi-angled arc to consider beam divergence. The scatter-reduced projection images were compared with the primary images only and the primary plus scatter radiation images with and without AMS to evaluate the effectiveness of scatter reduction. To obtain the full 2 dimensional (2D) projection image, the whole AMS system was moved to obtain closed septa of the AMS after the first image acquisition. Results: The primary radiation with and without AMS is identical to all the slit widths, but the profiles of the primary plus scattered radiation varied according to the slit widths in the 2D projection image. The average scatter reduction factors were 29%, 15%, 9%, and 8% when the slit widths were 5 mm, 10 mm, 15 mm, and 20 mm, respectively. Conclusion: We have evaluated the scatter reduction effect of the AMS in CBCT imaging using the Monte Carlo (MC) simulations. A preliminary study based on the MCNP simulations showed a mount of scatter reduction with the proposed system.