• Title/Summary/Keyword: 비파괴측정

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Swelling and Mechanical Property Change of Shale and Sandstone in Supercritical CO2 (초임계 CO2에 의한 셰일 및 사암의 물성변화 및 스웰링에 관한 연구)

  • Choi, Chae-Soon;Song, Jae-Joon
    • Tunnel and Underground Space
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    • v.22 no.4
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    • pp.266-275
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    • 2012
  • In this study, a method is devised to implement a supercritical $CO_2$ ($scCO_2$) injection environment on a laboratory scale and to investigate the effects of $scCO_2$ on the properties of rock specimens. Specimens of shale and sandstone normally constituting the cap rock and reservoir rock, respectively, were kept in a laboratory reactor chamber with $scCO_2$ for two weeks. From this stage, a chemical reaction between rock surface and the $scCO_2$ was induced. The effect of saline water was also investigated by comparing three conditions ($scCO_2$-rock, $scCO_2-H_2O$-rock and $scCO_2$-brine(1M)-rock). Finally, we checked the changes in the properties before and after the reaction by destructive and nondestructive testing procedures. The swelling of shale was a main concern in this case. The experimental results suggested that $scCO_2$ has a greater effect on the swelling of the shale than pure water and brine. It was also observed that the largest swelling displacement of shale occurred after a reaction with the $H_2O-scCO_2$ solution. The results of a series of the destructive and nondestructive tests indicate that although each of the property changes of the rock differed depending on the reaction conditions, the $H_2O-scCO_2$ solution had the greatest effect. In this study, shale was highly sensitive to the reaction conditions. These results provide fundamental information pertaining to the stability of $CO_2$ storage sites due to physical and chemical reactions between the rocks in these sites and $scCO_2$.

Analysis of the Manufacturing Techniques for the KwangDahoe Tying on the Sword in Joseon Dynasty (조선시대 도검 패용 광다회의 제작기법 분석)

  • Baek, Je-Sun;Chung, Kwang-Young
    • Korean Journal of Heritage: History & Science
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    • v.50 no.3
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    • pp.64-87
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    • 2017
  • Dahoe is a traditional braid in Joseon Dynasty. There are many Dahoe artifacts, which can give us a glimpse of the costume, culture, and life of that era. The study of Dahoe is necessary in various fields, but it is difficult because this manufacturing technique has been passed down from hand to hand. Few studies have been done so far. This research examines the manufacturing technique of KwangDahoe which is passed down by Maedeupjang (Decorative Knotting) and is generally used for knotting and/or tying objects. The main characteristic of TieKwangDahoe, made through the same method as WonDahoe, is the square hole in the middle. It was impossibile to remake the original braid because there is no confirmed number of the strand. Especially it is very difficult to do conservation and restoration on serious degradation state of the fiber. Therefore, it is necessary to analyze the non-destructive manufacturing techniques method for Dahoe and assess their applicability. First, we analyzed the artifacts' manufacturing technique based on the database of the Dahoe's manufacturing technique. In order to do that, we undertook schematization, restoration, morphological analyzation of the Dahoe. And then, X-ray CT scans were performed to improve the reliability of the DB. These results of scanning were interpreted based on the manufacturing technique. The selected Tie-KwangDahoe on the sword for the study are artifacts including artistic value and symbolism in Joseon Dynasty. Based on the analysis of the manufacturing technique, we found that both artifacts were made of 20-strand braid of single cross according to the length-scale measure. It was manufactured using 8-strand on left-right side, 12-strand on front-back side by the braiding manufacturing technique method Finally, this research suggests non-destructive analysis method of Dahoe's manufacturing technique is based on the database and the analysis results. I hope this research can be useful in various professional fields of Dahoe in the future. Moreover, I hope this can be of any help in preserving Korean cultural heritage.

Analysis of Magnetic Multi-layers by RBS and PIXE (후방산란법(RBS)/양성자 여기 X-선 방출법(PIXE)을 이용한 다층자성박막의 두께 및 조성 정량분석)

  • 송종한;김태곤;전기영;황정남;신윤하;김영만;장성호;김광윤
    • Journal of the Korean Magnetics Society
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    • v.11 no.6
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    • pp.272-277
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    • 2001
  • A spin valve structure of Ta/NiFe/CoFe/Cu/CoFe/Ru/CoFe/FeMn/Ta which has a synthetic antiferromagnet (CoFe/Ru/CoFe), was fabricated by using a magnetron sputtering system. The thickness and composition of magnetic free and pinned layers affect the magnetic properties such as exchange interaction strength of each layer and so on. Even though Rutherford Backscattering Spectrometry (RBS) has advantages of quantitative and non-destructive analysis, it is almost impossible to determine the thickness and composition of magnetic thin films using lBS because of its poor mass resolution for a higher atom number (Z>20). In this study, quantitative analysis of the element composition and thickness for the spin valve sample was performed by combining both Proton Induced X-ray Emission Spectrometry (PIXE), which is one of element specific analysis techniques, and grazing-exit RBS with a highly improved depth resolution and absolute quantitative analysis. For the quantitative analysis, standardization of PIXE was carried out with NiFe, CoFe, and FeMn layers, which are one of constituent layers of spin valve films. Through PIXE standardization and the aid of PHE experimental results of the spin valve sample, ire overlapped signal in a grazing-exit RBS spectrum were successfully resolved and the thickness of the Ru layer was determined with a resolution of ∼1 .

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Study on Characteristics of Controlled Low Strength Material Using Time Domain Reflectometry (시간영역반사법을 이용한 유동성 채움재의 특성 연구)

  • Han, Woojin;Lee, Jong-Sub;Byun, Yong-Hoon;Cho, Samdeok;Kim, Juhyong
    • Journal of the Korean GEO-environmental Society
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    • v.17 no.4
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    • pp.33-37
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    • 2016
  • The hydration process of Controlled Low Strength Material (CLSM) used for backfill is the primary factor to determine the construction period. The objective of this study is to monitor the hydration process of CLSM using the Time Domain Reflectometry (TDR) and to establish the relationship between dielectric constant and compressive strength. The CLSM specimen is composed of cement, flyash, silt, sand, accelerator, and water. The material characteristics of the CLSM including flow, unit weight, compressive strength are investigated. To measure the dielectric constant of the CLSM during the curing time, TDR probe incorporated with a mold and a reflectometer are used. Experimental results show that the dielectric constant remains constant at early stage, and then decreases as the curing time increases. In addition, the dielectric constant is related to the compressive strength in inverse power function. This paper suggests that the TDR technique may be used as a non-destructive testing method in order to estimate the compressive strength of the CLSM mixture under construction.

Neutron Activation Analysis of Human Hair for Human Health Assessment (인체보건 환경평가를 위한 모발의 중성자방사화분석)

  • Chung, Young-Sam;Kang, Sang-Hoon;Moon, Jong-Hwa;Kang, Young Hwan;Cho, Seung-Yon
    • Analytical Science and Technology
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    • v.14 no.2
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    • pp.131-139
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    • 2001
  • There is personal difference in the concentrations of trace elements in human hair according to human life or history suck as occupation, race, sex, age, food habit, social condition and so on. It is also found that the individual's deviation of elemental concentrations is reflecting the degree of environmental pollutants exposure to human body, intakes of food and metabolism. To compare the degree of accumulation in the hair tissue, human hair samples were collected from five positions of head and analyzed by non-destructive neutron activation analysis with and without washing according to IAEA's recommended method. Analytical quality control is performed using the certified reference material. The relative error of Cu, Cr, Na, Co, Mg, As, Se, Zn and those of Mn, Ca, Fe, Sr are within ${\pm}5%$ and ${\pm}10%$, respectively and the relative standard deviation of elements are within ${\pm}10%$. The deviations between the individuals and hair sampling positions were estimated. The deviation of individual was seven times more than that of positions. Under the defined condition, the difference and the correlation of elemental concentrations were compared with two different groups, office and factory workers. The result can be used as a fundamental data for human health and environment assessment.

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Estimation of Moisture Content in Watermelon Seedlings Using Htperspectral Imagery (초분광 영상을 이용한 수박 묘의 수분함량 추정)

  • Jun, Sae-Rom;Ryu, Chan-Seok;Kang, Jeong-Gyun;Kang, Ye-Seong;Kim, Seong-Heon;Kim, Won-Jun;Sarkar, Tapash Kumar;Kang, Dong-Hyeon
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2017.04a
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    • pp.41-41
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    • 2017
  • 본 연구는 초분광 영상을 이용하여 수박 모종의 수분함량을 비파괴적으로 추정하기 위해 수행되었다. 단계적으로 수분 스트레스를 받은 수박(n=45) 모종을 초분광 영상시스템으로 촬영하여 모종 영역의 반사율을 추출하였고, 매 촬영 후 모종의 생체중과 건물중을 측정하여 수분함량을 계산하였다. 모종의 반사율과 계측된 수분함량을 변수로 하여 Partial Least Square Regression(PLSR) 분석을 이용하여 수분 추정 모델을 구축하였다. 수분 추정모델을 작성한 결과 Calibration(Cal.)의 정확도($R^2$)는 0.66, 정밀도(RMSE 및 RE)는 각각 1.06%, 1.14%로 나타났다. 수박 모종의 수분함량 추정모델의 정밀도는 상당히 높게 나타났으나 정확도는 낮게 나타났다. 정확도를 개선하기 위해 Confidence ellipses의 신뢰구간을 95%로 설정하였을 때 3개의 모종이 타원 밖에 위치하는 것을 발견하였으며 이를 제거 후 재분석을 하였다. 3개의 모종을 제외한 수박 모종의 수분함량 추정모델의 정확도는 0.82, 정밀도는 0.73%, 0.78%로 나타났다. 3개의 모종을 제외함으로서 모델의 정확도 및 정밀도가 상승하여 3개의 모종이 정확도 및 정밀도를 낮추는 원인이라 판단된다. 작물은 가뭄스트레스를 받을수록 반사율이 낮아지지만(Yang et al., 2010) 3개의 모종은 다른 모종의 수분함량에 비해 반사율이 큰 차이를 나타내어 정확도 및 정밀도를 낮춘 것으로 판단된다. 본 연구를 통해 초분광 영상을 이용하여 수박 모종의 수분함량 추정가능성을 시사하였고, 모델의 정확도를 개선하기 위해 샘플 수 및 수분함량의 변이를 증가시키는 것이 필요하다고 판단된다.

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Effect of Liposome-coated Hemicellulase on the Tenderization of Burdock (리포좀 코팅한 hemicellulase가 우엉의 연화에 미치는 효과)

  • Kim, Kwang-Il;Lee, SangYoon;Lee, Jiseon;Lee, JungGyu;Min, Sang-Gi;Choi, Mi-Jung
    • Korean Journal of Food Science and Technology
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    • v.47 no.6
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    • pp.698-703
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    • 2015
  • The elderly or patients with masticatory disturbance and deglutition dysfunctions, may have difficulty in chewing or biting foods with a hard texture. Thus, softening of the texture of foods using hemicellulase immobilized by the nanoencapsulation technique was examined in this study. Burdock was cut into cylindrical-shaped samples, which were immersed in distilled water and non-coated or coated enzymes for 48 h at $4^{\circ}C$. The hardness of the treated samples decreased compared to the control. Microstructural observations revealed that the cells in the non-coated burdock were destroyed after 24 h. From the point of view of enzyme activity, the initial activity of the non-coated enzymes was higher than that of the coated enzymes. However, the enzyme activity was not significantly affected by the immersion time. Therefore, it appears that the encapsulation technique for enzymes may be useful for softening the texture of foods.

Geotomography Applied for the Integrity Test of Cast-in-place Piles (현장타설콘크리트말뚝의 건전도 평가를 위한 geotomography의 적용 연구)

  • Lee Jae-Kyung;Park Jong-Nam
    • Journal of the Korean Geotechnical Society
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    • v.21 no.4
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    • pp.5-12
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    • 2005
  • Recently, geophysical prospecting methods have played very important roles in civil and environmental engineering problems. Technical advances in geophysical instruments and computer system made it possible to get underground images with very high resolution far purposes to resolve those problems. It was possible partly due to ever increasing demand for development of technologies needed to precisely detect polluted areas and prevent ground-related accidents. Based on the same demand, integrity tests of cast-in place piles draw more attention and development of accurate test procedures is required. Ultrasonic methods is one of most advanced non-destructive procedures. In the paper, a geotomography method is employed for the cast-in place pile integrity test using ultrasonic waves. The image of pile interior is scanned and scrutinized far better and more accurate decision in the cast-in place pile integrity. In this study, we firstly examined the accuracy fur tomography program with idealized synthetic models built in water tank: their position and size were changed in the tank and each case was studied. In the next stage, real concrete pile models were fabricated and images of anomaly areas inside the pile were scanned to successfully locate those areas.

Development of Post-installable Pullout Bolts and a Loading Device for Evaluating Concrete Strength (콘크리트 강도평가를 위한 인발장치와 후매입 인발볼트의 개발)

  • Ko, Hune-Bum;Lee, Ghang;Won, Jong-Sung
    • Journal of the Korea Institute of Building Construction
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    • v.11 no.3
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    • pp.229-237
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    • 2011
  • The pullout test is a nondestructive testing method certified by the American Society for Testing and Materials (ASTM) and British Standards (BS). Research has shown that it is very reliable in terms of evaluating the concrete strength of reinforced concrete members. However, the pullout test is rarely performed on domestic construction sites due to the complex procedures and high costs involved. This study proposes a new pullout test composed of a post installable break-off bolt, an insert nut, and a pullout tester, which satisfy both economical and practical purposes on a construction site. Three different types of special fastening methods, a temporary fixed bolt, a plastic fixed panel, and a fixed bar, have been developed. A pullout tester is proposed that is driven by the circle force introduced into a handle composed of eight gears without a load cell and a hydraulic cylinder. The serviceability and reliability of these instruments were investigated through experiments at construction sites. Furthermore, the sample pullout test with a wall specimen was conducted to estimate the usefulness of the temporary fixed bolt type of fastening methods and pullout devices. Eventually, the developed instruments will be useful on construction sites if minor requirements are met.

Evaluation Techniques for Residual Structural Performance of a Reinforced Concrete slab under Fire Damage (화재 피해를 입은 철근콘크리트 슬래브의 잔존 구조성능 평가기법)

  • Choi, Kwang-Ho
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.2
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    • pp.588-594
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    • 2020
  • This study proposes non-destructive rebound-hardness and ultrasonic testing methods to more accurately evaluate the residual structural performance of reinforced concrete structures in a fire. Techniques are also proposed to assess the stiffness used in the deflection calculation with natural frequencies obtained by vibration tests. In the compressive strength evaluation using rebound hardness, the residual compressive strength of thick specimens and a larger water/cement (W/C) ratio were shown to be large. The homogeneity of concrete at high temperature compared to ambient temperature conditions was assessed by the velocity of ultrasonic waves that penetrate the concrete, and it followed W/C or thickness of slab makes little different results. To assess the stiffness of fire-damaged slabs and increase in deflection, the natural frequency was measured by vibration tests and incorporated into the equation of the stiffness. The application of this technique to the slab experiment showed that it can be a very reasonable evaluation technique. In addition, to evaluate the residual strength of a member after fire, a test of the strength of a component was carried out during and after heating.