• Title/Summary/Keyword: 불확도 평가

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Measurement of Traceability Error for Calibration Service Center Using Type S Thermocouples (S형 열전대를 이용한 교정검사기관의 소급성 오차측정)

  • Gam, Kee-Sool;Kim, Yong-Gyoo;Kim, Sun-Gon
    • Journal of Sensor Science and Technology
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    • v.4 no.1
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    • pp.43-50
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    • 1995
  • We measured the traceability error for nine high temperature calibration service centers including KRISS through the round-robin test. In this test the type S thermocouple, which used as a calibration standard thermometer commonly, was accommodated as a test thermocouple. Intercomparison data of three institutions were coincident with KRISS's data within ${\pm}0.5^{\circ}C$, which was the calibration uncertainty of the type S thermocouple, but the remaining six institution's data were deviated from the assigned uncertainty level. Deviation of the intercomparison data increased gradually according to the increase of the test temperature. and the maximum difference was so large as about $2.0^{\circ}C$ at the highest test temperature, gold point. In this study we found the traceability error of high temperature calibration service center for a high temperature standard was within $2.0^{\circ}C$.

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Realization of the national standard of candela traceable to the absolute cryogenic radiometer at KRISS (극저온 절대복사계에 소급한 칸델라 국가표준 실현)

  • Park, Seung-Nam;Kim, Yong-Wan;Lee, Dong-Hoon
    • Korean Journal of Optics and Photonics
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    • v.15 no.5
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    • pp.443-448
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    • 2004
  • We realized the national standard of the candela, one of the SI units, by using two photometers with the spectral responsivity measured in reference to the absolute cryogenic radiometer. The external apertures of the photometers were fabricated using a diamond turning machine, and measured in terms of area with uncertainty of 0.05 %(k = 1). The candela is realized using a 1 kW FEL lamp and the characterized photometers on an optical bench. The uncertainty is budgeted to be 0.25 %(k = 1) considering the uncertainty of the spectral responsivity and the response uniformity of the detectors, the area of the external apertures, the color temperature of the lamp, and the positioning reproducibility of the photometers and the lamp. We verified the realized scale by comparing with the scale of National Institute of Standards and Technology, USA. They coincided with each other within 0.1%.

Performance Characteristics of Thrust Measurement System for Hot-Firing Test of Small Liquid Propulsion Engines (소형 액체 추진기관 연소 시험을 위한 추력 측정 장치의 성능 특성 연구)

  • Kim, In-Tae;Huh, Hwan-Il;Kim, Jeong-Soo;Jang, Ki-Won;Lee, Jae-Won
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.32 no.9
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    • pp.122-129
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    • 2004
  • An accurate thrust measurement is one of the critical paths to the successful test and evaluation program of small liquid propulsion engines. This study describes the design factors for the development of thrust measurement system (TMS) as well as manufacturing practice of TMS hardware. We investigate characteristics of the TMS and its performance through hot-firing test of small liquid engine in a vacuum test cell which is capable of simulating 100,000 ft of altitude or higher. For performance test of TMS, we measure thrusts by changing propellant injection pressure at steady state firing mode as well as at pulse firing mode. Measured eigen frequency of the TMS is 67 Hz. Linearity test of the TMS shows good performance with less than 0.5% of linearity error.

Preparation of a CRM for QA/QC in dioxin analysis and inter-laboratory study (다이옥신 정도 관리용 CRM 제조와 실험실간 비교평가)

  • Yu, Byeong-Woon;Moon, Young-Hoon;Kim, Min-Kwan;Kyoung, Jong-Dai;Chang, Yoon-Seok
    • Analytical Science and Technology
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    • v.17 no.2
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    • pp.153-162
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    • 2004
  • Dioxin CRM for QA/QC was prepared with fly ash collected from municipal waste incinerator. With that CRM inter-laboratory test was carried out. The collected fly ash was conducted several homogeneity steps including sievings and mixing. Homogeneity test and estimation of uncertainty was performed by one-way ANOVA based on ISO guide 35. Compared concentrations of fly ash of participants to CRM values, PCDDs value was lower than that of CRM in almost participants, and showed higher PCDFs concentration than that of CRM. Although there is a small difference in PCDD/Fs concentrations with congeners of extract, the result was close to mean value.

Applicability test of broad leaf samples stored at the NESB for biomonitoring of airborne pollutants (국가환경시료은행 활엽 시료를 활용한 지역별 대기침적 오염물질 모니터링 활용성 검토)

  • Lee, Jongchun;Lee, Jangho;Park, Jong-Hyouk;Lee, Eugene;Shim, Kyuyoung;Jang, Heeyon
    • Journal of Environmental Impact Assessment
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    • v.25 no.6
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    • pp.532-541
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    • 2016
  • The National Environmental Specimen Bank (NESB) has been collecting broad leave samples to monitor environmental pollution from five different designated sampling areas. In order to ensure the reproducibility and comparability of the results, all the procedures from selecting trees and pooling leaves to make the representative sample are defined in the standard operation procedures(the SOP). The representative samples were subjected to the chemical analyses for some heavy minerals and Polycyclic Aromatic Hydrocarbons(PAHs). The uncertainty levels involved in each step of the SOP, that is, the sampling and the chemical analysis, were derived using the Robust ANOVA, which enables the relative comparison among the different levels of pollutants concentrations with confidence. Furthermore, the effect of the varying degrees of precipitation on the pollutants concentration of the leaves was also examined. Overall, the biological difference estimated from the duplicate samples was found to exceed the variation across the site, implying even aerial deposition over site. Samples from Gwanak Mt. showed highest heavy metal concentrations than the other sites. Washing off effect of the pollutants adhering in the form of particles on the leaf surface was found to be affected by the cumulative precipitation.

Study on the Measurement of TMP Pumping Speed (터보분자펌프(TMP) 배기속도 측정에 관한 고찰)

  • Kang, S.B.;Shin, J.H.;Cha, D.J.;Koh, D.Y.;Cheung, W.S.;Lim, J.Y.
    • Journal of the Korean Vacuum Society
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    • v.19 no.4
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    • pp.249-255
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    • 2010
  • Methods of the characteristics evaluation of turbo-molecular pumps (TMP) are well-defined in the international measurement standards such as ISO, PNEUROP, DIN, JIS, and AVS. The Vacuum Center in the Korea Research Institute of Standards and Science (KRISS) has recently designed, constructed, and established the integrated characteristics evaluation system of TMPs based on the international documents by continuously pursuing and acquiring the reliable international credibility through measurement perfection. The measurement of TMP pumping speed is normally performed with the throughput and orifice methods dependent on the mass flow regions. However, in the UHV range of the molecular flow region, the high uncertainties of the gauges, mass flow rates, and conductance are too critical to precisely accumulate reliable data. In order to solve the uncertainty problems of pumping speeds in the UHV range, we introduced a SRG with 1% accuracy and a constant volume flow meter (CVFM) to measure the finite mass flow rates down to $10^{-1}$ Pa-L/s with 3% uncertainty for the throughput method. In this way we have performed the measurement of pumping speed down to $10^{-4}$ Pa with an uncertainty of less than 6% for a 1000 L/s TMP. In this article we suggest that the CVFM has an ability to measure the conductance of the orifice experimentally with flowing the known mass through the orifice chambers, so that we may overcome the discontinuity problem encountering during introducing two measurement methods in one pumping speed evaluation sequence.

Comparison between Uncertainties of Cultivar Parameter Estimates Obtained Using Error Calculation Methods for Forage Rice Cultivars (오차 계산 방식에 따른 사료용 벼 품종의 품종모수 추정치 불확도 비교)

  • Young Sang Joh;Shinwoo Hyun;Kwang Soo Kim
    • Korean Journal of Agricultural and Forest Meteorology
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    • v.25 no.3
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    • pp.129-141
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    • 2023
  • Crop models have been used to predict yield under diverse environmental and cultivation conditions, which can be used to support decisions on the management of forage crop. Cultivar parameters are one of required inputs to crop models in order to represent genetic properties for a given forage cultivar. The objectives of this study were to compare calibration and ensemble approaches in order to minimize the uncertainty of crop yield estimates using the SIMPLE crop model. Cultivar parameters were calibrated using Log-likelihood (LL) and Generic Composite Similarity Measure (GCSM) as an objective function for Metropolis-Hastings (MH) algorithm. In total, 20 sets of cultivar parameters were generated for each method. Two types of ensemble approach. First type of ensemble approach was the average of model outputs (Eem), using individual parameters. The second ensemble approach was model output (Epm) of cultivar parameter obtained by averaging given 20 sets of parameters. Comparison was done for each cultivar and for each error calculation methods. 'Jowoo' and 'Yeongwoo', which are forage rice cultivars used in Korea, were subject to the parameter calibration. Yield data were obtained from experiment fields at Suwon, Jeonju, Naju and I ksan. Data for 2013, 2014 and 2016 were used for parameter calibration. For validation, yield data reported from 2016 to 2018 at Suwon was used. Initial calibration indicated that genetic coefficients obtained by LL were distributed in a narrower range than coefficients obtained by GCSM. A two-sample t-test was performed to compare between different methods of ensemble approaches and no significant difference was found between them. Uncertainty of GCSM can be neutralized by adjusting the acceptance probability. The other ensemble method (Epm) indicates that the uncertainty can be reduced with less computation using ensemble approach.

Correlations between the Important Physical Properties of Natural Gas (천연가스 주요 물성 간의 상관식)

  • Ha, Youngcheol;Lee, Seongmin;Her, Jaeyoung;Lee, Kangjin;Lee, Seungjun
    • Korean Chemical Engineering Research
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    • v.47 no.5
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    • pp.599-607
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    • 2009
  • This study was conducted to derive the five correlations which could predict specific gravity(or heating value), compression factor, density, etc., if we know heating value or specific gravity only. To make a sufficient number of raw data for regression, SGERG EOS was modified into equation of heating value. Based on these raw data, five correlations were obtained and the uncertainties of the correlations were evaluated. The results showed that the uncertainties were near 0.1% in most conditions of natural gas and so the correlations could be used in natural gas industry and academic fields.

Uncertainty evaluation in electrochemical noise resistance measurement (전기화학적 노이즈 저항 측정에서의 불확도 평가)

  • Kim, Jong Jip;Kang, Su Yeon
    • Corrosion Science and Technology
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    • v.12 no.5
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    • pp.220-226
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    • 2013
  • The uncertainty in statistical noise resistance measurement was evaluated for a type 316 stainless steel in NaCl solutions at room temperature. Sensitivity coefficients were determined for measurands or variables such as NaCl concentration, pH, solution temperature, surface roughness, inert gas flow rate and bias potential amplitude. The coefficients were larger for the variables such as NaCl concentration, pH, inert gas flow rate and solution temperature, and they were the major factors increasing the combined standard uncertainty of noise resistance. However, the contribution to the uncertainty in noise resistance measurement from the above variables was remarkably low compared to that from repeated measurements of noise resistance, and thus, it is difficult to lower the uncertainty in noise resistance measurement significantly by lowering the uncertainties related with NaCl concentration, pH, inert gas flow rate and solution temperature. In addition, the uncertainty in noise resistance measurement was high amounting to 17.3 % of the mean, indicating that the reliability in measurement of noise resistance is low.

Uncertainty Assessment for CAPSS Emission Inventory by DARS (DARS에 의한 CAPSS 배출자료의 불확도 평가)

  • Kim, Jeong;Jang, Young-Kee
    • Journal of Korean Society for Atmospheric Environment
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    • v.30 no.1
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    • pp.26-36
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    • 2014
  • The uncertainty assessment is important to improve the reliability of emission inventory data. The DARS (Data Attribute Rating System) have recommended as the uncertainty assessment technic of emission inventory by U.S. EPA (Environmental Protection Agency) EIIP (Emission Inventory Improvement Program). The DARS score is based on the perceived quality of the emission factor and activity data. Scores are assigned to four attributes; measurement/method, source specificity, spatial congruity and temporal congruity. The resulting emission factor and activity rate scores are combined to arrive at an overall confidence rating for the inventory. So DARS is believed to be a useful tool and may provide more information about inventories than the usual qualitative grading procedures (e.g. A through E). In this study, the uncertainty assessment for 2009 CAPSS (Clean Air Policy Support System) emission inventory is conducted by DARS. According to the result of this uncertainty assessment, the uncertainty for fugitive dust emission data is higher than other sources, the uncertainty of emission factor for surface coating is the highest value, and the uncertainty of activity data for motor cycle is the highest value. Also it is analysed that the improvement of uncertainty for activity data is as much important as the improvement for emission factor to upgrade the reliability of CAPSS emission inventory.