• Journal of the Mineralogical Society of Korea
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• v.15 no.2
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• pp.140-144
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• 2002

The sample environment at high temperature for the four circle diffractometer at HANARO in Korea Atomic Energy Research Institute is developed. The performance test was carried out for a structurally known sample through the high temperature experiment with this equipment. In this study we found out that the developed sample environment is stable for a long time experiment at over 900 K. By the neutron diffraction from a single crystal of $LiTaO_3$(phase transition temperature about 900 K) at 298 and 913 K, the lithium atomic positions at both temperatures and disordered state of lithium atom at high temperature were confirmed. These are hardly possible to determine by the conventional X-ray diffraction method.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 1995.04a
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• pp.57-59
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• 1995

• Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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• 2003.04a
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• pp.409-412
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• 2003

본 연구는 호소내 오염된 퇴적물 처리를 위한 전처리 장치로 Hydrocyclone의 이용가능 성을 평가하는 실험이다. 외국의 선행 연구자인 Rietema의 표준 규격을 참고하여 제작된 Hydrocyclone을 이용하여 기흥저수지 퇴적물로 실험을 실시하였다. 실험결과 입자에 따른 오염 도 평가에서는 입자가 작을수록 포함된 오염물의 농도가 높은 것으로 나타났다. 또한 퇴적물을 이용한 장치특성 및 운전조건 변화에 따른 실험에서 공급속도가 빠르고, 공급시료의 농도가 낮으며, 장치의 크기가 작을수록 입자별 분리효율이 높았다.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 1999.10a
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• pp.96-98
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• 1999

환경시료들은 매트릭스의 조성이 매우 복잡하여 공존하는 성분들이 목적성분의 검출에 영향을 미치므로 분리하는 조작이 필요하다. 환경 중에 존재하는 물질들은 동적인 평형상태를 유지하고 있기 때문에 시료를 채취하여 실험실로 운반하여 보관하는 동안에 분석 대상 물질이 용기에 흡착, 휘발 및 화학 반응의 진행 등으로 인하여 시료의 손실 및 변질을 초래 할 수 있다.(중략)

• Journal of the Korean Society for Marine Environment & Energy
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• v.3 no.3
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• pp.34-40
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• 2000

A multisample extraction device was newly designed for efficient extraction of dissolved lipophillic organic compounds from sea water sample. This device allowed extraction of organic compounds from up to 96 sample at a time using 96 multifolder on the principle of solid phase extraction with commercially available octadecyl silane (ODS) cartridges. The recovery yield of the new divice was higher than 90 % while that of conventional liquid-liquid extraction process are only 60 - 70 %. The amount of solvent required for the new device could be reduced to less than 20㎖ per 1ℓ of sample while 1 - 2 ℓ of solvent were used in the conventional liquid-liquid extraction process. The usefulness of this novel method was demonstrated with sea water samples collected from Yellow sea, and the qualitative and quantitative analyses results of the dissolved hydrocarbon showed this method was superior to that of conventional liquid-liquid extraction process in efficiency and reliability.

• Journal of Environmental Science International
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• v.1 no.1
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• pp.41-46
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• 1992

To perform a long-term ambient sampling study at a residential site, an air sampler was constructed to collect 24-hour integrated air samples suitable for the volatile organic compounds (VOCs) analysis. It includes an esthetically acceptance due to proximity to homes, as fell as providing the required sampling specifications. The VOCs sampler accomodates four 5/8 "stainless steel(SS) traps packed with adsorbent(Tenax) and is capable of four flow rates in the range of 5 to 50 cc/min. Sintered metal filters(10 micrometer) were directly connected to the inlet of the trap adapters. Additional specifications include: 1) constructed of organically inert materials, 2) weatherproof, 3) battery operated, 4) collecting of VOCs at a breathing zone level, and 5) quiet operation with micro diaphragm pumps wrapped by the sponge. The pump/battery system was separated from the sampling shelter. Sound levels measured for this system were below permissible sound levels (NJDEP) at a residential site. The sampler has been successfully operated at both ground level in a residential area and on the roof of a one story elementary school.hool.

• Proceedings of the Acoustical Society of Korea Conference
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• 1994.06c
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• pp.310-313
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• 1994

전화망을 이용하여 다양한 환경을 내포한 음성시료를 수집하여 스펙트럼 기울기의 변동을 검토함으로써 지역간 전화회선 특성을 파악하고, 시료수집은 발화자수 선정모델을 근거로 광주, 전남지역에 거주하는 84명을 대상으로 영역별, 연령별, 성별로 구분하여 수집하였다. 또한, 데이터 수집방법은 수집장치와 발화자가 시나리오의 정해진 순서에 따라 작성되었다.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 2003.11a
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• pp.372-373
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• 2003

오늘날 강수의 오염도는 대기오염의 중요한 지표가 되고 있으며, 특히 산성화된 강수는 생태계에 심각한 악영향을 주고 있어 전세계적으로 이에 대한 연구가 지속적으로 이루어지고 있다. 우리나라에서도 환경부 및 지방자치단체에서 산성비 측정망을 운영하면서 강수의 산성도 및 수용성 이온성분의 농도 측정을 수행하고 있으나 현재 강수자동채취장치와 수동채취장치를 같이 사용하고 있어 그 분석자료의 정도관리에 상당한 문제점이 있는 것으로 드러나고 있다. (중략)

• Analytical Science and Technology
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• v.26 no.1
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• pp.34-41
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• 2013

Split-flow thin cell (SPLITT) fractionation (SF) is a rapid separation technique capable of separating colloidal particles or macromolecules into two or more fractions. SF allows fractionations in a preparative scale as sample is fed continuously. Generally SF uses a thin ribbon-like channel equipped with two flow stream splitters at the inlet and outlet of the channel. Thus there exist two flow inlets and two flow outlets at the top and bottom of the inlet and outlet of the channel, respectively. There are two operating modes in SF, conventional mode and full-feed mode (FFD). Although the resolution in the FFD mode is lower than that in the conventional mode, FFD mode has some merits. The design of the channel and operation are simpler in the FFD mode, as it does not require the feeding of the solvent. Thus there is no flow stream splitter at the channel inlet, and only one pump is needed, unlike the conventional mode, where two pumps are required for the feedings of the sample and the solvent separately. Also the sample is not diluted in the FFD mode as there is no solvent feeding, which is important for fractionation samples with low colloidal concentrations such as environmental samples. For some of environmental samples, pre-concentration is often required. In this study, a new large-scale splitter-less FFD-SF channel was implemented, where there is no splitter at the outlet as well as at the inlet of the channel. It was possible to build the channel in a much larger dimension than conventional ones, allowing much higher sample throughput (TP). The new channel was tested and optimized with polyurethane (PU) latex beads, and then applied to large-scale separation of Polyacrylate (PA).

• Journal of the Korean GEO-environmental Society
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• v.7 no.2
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• pp.55-66
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• 2006

The existing Highway LA-1 of US is required to be replaced for covering increasing regional demands of transportation such as Hurricane evacuation and oil industry. This 28 km crosses wetlands and is a sensitive environmental area. Huge amount of soil investigation and laboratory tests were performed with best efforts to overcome inherit errors of sampling, disturbance, and testing procedures for this project. The data scattering was corrected through using central tendency theory.