• Title/Summary/Keyword: 비파괴조사

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Quantitative Analysis of Acid Value, Iodine Value and Fatty Acids Content in Sesame Oils by NIRS (근적외선분광광도법을 이용한 참기름의 산가, 요오드가, 지방산정량법에 관한 연구)

  • Kim, Jae-Kwan;Lee, Myung-Jin;Kim, Myung-Gill;Kim, Kyung-A;Park, Eun-Mi;Kim, Young-Sug;Ko, Hoan-Uck;Son, Jin-Seok
    • Journal of Food Hygiene and Safety
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    • v.21 no.4
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    • pp.204-212
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    • 2006
  • This study was conducted to investigate the possibility of rapid and non-des tructive evalution of AV (Acid Value), IV (Iodine Value) and fatty acids in sesame oils. The samples were scanned over the range $400\sim2500nm$ using transmittance spectrum of NIRS(Near-infrared spectroscopy). A calibration equation calculated by MPLS regression technique was developed and correlation coefficient of determination for AV, IV, palmitic acid, stearic acid, linoleic acid and linolenic acid content were 0.9907, 0.9677, 0.9527, 0.9210, 0.9829, 0.9736 and 0.9709 respectively. The validation model for measuring the AV content had R of 0.989, SEP of 0.058 and IV content had R of 0.944, SEP of 0.562 and palmitic acid content had R of 0.924, SEP of 0.194 and stearic acid content had R of 0.717, SEP of 0.168 and oleic acid content had R of 0.989, SEP of 0.221 and linoleic acid content had R of 0.967, SEP of 0.297 and linolenic acid content had R of 0.853, SEP of 0.480 by MPLS. The obtained results indicate that the NIRS procedure can potentially be used as a non-destructive analysis method for the purpose of rapid and simple measurement of AV, IV and fatty acids in sesame oils.

The Structural Safety Diagnosis of Three-Story Pagoda in Bulkuk Temple Using the Probability of Failure. (암석의 파괴 확률 분석을 통한 불국사 삼층석탑 구조 안전 진단)

  • Seo, Man-Cheol;Song, In-Seon;Choe, Hui-Su
    • Journal of the Korean Geophysical Society
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    • v.4 no.1
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    • pp.57-69
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    • 2001
  • We have carried out a nondestructive close examination for the purpose of the structural safety diagnosis of the Three-Story Pagoda(Seokga Pagoda) in Bulkuk temple in the city of Kyungju, Kyungbuk, Korea. Ultrasonic wave velocities were measured at 456 points of the pagoda comprising 44 blocks to estimate the mechanical properties of rock blocks constituting the pagoda. The measured velocities have the range of 1217 to 4403 m/sec with the average of 3227 m/sec. The empirical relationship between the ultrasonic velocity and the uniaxial compressive strength yielded the estimation of strength of each block, ranging from 134 to 844 kg/cm^2 and averaging 463 kg/cm^2. With an assumption that the strength of each block is described as a random variables having a normal distribution, we calculated the probability of failure of rock blocks of the pagoda. Our investigation revealed that the probability of the structural failure due to the weight of higher blocks is very low. However, the probability of partial failure around contact area is substantial, which is consistent with the appearance that edges and the corners of some blocks were broken off. The platform under the body of the pagoda appeared to be structurally weak as the probability of tensile failure of the lower platform is up to 18%, and diagonal fractures are shown where the probability of failure is high.

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Material Characteristics and Nondestructive Deterioration Assessment for the Celestial Chart Stone, Korea (천상열차분야지도 각석의 재질특성과 비파괴 훼손도 평가)

  • Yoo, Ji Hyun;Lee, Myeong Seong;Choie, Myoungju;Ahn, Yu Bin;Kim, Yuri
    • The Journal of the Petrological Society of Korea
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    • v.27 no.4
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    • pp.207-222
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    • 2018
  • Celestial Chart Stones (original and reproduction) in the National Palace Museum are representative scientific cultural heritage of Korea. Material analysis and nondestructive deterioration assessment were conducted for long-term preservation of these stones. Material analysis revealed that the original was composed of slate and the reproduction was made of dolostone. The original consists of quartz, mica, dolomite minerals, while the reproduction was made up of dolomite, calcite and forsterite. Major deterioration factors of the original stone were cracks and breakouts. In case of the reproduction, scratches and artificial materials were mainly observed. The green and black surface contaminants present at the sides and back of the two celestial chart stones were interpreted as resin-based paint materials. The physical property evaluation using ultrasonic velocity showed a low velocity in the upper left side of the original, while the front right side of the reproduction showed a weak property. Meanwhile, the To-Tc method using ultrasonic velocity was applied to major cracks that impede stability of the original. As a result, it has been calculated that the beginning and the center of the crack are the deepest.

Conservation Treatment and Material Analysis of Amber Relics Found in the Huryeongtong of Geumsansa Temple (금산사 후령통(候鈴筒) 내 발견 호박유물의 과학적 분석과 보존처리)

  • Ham, Chul-hee;Kang, So-yeong
    • Korean Journal of Heritage: History & Science
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    • v.46 no.4
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    • pp.78-89
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    • 2013
  • For safe conservation treatment of damaged accessory relics that were unearthed, the quality of the material should be accurately identified through a nondestructive analysis and failure analysis. This study provides the basic conservational scientific data regarding material analyses and conservation treatment that were conducted for 11 relics, including amber and agate that were discovered during the repair of Geumsansa Temple's Hall of Maitreya Buddha and Left Attendant Buddhas in June 2008. An ultraviolet analysis, SEM-EDS analysis and FT-IR microscope analysis revealed that the physical and chemical characteristics of the 11 relics are the same as those of amber. It is inferred that the cracks and exfoliation of the surface of most amber relics is attributable to darkening of the color due to C=C bond oxidation. It is also assumed that cracks and exfoliation occurred from the weathered layer on the amber surface. As such, it is appropriate to engage in conservation treatment of the damaged amber relics by using $Paraloid^{(R)}$ B67 reinforcing agent that is diluted in nonpolar solvent. The greatest care is needed for future handling of organic artifacts.

Study on the Baekje's Cotton Fabrics Excavated in Neungsan-ri Temple Site (부여 능산리 사지 출토 백제 면직물연구)

  • Sim, Yeon Ok;Chung, Yong Jae;Yu, Ji A;Namgung, Seung
    • Korean Journal of Heritage: History & Science
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    • v.44 no.3
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    • pp.4-17
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    • 2011
  • The Baekje's cotton fabrics were excavated from 'Neungsan-ri temple site in Buyeo' (September 1999-April 2000) and stored at Buyeo National Museum after conservation treatment. In this study, it carred out non-destructive, chemical and morphological analysis for fiber identification, also considered on influx, features and difference between the 'Baek-cheop-po(Three kingdom period's cotton fiber)' and 'Mok-myeon(imported by Munikjeom, late Korea dynasty)'. As a result, the fiber proved cellulose fiber through analytical researches like color reaction, FT-IR(chemical analysis). It was also confirmed lumens, typical dimensional structure(morphological analysis) as an features of cotton fiber. The fiber was the first evidence in ancient Korea's cotton. But it can not prove that whether weaving were made in Baekje's area. However there were documentation that people in Beakje make cloth to silk fabric from 'Mahan period'. We can suppose that they have had an old weaving techniques. This study has a great historical, academic values as the only evidence for the hypothesis of a weaving technique of the Baekje's cotton. Through comparison to each region's ancient cottons, we can investigate the species of Baekje's cotton and ancient Korea cotton's influx.

Estimation of the Terminal Velocity of the Worst-Case Fragment in an Underwater Torpedo Explosion Using an MM-ALE Finite Element Simulation (MM-ALE 유한요소 시뮬레이션을 이용한 수중 어뢰폭발에서의 최악파편의 종단속도 추정)

  • Choi, Byung-Hee;Ryu, Chang-Ha
    • Explosives and Blasting
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    • v.37 no.3
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    • pp.13-24
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    • 2019
  • This paper was prepared to investigate the behavior of fragments in underwater torpedo explosion beneath a frigate or surface ship by using an explicit finite element analysis. In this study, a fluid-structure interaction (FSI) methodology, called the multi-material arbitrary Lagrangian-Eulerian (MM-ALE) approach in LS-DYNA, was employed to obtain the responses of the torpedo fragments and frigate hull to the explosion. The Euler models for the analysis were comprised of air, water, and explosive, while the Lagrange models consisted of the fragment and the hull. The focus of this modeling was to examine whether a worst-case fragment could penetrate the frigate hull located close (4.5 m) to the exploding torpedo. The simulation was performed in two separate steps. At first, with the assumption that the expanding skin of the torpedo had been torn apart by consuming 30% of the explosive energy, the initial velocity of the worst-case fragment was sought based on a well-known experimental result concerning the fragment velocity in underwater bomb explosion. Then, the terminal velocity of the worst-case fragment that is expected to occur before the fragment hit the frigate hull was sought in the second step. Under the given conditions, the possible initial velocities of the worst-case fragment were found to be very fast (400 and 1000 m/s). But, the velocity difference between the fragment and the hull was merely 4 m/s at the instant of collision. This result was likely to be due to both the tremendous drag force exerted by the water and the non-failure condition given to the frigate hull. Anyway, at least under the given conditions, it is thought that the worst-case fragment seldom penetrate the frigate hull because there is no significant velocity difference between them.

Analysis of Carbonization Behavior of Hydrochar Produced by Hydrothermal Carbonization of Lignin and Development of a Prediction Model for Carbonization Degree Using Near-Infrared Spectroscopy (열수 탄화 공정을 거친 리그닌 하이드로차(hydrochar)의 탄화 거동 분석과 근적외선 분광법을 이용한 예측 모델 개발)

  • HWANG, Un Taek;BAE, Junsoo;LEE, Taekyeong;HWANG, Sung-Yun;KIM, Jong-Chan;PARK, Jinseok;CHOI, In-Gyu;KWAK, Hyo Won;HWANG, Sung-Wook;YEO, Hwanmyeong
    • Journal of the Korean Wood Science and Technology
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    • v.49 no.3
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    • pp.213-225
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    • 2021
  • In this paper, we investigated the carbonization characteristics of lignin hydrochar prepared by hydrothermal carbonization and established a model for predicting the carbonization degree using near-infrared spectroscopy and partial least squares regression. The carbon content of the hydrothermally carbonized lignin at the temperature of 200 ℃ was higher by approximately 3 wt% than that of the untreated sample, and the carbon content tended to gradually increase as the heating time increased. Hydrothermal carbonization made lignin more carbon-intensive and more homogeneous by eliminating the microparticles. The discriminant and predictive models using near-infrared spectroscopy and partial least squares regression approppriately determined whether hydrothermal carbonization has been applied and predicted the carbon content of hydrothermal carbonized lignin with high accuracy. In this study, we confirmed that we can quickly and nondestructively predict the carbonization characteristics of lignin hydrochar manufactured by hydrothermal carbonization using a partial least squares regression model combined with near-infrared spectroscopy.

Characteristics of defect on segmental lining of TBM tunnel in operational subway (운용중인 국내 지하철 TBM터널의 세그먼트라이닝 결함특성 분석)

  • Choo, Jinho;Lee, DongHun;Noh, EunChul
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.24 no.1
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    • pp.109-128
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    • 2022
  • The precise inspection for safety and diagnosis (PISD) of tunnel has been conducted by the special act on safety control of public structures. However, the present assessment for the segmental lining of TBM tunnel has limitation such as: NDTs for integrity, segmental configuration for field inspection, and consideration for jacking system. Even if the number of TBM tunnel is less than 1% of enrolled facility in FMS, more attention to maintenance should be necessary due to its usage such as multi-use facility and national important facility. Compared to NATM tunnel, excavated by drilling and blasting and then installed lining by cast-in-place within 6~12 m, TBM tunnel is cut out ground by disk and cutter-bit and then assembled 7 pieces of precast segment, 1.2~1.4 m wide. Different features of design, construction, and maintenance should be considered to be more exact evaluation of TBM tunnel. The characteristics of defect is categorized and analyzed with 11 operational TBM tunnels in domestic subway. To be more comprehend various particular defects, foreign studies have been also adapted. Crack and leakage are categorized in 7 patterns. Breakage/spalling and corrosion are also grouped into 3 patterns. Patterned defects or damages are fed back in design, construction, and are useful guidelines for maintenance stage in future.

Defect Inspection and Physical-parameter Measurement for Silicon Carbide Large-aperture Optical Satellite Telescope Mirrors Made by the Liquid-silicon Infiltration Method (액상 실리콘 침투법으로 제작된 대구경 위성 망원경용 SiC 반사경의 결함 검사와 물성 계수 측정)

  • Bae, Jong In;Kim, Jeong Won;Lee, Haeng Bok;Kim, Myung-Whun
    • Korean Journal of Optics and Photonics
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    • v.33 no.5
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    • pp.218-229
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    • 2022
  • We have investigated reliable inspection methods for finding the defects generated during the manufacturing process of lightweight, large-aperture satellite telescope mirrors using silicon carbide, and we have measured the basic physical properties of the mirrors. We applied the advanced ceramic material (ACM) method, a combined method using liquid-silicon penetration sintering and chemical vapor deposition for the carbon molded body, to manufacture four SiC mirrors of different sizes and shapes. We have provided the defect standards for the reflectors systematically by classifying the defects according to the size and shape of the mirrors, and have suggested effective nondestructive methods for mirror surface inspection and internal defect detection. In addition, we have analyzed the measurements of 14 physical parameters (including density, modulus of elasticity, specific heat, and heat-transfer coefficient) that are required to design the mirrors and to predict the mechanical and thermal stability of the final products. In particular, we have studied the detailed measurement methods and results for the elastic modulus, thermal expansion coefficient, and flexural strength to improve the reliability of mechanical property tests.

A Study on Manufacturing Techniques and Conservation Treatment for Yongjam, Ceremonial Hairpin with a Dragon-shaped Engraving in 17th Century - Focusing on Yongjam of the Clothes Worn by Oejae Yi Dan-ha and His wife, National Folklore Cultural Heritage No.4 - (17세기 대례용 용잠의 제작기법 조사와 보존처리 - 국가민속문화재 제4호 외재 이단하 내외옷 용잠을 중심으로 -)

  • Ryu, Dongwan;An, Boyeon;Lee, Ryangmi;Lee, Jaesung;Park, Yeonghwan;You, Harim
    • Journal of Conservation Science
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    • v.37 no.3
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    • pp.270-281
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    • 2021
  • The Yongjam of Oejae, Yi Dan-ha's wife, is an ornamental hairpin with a dragon-shaped engraving; designated as National Folklore Cultural Heritage No. 4. It is also a component of the ceremonial costume, and an artifact of great value as it clearly identifies the position of the wearer and the period of this artifact. The Yongjam has been well preserved in general; however, various pollutants and corrosive products have affected the engraved patterns, requiring conservation treatment. Furthermore, a non-destructive analysis was conducted to identify the components of the materials and the manufacturing techniques used in the ornament. The Yongjam is hollow inside to reduce its weight when placed in the hair and has a color contrast of gold, red, and black. The decorative part and the body were made separately. That is, the body was made from an alloy of copper, silver, and zinc, and its joint was elaborately connected without any overlaps. In the decorative part, different alloy ratios were identified in the dragon's face, beard, horn, body, and fin. Further, for the dragon's face with its delicate patterns, an alloy of silver and copper was used, likely to make the face appear as realistic as possible.