• Title/Summary/Keyword: 소결 온도

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A Study on the Material Characteristics of Contacts on Bias Track Relay (바이어스 궤도계전기 접점의 재질 특성에 관한 연구)

  • Kim, Hee-Dae;Lee, Sung-Il
    • Journal of the Korean Society for Railway
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    • v.15 no.6
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    • pp.597-603
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    • 2012
  • The cases for selecting contact materials of Ag and AgC for Bias Track Relay are the studies and their safety evaluations are proposed in this paper. The welding at the relative low current has occurred in Ag contacts, but the one has not occurred in AgC contacts although the high currents flow since it has an excellent temperature characteristic. In the repetitive switching experiment, more unstable resistance and transfer phenomena has occurred in contacts as the switching numbers of AgC contacts increase, which results in more consumption of contacts. In the experiments, there exists a trade off relationship between welding and resistance variation. AgC contacts have excellent characteristics in welding, but the caution is required in using them since a lot of repetition switching produces much resistance variation. However, Ag contacts have excellent characteristics in repetitive switching, but weak ones in welding.

Electrical properties of PZN-PZT thick films formed by aerosol deposition process (에어로졸 증착법에 의해 제조된 PZN-PZT 후막의 전기적특성)

  • Tungalaltamir, Ochirkhuyag;Jang, Joo-Hee;Park, Yoon-Soo;Park, Dong-Soo;Park, Chan
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.5
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    • pp.183-188
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    • 2020
  • Lead zinc niobate (PZN)-added lead zirconate titanate (PZT) thick films with thickness of 5~10 ㎛ were fabricated on silicon and sapphire substrates using aerosol deposition method. The contents of PZN were varied from 0 %, 20 % and to 40 %. The PZN-added PZT film showed poorer electrical properties than pure PZT film when the films were coated on silicon substrate and annealed at 700℃. On the other hand, the PZN-added PZT film showed higher remanent polarization and dielectric constant values than pure PZT film when the films were coated on sapphire and annealed at 900℃. The ferroelectric and dielectric characteristics of 20 % PZN-added PZT films annealed at 900℃ were compared with the result values obtained from bulk ceramic specimen with same composition sintered at 1200℃. As annealing temperature increased, dielectric constant increased. These came from enhanced crystallization and grain growth by post heat treatment.

Synthesis of β-tricalcium Phosphate by Using an Eggshell (달걀껍질을 이용한 생체용 β-tricalcium Phosphate 분말의 합성)

  • Kwon, Myoung-Do;Oh, Sun-Ho;Lee, Sang-Jin
    • Journal of the Korean Ceramic Society
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    • v.39 no.11
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    • pp.1103-1107
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    • 2002
  • Biocompatible ${\beta}$-Tricalcium Phosphate(${\beta}$-TCP) powder was successfully synthesized by using a re-cycled eggshell and phosphoric acid. The crystallization behavior of the synthesized powder was dependent on the mixing ratio between the eggshell and phosphoric acid, the starting condition of the eggshell and calcination temperature. The ${\beta}$-TCP was stably synthesized in the 1:1.3~1:1.5 (wt%) mixing ratios of calcined eggshell and phosphoric acid. The synthesis was achieved at about $900{\circ}$ for 1h in an air atmosphere. The crystalline development and microstructure of the synthesized powder were examined by X-ray diffractometer and scanning electron microscopy.

A Study on the Magnetic Properties of YIG Ferrites with Zr-Substitution (Zr치환에 따른 YIG계 페라이트의 자기적 특성 연구)

  • 양승진;윤종남;김정식
    • Journal of the Korean Ceramic Society
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    • v.40 no.5
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    • pp.428-433
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    • 2003
  • In this study, we investigated the variation of microstructural and electromagnetic properties of YIG ferrites for Isolator/Circulator application with the sintering temperature and Zr addition. The composition of the ferrites was Y$_{2.1}$Ca$_{0.9}$Fe$_{4.4-x}$V$_{0.5}$In$_{0.05}$Al$_{0.05}$Zr$_{x}$O$_{12}$ with x=0, 0.05, 0.1 and 0.2. The YIG ferrites were prepared by the conventional ceramic sintering process. The Zr-substituted YIG ferrite, Y$_{2.1}$ Ca$_{0.9}$Fe$_{4.4-x}$V$_{0.5}$In$_{0.05}$Al$_{0.05}$ Zr$_{x}$O$_{12}$ showed the highest saturation magnetization (1097 gauss) at x=0.1. The microwave properties were shown as isolation of 18.60 dB and insertion loss of 0.45 dB at x=0.2. Additionally, Zr-substitution was effective in decreasing ferromagnetic resonance linewidth with Zr content.

A study on the glass fabrication and sintering behaviour of glass/ceramics for SiO2-TiO2-RO(RO: BaO, CaO, SrO) system (SiO$_2$-TiO$_2$-RO(RO: BaO, CaO, SrO)계 고유전율 유리 제조 및 글라스/세라믹스의 소결 거동에 관한 연구)

  • 구기덕;오근호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.4
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    • pp.626-633
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    • 1998
  • For the fabrication of low temperature cofirable glass/ceramic with high dielectric constant, crystallizing glass [$SiO_2-TiO_2-RO (RO:BaO, CaO:SrO)$] was formed. The glass/ceramic composites were made by mixing this glass and alumina ceramic as filler, and its characteristics was investigated. With this glass compositon, it was possible to fabricate the glass which could be crystallized under $900^{\circ}C$. And it was found that the crystallizing temperature was changed in accordance with the composition of RO in glass. By adding $Bi_2O_3$ as flux, using $Al_2O_3$ as filler and sintering at $860^{\circ}C$, low temperature cofirable glass/ceramic with high dielectric constant was fabricated. The density of that composites was 3.96 g/$\textrm{cm}^3$, dielectric constant was 17 and Q. f was 600.

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Nb doped strontium titanate single crystal growth by floating zone method (Floating zone법에 의한 Nb를 첨가한 strontium titanate 단결정 성장)

  • Jeon, Byong-Sik;Cho, Hyun;Orr, Keun-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.3
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    • pp.215-222
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    • 1995
  • Nb doped strontium titanate single crystals were grown by the floating zone method. The doping amount of $Nb_2O_5$ was 0.2 wt %. Those crystals were grown in air and N z atmosphere and the growth rate was 5 mmlhr and rotation speed of upper and lower shaft was 30 rpm. The shapes of melt - feed rod interface depending on sintering temperatures were observed. In air atmosphere, the flow rate of air was 1.5 ${\ell}/min$ and in $N_2$ atmosphere, that of $N_2$ gas was 0.5 ${\ell}/min$. As grown crystals were analyseQ by XRD, Laue back - reflection and chemical etching. After annealing in $N_2$ atmosphere, resistivities of crystals were measured and the activation energies of each samples were calculated.

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Study on the Sintering Temperature and Electrical Properties of CuO Doped (Ba0.5,Sr0.5)TiO3 Ceramics (CuO를 첨가한 (Ba0.5,Sr0.5)TiO3 세라믹의 소결온도와 전기적 특성의 연구)

  • Yun, Seok-Woo;Lee, Ku-Tak;Kang, Ey-Goo;Koh, Jung-Hyuk
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.6
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    • pp.454-457
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    • 2010
  • The influence of CuO addition on what of the $(Ba,Sr)TiO_3$ ceramics was studied. The sintering temperature of $(Ba,Sr)TiO_3$ ceramics was lowered by the addition of CuO additives. The 1 - 5 wt% CuO were selected and employed as the sintering aids. Low-Temperature Co-fired Ceramic technologies are popular technologies used in the manufacture of microwave devices. In this study, crystalline and electrical properties of CuO doped $(Ba,Sr)TiO_3$ ceramics were investigated to determine the low temperature sintering properties. The addition of CuO to $(Ba,Sr)TiO_3$ lowered the sintering temperature from $1350^{\circ}C$ to $1150^{\circ}C$. The dependence of the sintering temperature shrinkage rate and mechanism of CuO doped $(Ba,Sr)TiO_3$ ceramics are investigated and discussed. Also, the crystalline structure of CuO - doped $(Ba,Sr)TiO_3$ ceramics is discussed by the X-ray diffraction (XRD) method.

Structural and Microwave Dielectric Properties of the $Mg_5B_4O_{15}$ (B=Ta, Nb) Ceramics with Sintering Temperature (소결온도에 따른 $Mg_5B_4O_{15}$ (B=Ta, Nb)세라믹스의 구조 및 마이크로파 유전특성)

  • Lee, Sung-Jun;Kim, Jae-Sik;Lee, Sung-Gap;Lee, Young-Hie
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.56 no.3
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    • pp.556-560
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    • 2007
  • In this study, both structural and microwave dielectric properties of the $Mg_5B_4O_{15}$ (B=Ta, Nb) cation-deficient perovskite ceramics with sintering temperature were investigated. All sample of the $Mg_5B_4O_{15}$ (B=Ta, Nb) ceramics were prepared by the conventional mixed oxide method and sintered at $1400^{\circ}C{\sim}1500^{\circ}C$. The bulk density and quality factor of the $Mg_5B_4O_{15}$ (B=Ta, Nb) ceramics were increased with increasing sinterning temperature in the range of $1400^{\circ}C{\sim}1450^{\circ}C$, but these were decreased the sintering temperature of above $1450^{\circ}C$. The dielectric constant of the $Mg_5Ta_4O_{15}$ ceramics was increased continuously with increasing sintering temperature. And the dielectric constant of the $Mg_5Nb_4O_{15}$ ceramics was increased in as the sintering temperature increasesfrom $1400^{\circ}C{\sim}1450^{\circ}C$ but was decreased at the temperatures above $1475^{\circ}C$. In the case of the $Mg_5Ta_4O_{15}\;and\;Mg_5Nb_4O_{15}$ ceramics sintered at $1450^{\circ}C$ for 5h, the dielectric constant, quality factor, and temperature coefficient of the resonant frequency (TCRF) were 8.2, 259,473 GHz, $-10.91ppm/^{\circ}C$ and 14, 37,350 GHz, $-52.3ppm/^{\circ}C$, respectively.

Piezoelectric Properties of 0.98(Na0.5K0.5)NbO3-0.02Li(Sb0.17Ta0.83)O3+0.01wt%ZnO Ceramics with a Sintering Temperature (소결 온도에 따른 0.98(Na0.5K0.5)NbO3-0.02Li(Sb0.17Ta0.83)O3+0.01wt%ZnO 세라믹스의 압전 특성)

  • Lee, Dong-Hyun;Lee, Seung-Hwan;Lee, Sung-Gap;Lee, Ku-Tak;Lee, Young-Hie
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.7
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    • pp.543-546
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    • 2011
  • We studied sintering temperature to enhance the piezoelectric properties of $0.98(Na_{0.5}K_{0.5})NbO_3-0.02Li(Sb_{0.17}Ta_{0.83})O_3$+0.01wt%ZnO (hereafter NKN-LST+ZnO) lead free piezoelectric ceramics. The synthesis and sintering method were the conventional solid state reaction method and sintering was executed at $1,080\sim1,120^{\circ}C$. We found that NKN-LST+ZnO ceramics at optimal sintering temperature showed the improved piezoelectric properties at the optimal sintering temperature. The NKN-LST+ZnO ceramics show good performance with piezoelectric constant $d_{33}$= 153 pC/N sintered at $1,090^{\circ}C$. The results reveal that NKN-LST+ZnO ceramics are promising candidate materials for lead-free piezoelectric application.

Adsorption of Heavy Metals on Sludge from the Treatment Process of Acid Mine Drainage (산성광산배수(AMD) 처리(處理) 슬러지의 중금속(重金屬) 흡착(吸着) 특성(特性))

  • Song, Young-Jun;Lee, Gye Seung;Shin, Kang Ho;Kim, Youn-Che;Seo, Bong Won;Yoon, Si-Nae
    • Resources Recycling
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    • v.21 no.4
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    • pp.35-43
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    • 2012
  • This study was carried out for the purpose of obtaining basic data to utilize the AMD sludge as sorbent for heavy metal ions. The sludge from the treatment process of Acid Mine Drainage mainly consists of fine iron hydroxide or iron oxide hydrate and calcite, and the fine iron hydroxide or iron oxide hydrate has a property of adsorbing heavy metal ions. In this study, we investigated the physical property of the AMD sludge like as mineral composition, particle size and shape and chemical composition and also investigated the influence of dosage of sludge, adsorbing time, pH, initial concentration and sintering temperature on the adsorption of heavy metal ions.