• Title/Summary/Keyword: 분별결정화

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Manufacture of High Purity KI Crystal by Fractional Crystallization Method from Aqueous Waste of KI (KI 폐용액(廢溶液)으로부터 분별결정법(分別結晶法)에 의한 고순도(高純度) KI결정(結晶) 제조(製造)에 관한 연구(硏究))

  • Kim, Dae Weon;Jang, Seong Tae;Choi, Sung Bum
    • Resources Recycling
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    • v.22 no.1
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    • pp.48-54
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    • 2013
  • A laboratory study was carried out to recover KI crystals with high purity by using fractional crystallization method from a waste solution generated from the production of polarizing film for LCD industry. The waste solution contains 1.3% KI, and other impurities such as B, Na, and PVA etc. With purity higher than 99.5% KI crystals were produced through refining process such as vacuum evaporation, fractional crystallization, filtering, and 24hr aging. Also the concentrated impurities were eliminated about 70% by recrystallization.

Recovery of Neodymium from NdFeB Oxidation-Roasted Scrap by Acetic Acid Leaching (NdFeB계 영구자서 산화배소 스크랩의 초산침출에 의한 네오디뮴 회수)

  • Yoon, Ho-Sung;Kim, Chul-Joo;Kim, Joon-Soo
    • Resources Recycling
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    • v.13 no.6
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    • pp.43-48
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    • 2004
  • For the separation of neodymium from NdFeB permanent magnet scrap, the scrap was roasted for oxidizing, and leached with acetic acid followed by fractional crystallization for selective separation. From the analysis results of the leached solution, the optimum condition for the recovery of neodymium was found that leaching temperature, leaching time and pulp density are 80$^{\circ}C$, 3 hours, and 35%, respectively. At this optimum condition, more than 90% of neodymium could be recovered. Concentration of neodymium acetate in acetic acid. The optimum condition for the recovery of neodymium acetate crystal from the leached solution was that the initial leaching solution was evaporated until the remaining volume was about 1/5 of the initial volume. At this condition, 67.5% of neodymium was recovered from the leached solution. The neodymium remaining in the concentrated solution was recovered by reacting it with oxalic acid.

Petrochemical Study of the Gadaeri Granite in Ulsan Area, Kyeongsang Province (경상남도 울산지역 가대리화강암에 대한 암석화학적 연구)

  • Choi, Seon-Gyu;Wee, Soo-Meen
    • Economic and Environmental Geology
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    • v.27 no.5
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    • pp.459-467
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    • 1994
  • The Gadaeri granite near Ulsan mine is an oval-shape isolated granitic body, and is genetically related to the iron-tungsten mineralization. The Gadaeri granite exhibits calc-alkaline and I-type characteristics, and generally shows the micrographic texture which indicates the shallow depth of emplacement. Consideration of the stratigraphic thickness of Ulsan formation and minimum-melt compositions suggests that the bulk magma crystallized at pressure of 0.5~2.0 kbar under water saturated condition. The evolutionary trend observed in the studied rocks represents that feldspar fractional crystallization has been a major magmatic process at the Gadaeri granite pluton. Different chemical characteristics between the Gadaeri and the Masan-Kimhae granites cannot be explained by fractional crystallization or different degrees of partial melting, and it reflects that the magma source for Gadaeri granite was different from that of the Masan and Kimhae granites.

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Recovery of High Purity KI Crystal from Aqueous Waste of Polarizing Film Manufacturing Process (LCD용(用) 편광(偏光)필름제조폐용액(製造廢溶液)으로부터 고순도(高純度) KI결정(結晶) 회수(回收)에 관한 연구(硏究))

  • Kim, Dae-Weon;Jang, Seong-Tae;Choi, Soon-Ryung
    • Resources Recycling
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    • v.21 no.2
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    • pp.53-58
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    • 2012
  • A laboratory study was carried out to recover KI crystals with high purity from a waste solution generated from the production of polarizing film for LCD industry. The waste solution contains 1 to 4% KI, and other impurities such as B, PVA and etc. More than 95% purity of KI crystals were produced through refining process such as vacuum evaporation and fractional crystallization. Most of B compounds and impurities were removed by concentrating the waste solution until KI content reached about 50%. The KI crystals were washed with solvents to remove most of PVA which gave result in producing 99.5% purity of crystals. The overall recovery of KI was about 90% during the concentration process.

Web Document Classification Based on Hangeul Morpheme and Keyword Analyses (한글 형태소 및 키워드 분석에 기반한 웹 문서 분류)

  • Park, Dan-Ho;Choi, Won-Sik;Kim, Hong-Jo;Lee, Seok-Lyong
    • The KIPS Transactions:PartD
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    • v.19D no.4
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    • pp.263-270
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    • 2012
  • With the current development of high speed Internet and massive database technology, the amount of web documents increases rapidly, and thus, classifying those documents automatically is getting important. In this study, we propose an effective method to extract document features based on Hangeul morpheme and keyword analyses, and to classify non-structured documents automatically by predicting subjects of those documents. To extract document features, first, we select terms using a morpheme analyzer, form the keyword set based on term frequency and subject-discriminating power, and perform the scoring for each keyword using the discriminating power. Then, we generate the classification model by utilizing the commercial software that implements the decision tree, neural network, and SVM(support vector machine). Experimental results show that the proposed feature extraction method has achieved considerable performance, i.e., average precision 0.90 and recall 0.84 in case of the decision tree, in classifying the web documents by subjects.

Optimization the Xylose Fractionation Conditions of Pepper Stem with Dilute Sulfuric Acid (농업부산물 고추대 (Pepper Stem)을 이용한 묽은 황산 자일로즈 분별공정의 최적화)

  • Won, Kyung-Yoen;Oh, Kyeong-Keun
    • KSBB Journal
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    • v.24 no.4
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    • pp.361-366
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    • 2009
  • Response surface methodology (RSM) was used for optimization the fraction conditions of xylose from pepper stem with dilute sulfuric acid. The independent variables were acid concentration in the range of 1.134 to 2.866%, reaction temperatures in the range of 142.68 to $177.32^{\circ}C$, and hydrolysis time in the range of 6.34 to 23.66 min. were studied. The dependent variables were xylose yield from pepper stem, and the production of by-products, for example, furfural, acetic aicd, HMF etc. Experimental results had a good match with statistical result. The maximum xylose yield obtained in this experiment was 71% concentration.

Rb-Sr Whole-rock Isochron Age and Petrology of the Mt. Geumjeong Granite, Busan (부산 금정산화강암체의 암석학 및 Rb-Sr 전암 등시선 연대)

  • Yun Sung-Hyo;Koh Jeong-Seon;Park Kwang-Sun;Ahn Hyo-Chan;Kim Young-Il;Yoo Sung-Hyeon;Lee Dong-Han;Yun Gi-Young
    • The Journal of the Petrological Society of Korea
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    • v.14 no.1
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    • pp.61-72
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    • 2005
  • The granitoids in the Mt. Geumjeong, Busan can be divided into granodiorite, hornblende granite, adamellite, tonalite, biotite granite and micrographic granite. The geochemical characteristics of the Mt. Geumjeong granites indicate that they were crystallized from a calc-alkaline series and that they belong to Ⅰ-type granitic rocks which evolved from granodioritic magma into hornblende granite, adamellite, biotitie granite, and finally micrographic granite through fractional crystallization of plagioclase. The crystallization pressures and temperatures of the minimum melt compositions of the granitic rocks were estimated to about 1∼5 kbar and 720∼700℃. The trace element composition and REE patterns, characterized by a high LILE/HFSE ratio and enrichments in LREE, indicate typical continental margin arc calc-alkaline rocks produced in the subduction environment. The Rb-Sr isotopic data for the Mt. Geumjeong granites define a well-defined isochron yielding as age of 69.6±1.9 Ma with an initial Sr isotopic ratio of 0.70503.

The Tire Damage Classification by Pulse Interval Time Density Function of Ultrasonic Wave Envelope on Driving (주행 중 타이어 손상에 의해 발생하는 초음파 포락선 신호의 펄스 간격 시간밀도함수에 의한 손상 분별)

  • Shin, Seong-Geun;Kang, Dae-Soo
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.11 no.3
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    • pp.41-46
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    • 2011
  • The tire damage classification method is researched by periodicity detection of ultrasonic envelope signals to occur at the driving vehicle tire. Because periodic signals is generated by rotations of the damaged tire, it should convert to pulse for using the density function. After time intervals of pulses are represented by the density function, the dominant periodicity is detected. The threshold to make a pulse is calculated by moving average of envelope signals. The result of time density function in case of one damage material, the first peak's time is equals to tire's rotation period, 162ms and 102ms, about the speed of 50km/h and 80km/h. In case of more than one damage material, the sum of each peak's time is equals to tire's rotation period about the speed.

Analysis on characteristics of shape indices through the comparison of regional woodland patches (지역별 산림패치 비교를 통한 형태지수의 특성분석)

  • Kim, Keun-Ho
    • Journal of Korean Society of Rural Planning
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    • v.16 no.1
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    • pp.63-71
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    • 2010
  • 지난 수십 년 동안 형태지수는 패치의 복잡성을 정량화하여 생물종 다양성 보존과 같은 경관생태계획에 활용되어 왔다. 지역계획 연구자들이나 정책결정자들에게 경관구조와 패턴을 정량화하는 경관생태지수는 대상지역을 모니터링할 수 있는 하나의 수단으로 활용되어 왔다. 그러나 경관생태지수관련 연구를 살펴보면 연구 목적 및 범위에 따라 활용하는 경관생태지수의 종류가 매우 다양하고 복잡한 것을 알 수 있다. 또한 연구목적에 적합한 경관생태지수를 선정하는 것은 복잡한 수학분석과 함께 많은 주의가 필요한 것을 알 수 있다. 따라서 본 연구에서는 형태지수들을 도시지역, 도시외곽지역, 농촌지역 그리고 산림지역 등 4군데 사례지역에 적용하여 그 결과를 통해 형태지수들의 특성을 살펴보았다. 그 결과, 평균형태지수값(MSI)에서는 도시외곽지역이 가장 높게 나타났고, 평균프랙텔차원지수(MPFD)에서는 농촌지역이 높게 나타났다. 넓은 면적을 가진 패치에 가중점을 고려한 평균형태지수값(AWMSI)과 평균프랙텔차원지수값(AWMPFD)에서는 산림지역이 가장 높게 나타났다. 사용한 네 가지 형태지수값의 순위가 4군데 사례지역에서 다르게 나타났다. 특히 둘레와 면적의 로그전환을 이용하고 있는 프랙텔차원지수들의 경우, 도시와 도시외곽지역의 MPFD값은 같고, 도시외곽지역, 농촌지역과 산림지역의 AWMPFD값 차이는 적어 순위 분별력이 떨어졌다. 따라서 넓은 면적을 가진 패치에 가중점을 고려한 평균형태지수(AWMSI)가 지역별 산림패치의 복잡성을 잘 정량화할 수 있음을 본 연구결과에서 보여주고 있다.

Determining a Syntactic Case of Auxiliary Postposition for Improving Accuracy of Polysemy Word-Sense-Disambiguation (다의어 분별 정확률 개선을 위한 보조사의 통사격 결정)

  • Shin, Joon-Choul;Ock, Cheol-Young
    • 한국어정보학회:학술대회논문집
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    • 2016.10a
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    • pp.102-104
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    • 2016
  • 하위범주화는 술어와 보어간의 의존 관계를 정의하는 언어정보로서 다의어 태깅이나 이 외에 자연어처리의 다양한 곳에 이용될 수 있다. 그러나 하위범주화에서 다루는 필수논항은 격조사로 표현되어 실제로 한국어에서 자주 나타나는 보조사는 여기에 포함되지 않는다. 이런 문제 때문에 하위범주화네 나타난 격조사만을 그대로 이용하려고 하면 재현율에 큰 문제가 발생하게 된다. 본 논문에서는 문장에서 격조사 대신 보조사가 사용되었을 때 하위범주화의 필수논항으로 인정할 수 있는 방법을 제시하고, 특히 보조사에 적용할 경우에 생기는 이점을 실험으로 증명한다.

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