• Title/Summary/Keyword: 비금속개재물

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Study on the Manufacturing Technology Applied on Iron Axes of Proto-Three Kingdoms excavated from Yangchon, Gimpo (김포 양촌유적 출토 원삼국시대 철부에 적용된 제작기술 검토)

  • Yu, Jae Eun;Lee, Jae Sung
    • Journal of Conservation Science
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    • v.29 no.4
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    • pp.367-378
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    • 2013
  • Microstructures and nonmetallic inclusions of five forged iron axes and one cast iron axe were analyzed. The axes were excavated from the Proto-Three Kingdom Period site located in Yangchon, Gimpo. The forging objects were made of almost pure iron and low carbon steel, and only one among five were quenched after its figuration. Malleable cast iron structures showing on the casting suggest that the decarbonized casting method were applied. According to the results of nonmetallic inclusion analysis, the axes were produced by hammering the iron bloom which was attained with low-temperature -solid-reduction-method. Showing higher Fe content over $SiO_2$, it is assumed that the re-collecting rate of Fe was low because of the insufficient forging temperature and the impurities were included during the smelting process. It is assumed that the lime was used as a preparation because of detecting high Ca contents.

라멜라 균열(Lamellar tearing)의 발생기구와 방지대책

  • 고진현
    • Journal of Welding and Joining
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    • v.5 no.4
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    • pp.1-11
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    • 1987
  • 라멜라 균열은 복잡한 현상이며 1960년대부터 연구가 되어 왔지만 국내에서는 그 중요성을 인정하면서도 연구가 되지 않았기 때문에 본 해설에서는 라멜라 균열에 대한 전반적인 이해를 돕기 위해, 라멜라 균열에 미치는 인자 및 비금속개재물, 형성기조, 개시온도 및 시간 그리고 방지책과 재료의 라멜라 균열에 대한 민감성을 평가하는 시험 방법과 용접구조물에서 라멜라 균열의 중요성 등을 기술하고저 한다.

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Determination of Lamellar Tearing Initiation Temperatures and the Effect of Non-metallic Inclusions on Tear (라멜라균열의 생성온도와 비금속개재물의 영향)

  • 고진현
    • Journal of Welding and Joining
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    • v.10 no.2
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    • pp.43-50
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    • 1992
  • This study was aimed at resolving uncertainties about lamellar tearing initiation temperatures and studying the effect of nonmetallic inclusions on the tear initiation. In order to measure the lamellar tearing initiation temperature, the slice bend test was conducted in the temperature range of 20.deg.C to 425.deg.C on A572 Grade 50 and A588 Grade A steels. In addition, the weld restrain test was carried out to measure directly the tear initiation temperature with A572 steel. In slice bend tests, A572 steel showed the most susceptible region to lamellar tearing to be in the range of 100 to 300.deg.C, where the steel showed the minimum ductility. The observed tear initiation by the weld restraint test was to be in the range of 200to 300.deg.C. The tears became narrower and less rounded at the susceptible temperatures. It was confirmed in this study that lamellar teraring initiated during cooling from welding in the range of 200 to 300.deg.C and they were initiated by strain aging embrittlement.

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A Study on the Metallurgical Characteristic of Hammer Scale Produced through Traditional Iron-making Experiments (전통 제철실험을 통해 생산된 단조박편의 재료과학적 특성 연구)

  • Cho, Sung Mo;Cho, Nam Chul
    • Journal of Conservation Science
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    • v.37 no.6
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    • pp.738-747
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    • 2021
  • This study attempted to investigate the metallurgical characteristic through material scientific analysis of hammer scale produced as a direct smelting method restoration experiment for each raw material of iron. To this end, four hammer scale groups were set up, respectively, by experimenting with Gyeongju-Gampo Iron sand and Yangyang Iron ore. For the analysis, principal component analysis, compound analysis, microstructure observation, and chemical composition were confirmed. As a result of principal component analysis, as forging and refining progressed, the content of Fe increased and the content of non-metallic objects decreased. As a result of compound analysis, iron oxide-based compounds were identified. As a result of confirming microstructure and chemical composition, Wüstite and Fayalite were observed overall, and agglomerated Wüstite were observed in some. Magnetite on shape of polygon and pillar was observed. In addition, it was confirmed that internal defects, impurities, and non-metallic interventions gradually decreased. In the future, it is necessary to investigate the metallurgical characteristic through material scientific analysis of hammer scale produced through restoration experiments using various raw material of iron, and compare them with those excavated from Iron manufacture ruins.

A Study on Iron Manufacturing and Technology through Analysis Reports of Iron artifacts in the Baekje Area (유물분석 자료를 통한 백제지역의 제철과 철기 제작기술 연구)

  • Kim, Soo-Ki
    • Journal of Conservation Science
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    • v.30 no.4
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    • pp.335-343
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    • 2014
  • This study classified the result of non-metallic inclusion analysis and result of microstructure investigation on the ironware excavated in the Baekje region into Han River, Geum River, and Yeongsan River to estimate the iron making temperature and study the characteristics of regional and temporal characteristics of the heat treatment technology and steel making technology. Regardless of era, bloom iron and sponge iron are judged to be the major method for making as a directreduction process in all three regions. The result of the reinterpretation of the non-metallic inclusion by the oxide ternary constitutional diagram suggest that the temperature inside of the furnace is estimated to be between $1,100{\sim}1,300^{\circ}C$ while making the steel. The magnetic iron ores are the major raw material of steel ore and irons with high $TiO_2$ are estimated to use iron sands. Ironware with $CaO/SiO_2$ rate higher than 0.4% are considered to have artificially added the flux of calcareous materials. It was found that the iron making method is the solid caburizing-steel which caburizes low-carbon steels by the CO gas and $CO_2$ gas created when heating the forging furnace with charcoal. Also, the ironware manufacturers in the Baekje during 3rd century recognized the heat treatment technology as they performed carburizing process and quenching to intentionally increase the strength of necessary parts.

Effect of non-metallic inclusion on susceptibility to lamellar tearing (라멜라 테어 발생감수성에 미치는 비금속개재물의 영향)

  • 방국수;이종봉
    • Journal of Welding and Joining
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    • v.3 no.1
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    • pp.3-10
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    • 1985
  • Lamellar tearing susceptibility and through-thickness tensile ductility have been investigated in $40kg/mm^2 and 50kg/mm^2$ class tensile strength steel plates in terms of cleanliness of non-metallic inclusion and welding condition. The plate which had 0.01% cleanliness of A-type inclusion (MnS) had 61% of the reduction of area in the through-thickness direction and did not show lamellar tearing. Lamellar tearing susceptibility decreased with increasing the preheat and interpass temperature. The plate which had 0.04% cleanliness of A-type inclusion did not show lamellar tearing under the condition of 75.deg. C of preheat and interpass temperature.

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A Study of Manufacturing Techniques based on Classification by Uses of Excavated Iron Objects from the Remains in Geumcheok-ri, Gyeongju (경주 금척리 유적 출토 철기의 용도별 분류에 따른 제작기법 고찰)

  • You, Ha Rim;Cho, Nam Chul;Shin, Yong Bi
    • Journal of Conservation Science
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    • v.38 no.3
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    • pp.217-233
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    • 2022
  • The remains found in Geumcheok-ri, Gyeongju are located in close proximity to the Ancient Tombs in Geumcheok-ri, Gyeongju (Historic Site) which were built between the late 5th and early 6th centuries, and these tombs are known to belong to the powerful rulers of that area. Using metallurgical techniques, this study was conducted on the iron objects obtained from the excavated remains in Geumcheok-ri, Gyeongju which are presumed to have a close relation to the nearby ruins that played an important role in the growth of Silla. To identify differences in manufacturing techniques based on the purpose of the iron objects, eight objects were selected after classifying them by use and the microstructure and non-metallic inclusions were investigated. The analyses results confirmed that the manufacturing process involved forging iron with a high or low carbon content to produce a particular shape, and that the carburization process was applied to iron post forging a shape to increase its strength when necessary. The mechanical properties were improved by selectively applying the steelmaking method and the heat treatment technique considering the functions of the parts, and the low temperature reduction was applied to the smelting process. Furthermore, in comparison with the iron objects excavated from the remains located in the center of Gyeongju and its outskirts, it is confirmed that there is similarity in the smelting and manufacturing techniques between these objects.