• Title/Summary/Keyword: 시간 분해 측정

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Chemical Age Dating of Zircon and Monazite by E1ectron Microprobe (전자현미분석기를 이용한 저어콘 및 모나자이트의 화학적 연대 측정법)

  • 이석훈
    • The Journal of the Petrological Society of Korea
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    • v.10 no.3
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    • pp.179-189
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    • 2001
  • The determination of trace concentration of U, Th and Pb was carried out for chemical dating of zircon and monazite by electron microprobe. Detection limit and error range should be considered to measure characteristic X-rays of M-line from those minerals, which are low in the ionization of atom and low peak intensity in the spectrum. The element of U, Th and Pb were simultaneously measured with 3 spectrometers equipped with PET crystal to reduce a total counting time and error due to drift of instrumental operating condition. Detection limit could be improved from increase of the peak/background ratio through adjusting pulse height analyzer about 1000 mv baseline. Under permissible maximum analytical conditions, theoretical detection limit of U, Th and Pb is down to 30 ppm (99% confidence level). The analytical result was maintained at a relative error $\pm$10% ($2{\sigma}$) in 800 ppm Pb, $\pm$5% ($2{\sigma}$) in 2330 ppm U and $\pm$10% ($2{\sigma}$) in dating from a single measurement of zircon at 15 keV and 100 nA. However, for the precise dating of zircon and monazite, if it is considered a 3 $\mu\textrm{m}$ spatial resolution, <100 ppm ($3{\sigma}$) detection limit and <$\pm$10% ($2{\sigma}$) relative error, optimum analytical conditions are given as 15~20 keV accelerating voltage, 100~200 nA beam current and 300~1200 sec total counting time. To reduce material damage by high current, there is need to be up to 3~5 $\mu\textrm{m}$ of electron beam diameter, or to use arithmetic average of multiple measuring at a shorter counting time. A younger or relatively low concentration rocks can be dated chemically by lower detection limit and improved precision resulted from increase of current and measuring time.

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TomoTherapy: Analysis of treatment time and influencing factor (TomoTherapy: 치료 소요시간 및 영향 요인 분석)

  • Son, Jong Gi;Kang, Hyun Sung;Hwang, Chul Hwan;Se, Seung Jeong;Choi, Min Ho
    • The Journal of Korean Society for Radiation Therapy
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    • v.29 no.2
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    • pp.119-128
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    • 2017
  • Purpose: The purpose of this study was to measure the average actual treatment time at the time of Tomotherapy treatment. We want to investigate the time required for the procedure in the treatment process that affects the actual treatment time. Patients and Methods: We measured the time required by the procedure in 31 patients who were treated with tomography therapy. Beam-on time, Image registration time, Set-up with scan time and Actual treatment time were measured and stepwise regression analysis was performed. Result: The average treatment time per a patient was 21.44 - 23.92 minutes. Beam-on time, Image registration time, and Set-up with Scan time were the important factors affecting the actual treatment time. The biggest influence was Beam-on time and Registration time was less affected by analysing. Conclusion: The average treatment time per a patient in tomotherapy treatment was $22.68{\pm}3.37$ minutes. The Approximately 21 patients are expected to be treated within 8 hours of regular work time. However, if the treatment is interrupted or the time of the procedure is changed during the treatment process, it affects the schedule of the daily treatment patients and the workload is expected to increase.

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Measurement of Molecular Weight and Heating Properties of Korean White Ginseng Protein (백삼 단백질의 가열특성과 분자량 측정)

  • 박상욱
    • The Korean Journal of Food And Nutrition
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    • v.17 no.1
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    • pp.66-71
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    • 2004
  • This study was carried out to elucidate the molecular weight and the heating properties of Korean white ginseng protein by CM-cellulose column chromatography and electrophoresis. Thermostable protein contents were 0.17% in xylem-pith and 0.15% in cortex-epidermis of tap root by 90min of heating. The contents of thermostable protein were decrease after 90min of heating. By Electrophoresis, seven bands of 66, 45, 29, 24, 22, 20, 12kD were observed up to 30min of heating, but the band of 22kD was disappeared after 60min. of heating. The cationic protein content of thermostable protein fraction (28.24%) was higher than the anion protein content(0.80%). The molecular weight of thermostable protein fractions were 66kD, 55kD, 36kD and those of thermolabile protein fractions were 29kD, 24kD, 22kD, 20kD.

Labeling Efficiency of $^{99m}Tc$-Labeled RBC Due to Labeling Time Change (표지시간 변화에 의한 $^{99m}Tc$과 적혈구 표지효율)

  • Dong, Kyeong-Rae;Kim, Ho-Seong;Choi, Seong-Kwan
    • Journal of radiological science and technology
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    • v.30 no.3
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    • pp.259-263
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    • 2007
  • For the preparation of $^{99m}Tc$-labeled RBC, $10{\sim}20\;{\mu}g/kg$ of Stannous(II) chloride and $10{\sim}40\;min$ of preparation was used. For finding out the effect of contrast agent, the blood samples were collected in three days, seven days, and 1 months after the diagnostic procedure. In the normal volunteer, the concentration of reducing agent and preparation time did not effect on the radiochemical yield. But in the patients, 10 mg of Stannous(II) chloride and 60 min incubation times was shown high radiochemical yield. Contrast agent has a significant effect on the radiochemical yield. Although the blood samples which were collected after seven days of diagnostic procedure did not effect on the radiochemical yield of $^{99m}Tc$-labeled RBC, but the radiochemical yield of $^{99m}Tc$-labeled RBC which was prepared with a sample of high concentration of contrast agent in blood led to low radiochemical yield. For these samples, the modified method showed high radiochemical yield than previous in vivo preparation method. The recommended method is followed. Blood collecting was performed at 30 minutes after injection of reducing agent, and it is centrifuged for removal of plasma. After addition of $^{99m}TcO^-_4$, sample reservoir was rotated. After addition of normal saline, and it is centrifuged for separation of saline. Then $^{99m}Tc$-labeled RBC was obtained after removal of saline.

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An Improvement of Recovery Characteristics of ISFET Glucose Sensor by Employing Oxygen Electrolysis (산소분자의 전기분해법을 도입한 ISFET 포도당센서의 회복특성 개선)

  • Park, Keun-Yong;Choi, Sang-Bok;Lee, Young-Chul;Lee, Min-Ho;Sohn, Byung-Ki
    • Journal of Sensor Science and Technology
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    • v.9 no.3
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    • pp.203-207
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    • 2000
  • The sensitivity of ISFET glucose sensor is improved by employing amperometric actuation method. However, this method takes long time to recover the primary output voltage after measurement because of slow migration of the hydrogen ion between internal and external sensing membranes. Consequently, such a recovery-time delaying problem is one of obstacles to a practical use. In this paper, a new method is proposed to control the concentration of hydrogen ion in internal membrane, which applies a reduction potential to the working electrode for supplying hydroxide ion. Experimental results show that the recovery-time was reduced within 2 minute against decades minute of conventional method.

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Determination of Optimum Sterilization Condition for the Production of Retort Pouched Curry Sauce (레토르트 카레 소스 생산을 위한 최적살균 조건의 설정)

  • Chung, Myong-Soo;Cha, Hwan-Soo;Koo, Bon-Youl;Ahn, Peong-Ug;Choi, Chun-Un
    • Korean Journal of Food Science and Technology
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    • v.23 no.6
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    • pp.723-731
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    • 1991
  • In order to optimize sterilization conditions of retort pouched curry sauce, sterilization processes for eighteen conditions by varying temperature, time and method were conducted through $3^{2}{\times}2^{1}$ experimental factorial design. Quality evaluations before and after sterilization included measurements of vitamin (niacin) retention, pH and color differences, and organoleptic test(taste, color and viscosity). $F_{o}$ values were also measured at each condition. Product qualities were mainly affected by sterilization temperature and time, whereas sterilization method had no significant effect. Effect of sterilization time on product qualities was higher than that of sterilization temperature. From the response surface analysis, an optimum range of sterilization condition simultaneously satisfying desired specifications was determined to be $123.5^{\circ}C$, 21.5 min to $127.5^{\circ}C$, 17.0 min. In this range, the sterility($F_{o}$ value) at a cold point during sterilization was approximately 15.0 min.

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Biocompatibility of Biodegradable Films by Natural Polymers (천연고분자 분해성 필름의 생체적합성 연구)

  • Hwang, Sung Kwy;Lee, Ki Chang;Rhim, Kook Hwan
    • Applied Chemistry for Engineering
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    • v.10 no.6
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    • pp.939-943
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    • 1999
  • Recently there has been an explosion of interest in the topic of biodegradable polymers for medical applications. In this study, films were prepared by solution casting method using natural polymers (xanthan, locust bean, guar gum, chitosan and algin) as biomaterials. Biocompatibility of films prepared from natural polymer as a skin implant was evaluated. These biodegradable films were subcutaneously implanted in the back of rats and their biodegradability was investigated by the evaluation of changes in structure, film weight and hematology as a function of time for the biotransformation. The result of rats test showed that locust bean and guar gum induced some suspects of non-biocompatibility in the tissue by foreign body reaction 24 and 48 hrs after implantation. These results showed the potential of partial biodegradable films prepared from natural polymer for ideal skin biomaterials at short period.

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Changes in Methyl Pyrazines of Cocoa Beans during Microwave Roasting (Microwave Roasting에 의한 Cocoa Bean의 Methyl Pyrazine류의 변화)

  • Lee, Joo-Hee;Kim, Suk-Shin
    • Korean Journal of Food Science and Technology
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    • v.32 no.3
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    • pp.654-658
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    • 2000
  • Flavor components focused on the methyl pyrazines(2,3-dimethyl pyrazine, 2,3,5-trimethyl pyrazine, tetramethyl pyrazine) of microwave-roasted cocoa beans were determined and compared with those of conventionally-roasted cocoa beans. Domestic microwave oven was modified to design the microwave roasting system. Temperature measurement technique using thermocouple probes was developed to determine the center temperature of cocoa beans during microwave roasting. Microwave roasting was carried out under two different conditions. Under the first condition, roasting time was fixed to 30 min, while roasting temperature was varied to $110^{\circ}C,\;120^{\circ}C,\;130^{\circ}C,\;140^{\circ}C,\;and\;150^{\circ}C$ Under the second condition, roasting temperature was fixed to $130^{\circ}C$, while roasting time was varied to 5 min, 10 min, 20 min, and 30 min. Conventional roasting was done at $120^{\circ}C$ for 15 min as a reference. Amount of methyl pyrazines and their ratios were influenced by microwave roasting temperature and roasting time. The most suitable methyl pyrazine ratio of cocoa beans was obtained at $140^{\circ}C$ for 30 min of microwave roasting.

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Measurement of Viscoelastic Properties of Heat Denatured Gluten Network (열변성 글루텐의 점탄성 측정에 관한 연구)

  • Hong, Sung-Hie;Lee, Cherl-Ho
    • Korean Journal of Food Science and Technology
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    • v.20 no.2
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    • pp.148-156
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    • 1988
  • A method for the measurement of viscoelastic properties of heat denatured gluten network was developed in order to evaluate the noodle making quality of wheat flour. The stress relaxation of elongated heat denatured gluten network could be expressed by 6-element generallized Maxwell model. The tensile force of heat denatured gluten network increased by the heating time. The elastcity and viscosity of the first exponential term which covers 70-74% of the total relaxation increased as cooking time was extended up to 1q min. The addition of gluten network strengthening agent, potassium bromate, at 1000ppm level reduced the elasticity and viscosity, while weakening agent, L-cystein, increased them. The relaxation time decreased after 11 min of cooking in both cases. The elasticity and viscosity of heat denatured gluten were affected differently by the concentration of added urea.

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A Study on Degradation Rate of Carbofuran in Sterilized Soil and Sulfate-added Paddy Soil (Carbofuran의 담수토양중(湛水土壤中) 분해(分解)에 대한 토양(土壤)의 멸균(滅菌)과 황산염(黃酸鹽) 첨가(添加)의 영향(影響)에 관(關)한 연구(硏究))

  • Tu, Ock-Ju
    • Korean Journal of Environmental Agriculture
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    • v.17 no.1
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    • pp.11-15
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    • 1998
  • Carbofuran was incubated for four weeks in five types of paddy soil samples at $25^{\circ}C$. The soil samples prepared in the study were as follows : control soil, sterilized soil, 10% cellulose added soil, 10% cellulose and 1% ferrous sulfate added soil, and 10% cellulose and 1% magnesium sulfate added soil. The degradation rate of carbofuran was significantly decreased(p<0.05) in sterilized soil.The degradation rate of carbofuran was significantly decreased by addition of cellulose(p<0.05) in femous sulfate added soil and magnesium sulfate added soil(p<0.01).

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