• Journal of Hydrogen and New Energy
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• v.21 no.4
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• pp.340-345
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• 2010

For the conversion into hydrogen society, not only studying facilities of hydrogen production, storage, transportation and charging system but also developing technique of ensuring safety are essentially needed. Hence, for the first step of that, evaluated the hydrogen embrittlement of Inconel alloy 617, Ni-based super heat-resisting alloy, by small punch test. Prepared the various specimens through changing electrochemical charging time and measured the toughness degradation of the specimens by small-punch test. The analysis of hydrogen embrittlement behavior were carried out by investigating the fractured surface of specimens. This study has significance on revealing mechanism of hydrogen embrittlement behavior and the factor affecting hydrogen embrittlement in the future study.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.7 s.178
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• pp.1753-1762
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• 2000

An inverse method is presented to obtain material's flow properties by using small punch test. This procedure employs, as the objective function of inverse analysis, the balance of measured load-di splacement response and calculated one during deformation. In order to guarantee convergence to global minimum, simulated annealing method was adopted to optimize the current objective function. In addition, artificial neural network was used to predict the load-displacement response under given material parameters which is the most time consuming and limits applications of global optimization methods to these kinds of problems. By implementing the simulated annealing for optimization along with calculating load-displacement curve by neural network, material parameters were identified irrespective of initial values within very short time for simulated test data. We also tested the present method for error-containing experimental data and showed that the flow properties of material were well predicted.

• Proceedings of the KSME Conference
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• 2000.11a
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• pp.193-198
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• 2000

The small punch test have been developed to evaluate the material strength of the power plant components. This small punch test specimen is very small than the conventional strength test specimens. Korea Electric Power Research Institute (KEPRI) have been applying this test to assess accurately the life of thermal power plant and enhancing the reliability. The small punch test for gas turbine blades is under development. It's possible to compare the relative strength among the same materials having different operation histories. In this paper, the strength reductions of gas turbine materials are investigated by the small punch tests. All materials shows the almost same strength and deformation with the allowable deviation. At the same test temperature, the damaged material has the maximum load value. The strength reduction is not shown in this small punch test results.

• Journal of Energy Engineering
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• v.18 no.1
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• pp.49-55
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• 2009

Occurrence of hydrogen embrittlement could be one of the main obstacles for using structural equipment under hydrogen environment. It is required to develop assessment methods of hydrogen embrittlement for the metals used in production, storage, transmission and application utilities of hydrogen. The most probable method of hydrogen mass transmission is using existing natural gas pipeline. Base or weld part of the pipeline can be damaged by mixed gas of hydrogen in the pipeline. In this study small punch (SP) testing was employed to evaluate the hydrogen embrittlement behavior for a line pipe steel (API X65) with electrochemically hydrogen charged specimens. Results showed that the SP test can be a good candidate test method for hydrogen damage evaluation method. Strength of steel is known to be decreased with the level of hydrogen charging. However, for API X65 steel base metal need in this study, the effect of hydrogen to strength was not significant. It can be negligible regardless of the hydrogen contents in the steel. With this test different strength levels with various hydrogen charging conditions were observed. It can also be anticipated that more sensitive evaluation of material behavior be obtainable by the SP test method.

• Proceedings of the KWS Conference
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• 1998.05a
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• pp.49-51
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• 1998

• Proceedings of the Korean Nuclear Society Conference
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• 1998.10a
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• pp.207-207
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• 1998

• Journal of the Korean Institute of Gas
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• v.15 no.4
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• pp.21-26
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• 2011

Type-3 cylinder liner has a limitation of machining the standard specimen for fracture toughness test because it has approximately 5 mm in thickness as well as a curvature. Hence, it needs to be employed a miniature specimen test technique to evaluate fracture toughness of the cylinder liner. In this study, small punch (SP) test method was employed to evaluate fracture toughness of the cylinder liner. Load-displacement curve result measured from the SP test showed that the liner material was failed during membrane stretching in the general SP load-displacement curve. Additionally, it was shown that liner material was isotropic although the amount of plastic deformation was different depending on the direction due to manufacturing process characteristics. Fracture toughness, $J_{Ic}$, was evaluated using the SP test data. The value of fracture toughness obtained was $13.0kJ/m^2$. This value was similar to that of the same kind of materials. Therefore, the fracture toughness evaluated using the SP test data was reasonable.

• Transactions of the Korean Society of Mechanical Engineers
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• v.17 no.8
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• pp.2033-2042
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• 1993

In conventional SCC susceptibility test, there are constant strain test, constant load test, slow strain rate test(SSRT) and K$_{ISCC}$ test. Among them, the SSRT method is much more aggressive in producing SCC than the other tests, so that the test time of it is considerably reduced. But this SSRT method has mostly been worked using the uniaxial tensile specimen untill now. Therefore, the SSRT method using the tensile specimen(Ten-SSRT) has much difficulty in SCC susceptibility evaluation of a localized region like weldment and the advantage material of high order. Recentely, the small punch(SP) test method using miniaturized small specimen is the very effective test method for fracture strength evaluation of a localized region like weldment and fusion reactor wall irradiated in the nuclear power plant. This paper investigated the possibility of SCC susceptibility evaluation by the SP-SSRT method using the miniaturized small specimen. Therefore, we obtained the result that the SP-SSRT had the possibility for the evaluations of SCC susceptibility for shorter time to corrosive environment compare to Ten-SSRT which was conventional method.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.12
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• pp.1497-1502
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• 2013

When using hydrogen gas as an ecofriendly energy sources, it is necessary to conduct a safety assessment and ensure thereliability of the hydrogen pressure vessel against hydrogen embrittlement expected in the steel materials. In this study, by applying the in-situ SP test method, the gas hydrogen embrittlement behaviors in SA372 steel, which is commonly used as a pressurized hydrogen gas storage container, were evaluated. To investigate the hydrogen embrittlement behavior, SP tests at different punch velocities were conducted for specimens with differently fabricated surfaces at atmospheric pressure and under high-pressure hydrogen gas conditions. As a result, the SA372 steel showed significant hydrogen embrittlement under pressurized hydrogen gas conditions. The effect of punch velocity on the hydrogen embrittlement appeared clearly; the lower punch velocity case indicated significant hydrogen embrittlement resulting in lower SP energy. The fractographic morphologies observed after SP test also revealed the hydrogen embrittlement behavior corresponding to the punch velocity adopted. Under this pressurized gas hydrogen test condition, the influence of specimen surface condition on the extent of hydrogen embrittlement could not be determined clearly.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.12
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• pp.2565-2573
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• 2002

A basic research was performed to ensure the usefulness of Small Punch-creep(SP-creep) test for residual life evaluation of heat resistant components effectively. This paper presents analytical results of initial stress and strain distributions in SP specimen caused by constant loading for SP-creep test and its experimental correlations with uniaxial creep(Ten-creep) test on 9Cr1MoVNb steel. It was shown that the initial maximum equivalent stress, ${\sigma}_{eq{\cdot}max}$ from FE analysis was correlated with steady-state equivalent creep strain rate, ${\epsilon}_{qf-ss'}$ rupture time, $t_r$, activation energy, Q and Larson-Miller Parameter, LMP during SP-creep deformation. The simple correlation laws, ${\sigma}_{sp}-{\sigma}_{TEN}$, $P_{sp}-{\sigma}_{TEN}\; and\; Q_{sp}-Q_{TEN}$ adopted to established a quantitative correlation between SP-creep and Ten-creep test data. Especially, the activation energy obtained from SP-creep test is linearly related to that from Ten-creep test at $650^{\circ}C$ as follows : $Q_{SP-P}\;{\risingdotseq}\;1.37 \;Q_{TEN},\; Q_{SP-{\sigma}}{\risingdotseq}1.53\; Q_{TEN}$.