• Title/Summary/Keyword: 성분

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Gas Chromatographic Performances for Simultaneous Determination of Multi-pesticide Residues and Extraction of Pesticides with Three Partition Solvents (잔류농약 다성분 동시분석을 위한 기체 크로마토그래피 분석성능과 3종 분배용매에 의한 농약추출)

  • Kim, Chan-Sub;Kim, Jin-Bae;Im, Geon-Jae;Park, Hyun-Ju;Lee, Young-Deuk
    • The Korean Journal of Pesticide Science
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    • v.13 no.3
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    • pp.133-147
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    • 2009
  • In order to develop the simultaneous analytical method for pesticide residues which ones in soil are rapidly and inexpensively measured by, many analytical methods for individual pesticide residue and several methods for multi-pesticide residues in agricultural commodities and food were reviewed. Various gas chromatographic conditions and pre-treatment procedures were intensively investigated and modified. And then new optimum procedure was established and its proficiency was validated. The response on detectors of simultaneous determination of 180 pesticides out of pesticides used in Korea was tested. The number of pesticides that their limits of detection (LOD) equal or lower than $0.05\;mg\;kg^{-1}$ were 137 pesticides on ECD, 170 pesticides on NPD and 179 pesticides on ECD/NPD integrated. The retention times of most pesticides ranged appropriately between 10 minutes and 40 minutes in the proposed chromatographic conditions. But about 90 pesticides eluded between 20 minutes and 30 minutes and so they were not resolved enough. In partition with dichloromethane, ethyl acetate/hexane (1:1) and ethyl acetate, number of pesticides whose extraction efficiency ranged from 70% to 120%, were 163, 154 and 147, respectively.

Changes of Volatile Flavor Components on Roasting Conditions in Cassia tora Seeds (결명자 종실의 볶음조건에 따른 향기성분 변화)

  • Kim, Jong-Kuk;Hawer, Woo-Derck;Ha, Jae-Ho;Moon, Kwang-Deok;Chung, Shin-Kyo
    • Korean Journal of Food Science and Technology
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    • v.27 no.5
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    • pp.736-741
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    • 1995
  • This study was conducted to investigated the change of volatile flavor components of Cassia tora seeds during roasting treatments. The flavor components of Cassia tora seeds were analyzed by gas chromatography(GC) and combined gas chromatography-mass spectrometry(GC/MS). Among the flavor compounds collected by simultaneous steam distillation and extraction(SDE) method, 38 components were separated and identified. They consisted of 3 pyrazines, 4 pyrroles or pyridine, 4 alcohols, 11 aldehydes or ketones, 9 furans or phenols and 7 others. The flavor compounds collected from unroasted Cassia tora seeds were 7 components. During roasting process, many other flavor components were formed and increased in their contents. The contents of pyrazines and furans were highest and increased conspicuously, whereas, the contents of aldehydes, ketones, alcohols and pyridines were not increased significantly.

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Extraction of Runoff Component from Stage in Tidal River Using Wavelet Transform (Wavelet Transform을 이용한 감조하천 수위자료의 유출성분 추출)

  • Oh, Chang-Ryeol;Lee, Jin-Won;Jung, Sung-Won;Park, Sung-Chun
    • Journal of Korea Water Resources Association
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    • v.40 no.10
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    • pp.793-800
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    • 2007
  • This research applied to Wavelet transform that have soft resolution time and frequency area for stage of Hadong2 station in order to extract to discharge component by rainfall and tidal level component by tide. Approximation component(A6) of last level for wavelet decomposition displayed the biggest energy value 87.77%, and detail component(D3) energy value was 10.70% with periodicity of semidiurnal tide type(about 12 hours). Also skewness, kurtosis values of D3 have similar to tidal level of Yeosu. Approximation component(A6), Detail component(D6, D5) for Hadong2 stage was runoff component, and detail component(D4, D3, D2) was tide component according to effect of tide.

유청 단백질에서 유도되는 생리활성 펩타이드에 관한 연구

  • Yun, Seung-Seop
    • 한국유가공학회:학술대회논문집
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    • 1996.11a
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    • pp.18-29
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    • 1996
  • 1. CWPC중의 새로운 생리활성물질의 검색 Mouse 임파세포의 증식효과를 지표로 하는 면역기능을 검토하여 CWPC중의 면역 부활작용을 갖는 새로운 성분의 검색을 실시하였다. CWPC를 여러 가지 분획법으로 분획하여 mouse 임파세포의 증식효과를 지표로 면역 활성성분을 검색하였다. 그 결과 gel filtration, 음이온교환법을 사용하여 분획한 당을 다량 포함한 부분에 강한 면역부활담당세포에 대하여 증식활성을 나타내는 물질을 발견하였다. 이 물질은 SDS-PAGE상에서 분자량이 약 16kDa에 위치하여 Ca, P 및 당쇄를 포함한 물질이며, 이것을 GPP로 하였다. GPP에는 우유케이신의 trypsin분해물이며 Ca와 무기인을 풍부하게 포함하는 ${\beta}$-CPP와 유사한 phosphoserin 영역을 갖는 성분과 갖지 않는 성분의 2종류가 존재하며, 각각의 면역 부활활성이 인정되었다. 각 성분의 아미노산 분석, 당 분석의 결과에서 지금까지 보고된 우유중의 면역 담당세포에 대한 증식활성을 갖는 물질과는 상이한 성분인 것으로 밝혀졌다. 더욱이 이 활성물질 (GPP)은 PP cell에서도 동등한 활성이 있는 것으로 판단되었다. 이러한 결과를 종합하여 보면 CWPC중에서 지금까지 알려지지 않았던 새로운 면역 부활물질이 존재하며, 그 성분에는 CPP와 유사한 phophoserine 영역이 존재하는 성분이 포함되어 있고, N-글리코실 결합의 당쇄가 존재하는 것으로 시사되었다. 이 성분은 전신면역의 지표인 비장세포에 대해서만이 아니고, 장관면역계에 중요한 역할을 담당하는 PP cell에서도 활성이 있는 것으로 보아 전신 및 국부적인 면역기능의 부활성분으로서 응용의 가능성이 시사되었다. 2. GPP의 면역담당세포에 대한 증식활성의 메카니즘의 검토 CWPC중의 GPP의 면역담당세포증식활성의 메카니즘을 해명하기 위해 먼저 이 성분중의 어느 부분이 활성에 관여하는지를 pronase 분해 및 phophoserine 영역을 인식하는 항체를 사용하여 검토하였다. 그 결과 pronase 분해처리에서도 활성의 감소를 나타내지 않았으므로 이러한 활성에는 당이 필수 불가결하다는 점이 시사되었다. 또한 phosphoserine 영역을 인식하는 항체에 의해서도 활성은 감소하지 않는 것으로 보아 phosphoserine 영역이 세포증식활성에 관여하지 않는 것으로 판단되었다. 또한 분획한 면역담당세포에 대한 증식활성을 측정하는 것으로 이 성분의 표적면역담당세포를 동정하여, B세포에 대해서만 특이적으로 증식활성을 나타내는 것으로 밝혀졌다.

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3, 4성분계 DSA 전극의 제조와 성능 평가

  • Park, Yeong-Sik;Kim, Dong-Seok
    • Proceedings of the Korean Environmental Sciences Society Conference
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    • 2008.11a
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    • pp.482-487
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    • 2008
  • 성능이 우수한 다성분계 전극을 개발하기 위하여 Ru를 주 전극성분으로 Pt, Sn, Sb 및 Gd를 보조 전극성분으로 하여 3, 4성분계 전극의 성능과 산화제 생성량 및 전극 표면 분석을 행하여 다음의 결과를 얻었다. 1. 2분 동안 단위 W당 제거된 RhB 농토는 Ru:Sn:Sb=9:1:1 > Ru:Pt:Gd=5:5:1 > Ru:Sn=9:1 > Ru:Sn:Gd=9:1:1 > Ru:Sb:Gd=9:1:1로 나타났다. Ru:Sn:Sb=9:1.1 전극에서 발생하는 free Cl, ClO$_2$ 및 H$_2$O$_2$농도가 다른 전극보다 높은 것으로 나타나 산화제 생성경향과 RhB 분해율과는 상관관계가 있는 것으로 사료되었다. 4성분계 전극 중에서 Ru:Sn:Sb:Gd 전극의 성능이 가장 우수한 것으로 나타났으나 3성분계 전극인 Ru:Sn:Sb=9:1.1 전극보다 성능이 떨어지는 것으로 나타났다. Ru:Sn:Sb=9:1:1 전극에서 생성되는 산화제 농도가 다른 두 종류의 산화제 농도보다 높은 것으로 나타났고 4성분 전극의 경우 Ru:Sn:Sb:Gd 전극의 산화제 농도가 Ru:Sn:Sb:Gd 전극이 높거나 유사한 경우로 나타나 산화제 생성 경향과 RhB분해 능과는 상관관계가 있는 것으로 나타났다. 초기 RhB 분해 속도가 높은 전극의 COD 제거율도 높은 것으로 나타났다. OH 라디칼은 발생하지 않지만 염소계 산화제 농도가 높고 RhB제거율이 높아 Ru를 주 성분으로 한 전극의 RhB분해는 주로 간접 산화작용에 의한 것이며, 개발된 3, 4성분계 산화물 전극은 간접 산화용 전극임을 알 수 있었다. 에칭을 하기 전의 Ti판은 표면이 매끄러운 것으로 나타났으며, 35% 염산으로 에칭한 후의 Ti메쉬는 매우 거친 표면조직을 가지는 것을 관찰할 수 있었다. Ru:Sn:Sb=9:1:1 전극과 Ru:Sn:Sb:Gd 전극의 SEM 사진을 관찰한 결과 두 전극 모두 전극 물질이 균일하게 도포되어 있었으며, 두 전극 모두 열소성을 통해 전극 성분을 코팅할 때 발생하는 "mud crack"이 발생한 것이 관찰되었다 EDX 분석에서 Cl이 관찰되었는데, 전극 성분의 불완전 산화로 인한 비양론적 산화물 때문이며 이는 RhB 분해성능과 관련 있는 것으로 사료되었다.

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An Automatic Cosmetic Ingredient Analysis System based on Text Recognition Techniques (텍스트 인식 기법에 기반한 화장품 성분 자동 분석 시스템)

  • Ye-Won Kim;Sun-Mi Hong;Seong-Yong Ohm
    • The Journal of the Convergence on Culture Technology
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    • v.9 no.1
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    • pp.565-570
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    • 2023
  • There are people who are sensitive to cosmetic ingredients, such as pregnant women and skin disease patients. There are also people who experience side effects from cosmetics. To avoid this, it is cumbersome to search for harmful ingredients in cosmetics one by one when shopping. In addition, knowing and remembering functional ingredients that suit you is helpful when purchasing new cosmetics. There is a need for a system that allows you to immediately know the cosmetics ingredients in the field through photography. In this paper, we introduce an application for smartphones, <Hwa Ahn>, which allows you to immediately know the cosmetics ingredients by photographing the ingredients displayed in the cosmetics. This system is more effective and convenient than the existing system in that it automatically recognizes and automatically classifies the ingredients of the cosmetic when the camera is illuminated on the cosmetic ingredients or retrieves the photos of the cosmetic ingredients from the album. If the system is widely used, it is expected that it will prevent skin diseases caused by cosmetics in daily life and reduce purchases of cosmetics that are not suitable for you.

Analysis of the Volatile Organic Compounds of Persimmon Flower according to Tree Age and Floral Organ (감나무 수령과 감꽃 기관에 따른 휘발성 향기성분 분석)

  • Kim, Ji Hye;Hong, Sae Jin;Shin, Il Sheob;Eum, Hyang Lan
    • Journal of Bio-Environment Control
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    • v.23 no.4
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    • pp.321-328
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    • 2014
  • This study was conducted to investigate volatile organic compounds (VOCs) of persimmon (Diospyros kaki Thunb) flower. VOCs of persimmon flower was collected via SPE (solid phase micro extraction) and determined by GC-MS according to tree age and organs such as flower and calyx. The ratio of early bloom was higher in more than 15 year old tree than other trees showing tree age was related with flowering rate. Major VOCs of persimmon flower was a-pinene, butane, caryophyllene, cubebene, lavandulol, D-limoneneylangene, ylangene, mainly included green, fruit, and floral flavors. The number of VOCs in persimmon flower was 30 compounds in 5-9 years old tree, 24 compounds in 10-14 years old tree, and 32 compounds in more than 15 years old tree. In comparison with VOCs in organs of sweet persimmon 'Fuyu' cultivar, flower has 10 compounds of VOCs and 26.35% of relative peak area, while calyx has 14 compounds and 46.28%, respectively. In astringent persimmon, flower has 6 compounds of VOCs and 17.58% of relative peak area, while calyx has 9 compounds and 50.27%, showing calyx of both cultivars has various volatile compounds. This study will contribute to provide a basic data for the fragrance industry to use the flavor of persimmon flower.

Investigation of Importance of Evanescent Modes in Predicting the Transformation of Water Waves by the Linear Wave Theory: 1. Derivation of Equations of Wave Energy (선형파 이론에 의한 파랑변형 예측 시 소멸파 성분의 중요성 검토: 1. 에너지 식 유도)

  • 이창훈;조용식
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.14 no.4
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    • pp.282-285
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    • 2002
  • The magnitude of evanescent modes in terms of dynamics is investigated in case that the transformation of water waves is predicted using the linear wave theory. In other words, derivation is made of both the kinetic and potential wave energies of evanescent modes as welt as propagating modes. The evanescent modes consist of compound components of propagating and evanescent modes, those of identically equal evanescent modes, and those of identically different evanescent modes. The wave energy per a horizontal distance decreases exponentially with the distance.

Variation of the Electrical Resistivity with ion Components of Pore Water in the Sand (사질토 간극수의 이온 성분들에 따른 전기비저항값의 변화)

  • Yu, Chan;Yoon, Chun-Gyeong;Lee, Young-Nam;Lee, Yong-Gil
    • Journal of the Korean Geotechnical Society
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    • v.15 no.1
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    • pp.185-196
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    • 1999
  • A laboratory experiment was performed to examine the relationship between resistivity and ionic components in the pore water of a sand by using soil resistivity test box and STING-Rl. The resistivity measurement was performed with the concentration changes of ionic components. Also, the resistivity change was evaluated for multiple components. The results showed that the resistivity of Arsenic was less than other heavy metals. In the case of complex components, resistivity ranges depended on the resistivity of components existed in the pore water.

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Adaptive Retinex Algorithm using Skewness for Contrast Enhancement (대조비 개선을 위한 비대칭도 특성을 이용한 적응적인 레티넥스 방식)

  • Oh, Jong Geun;Hong, Min-cheol
    • Journal of the Institute of Electronics and Information Engineers
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    • v.53 no.10
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    • pp.77-83
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    • 2016
  • This paper presents an adaptive retinex algorithm using skewness for contrast enhancement of color images. In order to estimate the degree of low contrast of an image, skewness of luminance of an observed image is used to define a parameter, and a non-linear function is proposed to compensate the reflectance using the parameter and estimated reflectance. In addition, determination of gain and offset of the non-linear function is addressed using statistics of the estimated reflectance. The relation between an observed luminance and the compensated luminance is used to compensate color components with the reduction of computational cost. The experimental results show that the proposed algorithm has the capability to effectively improve the contrast without color distortion.