• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1998.10a
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• pp.248-253
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• 1998

Recently, the uses of Ceramic/metal bonded joints, resin/metal joints, adhesive joints, composite materials which are composed of dissimiliar materials have increased in various industry fields. Since the ceramic/metal bonded joints material is made at a high temperature, residual stress distributions due to differences in material properties were investigated by varying material parameters. The two dimensional finite element analysis was performed to study residual stress distribution in Si3N4/SM45C bonded joint with a copper interlayer between the silicon nitride(Si3N4) and the structural carbon steel(SM45C) and 4-point bending tests were carried out under room temperature. Fracture surface and crack propagation path were observed using scanning electron microscope and characteristics of its fracture was discussed.

• Proceedings of the Acoustical Society of Korea Conference
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• spring
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• pp.383-386
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• 1999

본 연구에서는 공중용 초음파 센서에 많이 사용되고 있는 원판형 압전소자, 정합층, 그리고 후면충, 세 부분으로 이루어진 다층 접합체의 진동 특성을 기계적 진동 방정식을 이용하여 이론적으로 해석하였으며, 해석결과의 타당성을 유한요소 해석방법을 사용하여 검증하였다. 본 연구의 해석 방법은 다층 판, 특히 압전세라믹과 정합층으로 이루어진 2층과 후면층이 추가된 3층에 대한 진동 방정식에 적절한 경계 조건 및 수렴조건을 적용하여 고유진동 주파수를 유도하였다. 그리고 이를 이용하여 초음파 탐측자 개발 시 널리 사용되고 있는 설계변수 즉, 각 층의 반경, 두께, 밀도, 그리고 영률의 변화에 대한 공진주파수의 변화 경향을 분석하였다. 공진주파수 변화 경향에 대한 이 해석 방법의 타당성을 널리 사용되고 있는 유한 요소해석법을 사용하여 검증한 결과, 두 해석결과는 좋은 일치를 보였다. 그러므로 본 연구의 결과는 종래의 등가회로나 유한요소 해석법에 비해 더 간편하고, 더 정확한 해석결과를 제공할 수 있는 해석도구로써 이용될 수 있을 것이다.

• Journal of Welding and Joining
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• v.23 no.2
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• pp.59-65
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• 2005

A leaky surface acoustic wave (LSAW) velocity was measured using a scanning acoustic microscope on the ceramic/metal interface in order to investigate material properties. The inverse Fourier transform (IFFT) of the V(z) curve contains the reflectance function of a liquid-specimen interface. So, the longitudinal, transverse, and Rayleigh wave velocities for each layer are obtained by the inversion of the V(z) curve at the same time. This paper contains mainly the experimental procedure for measurements of the LSAW velocity, and the results obtained for the velocity variation of individual layer after the thermal shock. It is shown that this method is useful in measuring the material properties under external stress.

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.11a
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• pp.45.2-45.2
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• 2009

무가압 소결과 분말 야금법을 통하여 금속-세라믹 복합체를 제작하였다. 사용된 각각의 분말은 니켈과 알루미나가 사용되었으며 60wt% Ni을 제조하였다. 60wt% Ni은 본 연구의 선행 연구에서 가장 밀도가 적고 최적 분산이 이뤄지지 않는 혼합 비율로써 이러한 결과는 복합체를 접합의 중간층으로 사용 시 크랙이 발생하는 등 물리적 특성 저하로 연결되고 있다. 선행 연구에서는 본 조성의 이러한 원인을 마이크로 크기의 분말 사용으로 인해 분산과 밀도 측면에서의 최적화가 이루어지지 않았기 때문으로 분석하였다. 이러한 문제를 해결하기 위하여 나노 분말을 사용하였으며 나노분말의 크기는 소결 구동력을 극대화시키고 분산을 더욱 촉진시켜 이를 가능하게 할 수 있다. 하지만 나노분말의 특성 중 하나인 Agglomeration의 존재는 이러한 나노 분말의 장점을 상쇄시켜 원하는결론에 도달하는 것을 방해한다. 따라서 본 연구에서는 나노 분말의 Agglomeration을 효율적으로 제어함으로써 제작된 샘플의 최적 분산과 밀도를 향상시키고 그 결과를 SEM, TEM 등을 통하여 확인하였다.

• Journal of the Korean Ceramic Society
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• v.15 no.2
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• pp.89-97
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• 1978

The basic mechanism of adherence in sintered high purity alumina ceramic-to-metal bonding was studied. Emphasis was placed on flux composition, porosity of the fired ceramics, and metallizing mixtures. The study was conducted on 95 and 99.5% alumina, using molydbenum-manganese, molybdenum-manganese-silicon dioxide metallizing compositions. Metallizing was performed in wet hydrogen (dew point, ＋17$^{\circ}C$) at 145$0^{\circ}C$ for 45min. This experiment indicated that adhernece mechanism of ultra high purity alumina ceramic was attributed to formation of $MnAl_2O_$4, and in the case of 95% alumina containing glass, the migration of glass from the interface into the void of the metal coating was the main role to the adhrence. It showed also that greater the bond-strength was resulted as porosity was increased.

• Journal of the Korean Ceramic Society
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• v.29 no.5
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• pp.377-382
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• 1992

For the development of solid oxide fuel cell the joined interface formation between perovskite oxygen electrode and YSZ solid electrolyte is emphasized in the aspect of reducing the undisirable overpotential. The diffusion couple of LaMnO3 and YSZ was prepared by hot pressing at 130$0^{\circ}C$ in the flow of oxygen gas. The high temperature solid state reaction mechanism between LaMnO3 and YSZ is discussed on the basis of the cation composition profile through EDX analysis. The cation components in perovskite compound diffuse considerably into YSZ, while cations of YSZ diffuse little into perovskite.

• Journal of the Korean Ceramic Society
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• v.30 no.5
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• pp.357-364
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• 1993

Chemical reaction occurred in the interface of Mn-Zn ferrite and glass after bonding. Effects of the formation of reaction layer on the magnetic properties were investigated. The composition of glass was 23PbO-61SiO2-6ZnO-8Na2O-2K2O and the ferrite was chosen to have a high permeability. Toroid samples of ferrites bonded with glasses, were heat-treated at $700^{\circ}C$, 80$0^{\circ}C$ and 90$0^{\circ}C$ for 1h. The reaction was observed to increase with bonding temperature, resulting in the development of reaction layer. Subsequently the initial permeability was found to be decreased. The permeabilities decreased by 25% with increasing bonding temperature from $700^{\circ}C$ to 80$0^{\circ}C$. At the bonding temperature of 90$0^{\circ}C$, the permeability was decreased by 45%, compared to that of 80$0^{\circ}C$.

• Journal of Welding and Joining
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• v.10 no.4
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• pp.181-189
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• 1992

The purpose of this investigation is to examine the effects of the strengthening treatments on the mechanical properties of the flame-sprayed titania ceramic coating layer. The strengthening treatments for flame sprayed specimens were carried out in 12 different conditions in vaccum furance. The mechanical properties such as microhardness, thermal shock resistance, adhesive strength and erosion resistance were tested for the sprayed specimens after strengthening treatments. And it was clear that the mechanical properties of coating layer were much improved by the strengthening treatments. The results obtained are summarized as follows; 1. It was shown that the metallurgical bond was formed between substrate and coating layer by the strengthening treatments and that thermal shock resistance and adhesive strength were remarkably raised. 2. Microhardness of coating lay was considerably increased by the strengthening treatments. 3. Erosion resistance and porosity of coating layer were slightly improved by the strengthening treatments.

• Journal of Welding and Joining
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• v.9 no.3
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• pp.18-25
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• 1991

The purpose of this paper was to investigate the effect of deposition configuration on the mechanical properties of the flame sprayed titania ceramic coating. The sprayed deposition configuration was made in different five types with titania ceramic and Ni-base alloy on the mild steel substrate. The composite coating exhibited superior mechanical properties such as hardness, adhesive strength, thermal shock resistance and corrosion resistance, whereas the mixed coating proved to be more resistant to erosion. Especially graded coating, which consist of Ni-base alloy undercost, intermediate grade coat and titania ceramic overcost, showed excellent mechanical properties.

• Journal of the Korean Ceramic Society
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• v.30 no.6
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• pp.469-477
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• 1993

Residual stresses is one of the major factors to degrade the magnetic properties of VCR magnetic heads. Vicker's indentation technique was adapted to estimate the residual stresses Residual stresses and distribution in the glass and ferrite were obtained after bonding ferrite with glass, varing the cooling rate. The compressive and tensile stresses were developed in the interface and gradually decreased with increasing distance from the interface. The stresses were decreased with a cooling rate. The mean values of residual stress in ferrite were 10MN/㎡, 8MN/㎡, 5MN/㎡ with cooling rate 10℃/min, 5℃/min, 1℃/min respectively. When the bonded sample was annealed above the glass transition temperature followed by cooling at 5℃/min cooling rate, the residual stress was reduced to 6MN/㎡.